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recovery of metals from Anodic Dissolution Slime of Waste from Electric and Electronic Equipment（WEEE） by Extraction in Ionic Liquids

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Chemical Research in Chinese Universities 2018年第1期34卷 113-118页

作者： Ana Maria POPESCU Kazimir YANUSHKEVICH Vasile SOARE Cristina DONATH Elena Ionela NEACSU Virgil CONSTANTIN "Ilie Murgulescu" Institute of Physical Chemistry of Romanian Academy Laboratory of Electrochemistry and Corrosion Splaiul lndependentei 202 Bucharest 060021 Romania Scientific-Practical Materials Research Centre National Academy of Belarus P. Brovki 19 str. 220072 Minsk Belarus National R&D Institute for Nonferrous and Rare metals-IMNR 102 Biruintei Blvd. Pantelimon Ilfov County Romania

The recovery of metals from a multi-component alloy obtained by crushing, melting and anodic dissolution of waste from electric and electronic equipment（WEEE） was investigated. The anodic dissolution of the alloy was carried out in an electrolysis cell with one copper cathode and a central cast anode, immersed in the electrolyte formed by choline chloride-ethylene glycol-iodine. The temperature of the electrolyte during the process was 343 K. Depending on the electrolysis parameters（current density and cell voltage）, cathodic deposits of Sn, Pb and Zn of 〉99% purity were obtained. Cyclic voltammetry was used in order to determine the deposition potentials of the studied metals. The obtained metallic deposits were subject of determination of XRD, SEM/EDX and AFM in order to evidence the deposits structure and morphology. The experiments performed demonstrated the possibility of separating/selective recovery of metals from the multi-component alloy resulted from the waste from electrical and electronic equipment by anodic dissolution in ionic liquids.

关键词： metals recovery Ionic liquid Waste from electric and electronic equipment(WEEE)

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Microbial Community with Potential for Metal Release Isolated from Palca Mine Tailings Pond in Peru

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Journal of Geoscience and Environment Protection 2024年第7期12卷 109-121页

作者： César Wilber Guzmán Moreno Bruno Karolski Solange Kazue Utimura Roberto Castellanos Cabrera Jhon Albert Centeno Torres Daladier Miguel Castillo Cotrina Elisabete de Santis Braga Dayana Sarai Gamonal Fermandez Denise Crocce Romano Espinosa Joel Barbujiani Sigolo Department of Sedimentary and Environmental Geology Institute of Geoscience USP So Paulo Brazil Department of Chemical Engineering LAREX USP So Paulo Brazil CEPEMA Environment Training and Research Center USP So Paulo Brazil Facultad de Ciencias Universidad Nacional Jorge Basadre Grohmann UNJBG Tacna Per Department of Physical Chemical and Geological Oceanography USP So Paulo Brazil Facultad de Ciencias Biolgicas Universidad Nacional Pedro Ruiz Gallo UNPRG Lambayeque Per

The improvement of microbial characterization has increased the comprehension of microbial population and their ability in the microbiological metal dissolution. Bioleaching processes have been expanded to use microorganisms for the recovery of metals from ores and wastes. This study introduces Palca mine tailings pond in Peru which turned into acid mine drainage (AMD). AMD is a source of microbial communities whose microorganisms may support the aqueous extractive metallurgy for metal recovery. Four samples of AMD were collected from different locations and the elemental characterization showed concentrations of metals, such as Cu, Zn, Al, Mn, and Fe. The pH of the samples showed variation between 1.9 - 6.8. Twenty-one microorganisms were isolated and selected according the cell morphology. 16s rRNA gene sequences identified five species of which three belong to the bacterial kingdom and two to the Fungi kingdom. Two of the bacterial species were ferrous ion oxidizing bacteria, identified as Acidithiobacillus ferriphilus and Acidithiobacillus ferridurans;and the other one a ferric ion reducing bacteria identified as Acidiphilium acidophilum. The fungi species identified were Rhodotorula sinensis and Exophiala xenobiotica, a filamentous fungus isolated for the first time from an AMD.

关键词： Acidophilic Microorganisms Acid Mine Drainage—AMD Bioleaching Process metals recovery Acidithiobacillus

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Enhanced recovery of zinc and lead by slag composition optimization in rotary kiln

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Transactions of Nonferrous metals Society of China 2022年第9期32卷 3110-3122页

作者： Hong-fu LIN Wei WENG Shui-ping ZHONG Guan-zhou QIU School of Minerals Processing and Bioengineering Central South UniversityChangsha 410083China State Key Laboratory of Comprehensive Utilization of Low Grade Refractory Gold Ores Zijin Mining Group Co.Ltd.Shanghang 364200China Zijin School of Geology and Mining Fuzhou UniversityFuzhou 350108China

High-efficiency recovery of Zn and Pb from silicon-rich zinc leaching residues is realized in a rotary *** by means of XRD,SEM,EDS and ICP reveal that the leaching residue contains 12.4 wt.%SiO_(2),16.1 wt.%Zn,and 7.4 wt.%*** analysis shows that metallic vapor of Zn and Pb can be easily generated from the zinc leaching residue at 1150-1250°C inside the rotary *** and melting points of 13 slag compositions were analyzed and three slag compositions(47wt.%SiO_(2)-23wt.%CaO-30wt.%FeO,40wt.%SiO_(2)-28wt.%CaO-32wt.%FeO,and 40wt.%SiO_(2)-30wt.%CaO-30wt.%FeO)possessed the desirable physical properties,with the melting point and viscosity in the range of 1150-1280°C and 0.2-0.5 Pa·s,*** industrial tests show that adopting the optimized slag composition can contribute to very high recovery rates of Zn and Pb(97.3%for Zn and 94.5%for Pb),corresponding to slags with very low average contents of Zn and Pb(0.51 wt.%Zn and 0.45 wt.%Pb).The National-Standard leaching tests of the water-quenched slags result in 1.82 mg/L Zn,~0.01 mg/L Cu,0.0004 mg/L As,~0.01 mg/L Cd,0.08 mg/L Pb,and~0.02 mg/L Hg in the leachate,verifying the detoxification of the zinc leaching residue at the same time.

关键词： zinc leaching residues metals recovery rotary kiln slag composition optimization detoxification

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Electrochemical recycling of Pd and Ag from simulated high-level liquid waste

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Transactions of Nonferrous metals Society of China 2022年第3期32卷 1031-1040页

作者： You-bin WANG Rui ZOU Yue-zhou WEI Tsuyoshi ARAI Toyohisa FUJITA School of Resources Environment and MaterialsGuangxi UniversityNanning 530004China Guangxi Key Laboratory of Processing for Non-ferrous Metal and Featured Materials Guangxi UniversityNanning 530004China Department of Material Science and Engineering Shibaura Institute of TechnologyTokyo 3-9-14Japan

For the recycling of Pd and Ag from high-level liquid waste(HLLW), the electrochemical behaviors of Pd and Ag in the simulated HNO_(3) solutions were investigated by cyclic voltammetry and potentiostatic *** electron microscopy(SEM) and X-ray diffraction(XRD) were used to-observe the deposits morphology and to evaluate their composition. The results indicate that the formation of NO_(2)^(-)electrodeposited. When Pd and Ag are electrodeposited together, more metals are gained in the same time, and the deposited Ag does not dissolve in this situation. The metals are electrodeposited completely at the potentials from -0.4 to -0.6 V(vs MSE) and the deposits contai-n Ag and PdHx. The electrodeposition of Pd can boost h-ydrogen evolution,and then the reaction between H;and NO_(2)^(-)is sped up, thereby lowering the concentration of NO_(2)^(-)and inhibiting the dissolution of Ag.

关键词： electrodeposition metals recovery nitrite generation promoting effect morphology characteristics

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