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Enhanced mechanical property by introducing bimodal grains structures in Cu-Ta alloys fabricated by Mechanical alloying

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Journal of Materials Science & Technology 2024年第5期172卷 104-112页

作者： Ningyu Li Yongqin Chang Mingyang Li Yuxiang Chen Xinrui Luo Shichao Pei Fan Yang School of Materials Science and Engineering University of Science and Technology BeijingBeijing 100083China Xi’an Rare Metal Materials Institute Co.Ltd Xi’an 710016China

Dispersion-strengthened copper alloys can achieve ultra-high strength,but usually at the expense of duc-tility.In this study,a strategy for overcoming strength-ductility tradeoffof Cu alloys is realized through the introduction of bimodal grains structures.Cu-Ta alloys with only 0.5 at.%Ta content were successfully prepared by Mechanical alloying combined with spark plasm sintering.The samples prepared by one-step and two-step ball milling methods are named as Cu-Ta(Ⅰ)and Cu-Ta(Ⅱ),respectively.The microstructural characterizations revealed that ultra-fine equiaxed grains with uniformly dispersed Ta precipitates were obtained in the Cu-Ta alloys.High strength of 377 MPa for yield strength together with elongation of∼8%was obtained in Cu-Ta(Ⅰ).Bimodal grains structures composed of fine-grain zones and coarse-grain zones were successfully introduced into Cu-Ta(Ⅱ)by a two-step ball milling approach,and both yield strength(463 MPa)and elongation(∼15%)were significantly synergistic enhanced.The hardness values of both Cu-Ta(Ⅰ)and Cu-Ta(Ⅱ)were almost kept nearly constant with the increase of annealing time,and the softening temperatures of Cu-Ta(Ⅰ)and Cu-Ta(Ⅱ)are 1018 and 1013℃,reaching 93.9%and 93.5%T m of pure Cu(1083℃),respectively.It reveals that the Cu-0.5 at.%Ta alloys exhibit excellent thermal stability and exceptional softening resistance.Ta nanoclusters with semi-coherent structures play an essential role in enhancing the strength and microstructural stability of alloys.Bimodal structures are beneficial to the activation of back stress strengthening and the initiation and propagation of microcracks,thus obtaining the extraordinary combination of strength and elongation.This study provides a new way to fabricate dispersion-strengthened Cu alloys with high strength,high elongation,excellent thermal stability and softening resistance,which have potential application value in the field of the future fusion reactor.

关键词： Cu-Ta alloy Mechanical alloying Ta precipitates Bimodal structures mechanical property

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Influences of Milling Time and NbC on Microstructure of AlCoCrFeNi_(2.1)High Entropy Alloy by Mechanical alloying

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Journal of Wuhan University of Technology(Materials Science) 2023年第2期38卷 423-429页

作者： LI Li JIANG Hui NI Zhiliang HAN Kaiming WANG Rui WANG Haixia College of mechanical and Electronic Engineering Shandong University of Science and TechnologyQingdao266590China Yangzhou Fengming Photoelectric New Material Co.Ltd Yangzhou225200China

AlCoCrFeNi_(2.1)eutectic high entropy alloy(EHEA)and AlCoCrFeNi_(2.1)-x NbC(x=2.5wt%,5.0wt%,7.5wt%,and 10wt%)high entropy alloy(HEAs)were prepared by Mechanical alloying(MA).The effects of milling time and NbC content on the alloying behavior and grain size of the AlCoCrFeNi_(2.1)EHEA were investigated.The experimental results show that the AlCoCrFeNi_(2.1)EHEA primarily consists of order BCC(B2)and face-centered-cubic(FCC)phases,while the AlCoCrFeNi_(2.1)-x NbC(x=2.5wt%,5.0wt%,7.5wt%,and 10wt%)HEAs are composed of B2,FCC,and NbC phases.With the increase of milling time,the powder goes through three stages,irregularity,cold welding fracture and spheroidization.The particle size of AlCoCrFeNi_(2.1)EHEA powder shows a trend of first increasing and then decreasing.Therein,the particle size presents a normal distribution during 0-50 h alloying.With the addition of NbC,the AlCoCrFeNi_(2.1)-x NbC HEAs powders are significantly refined.And the degree of grain refinement gradually increases with the increase of NbC content.

关键词： utectic high entropy alloy Mechanical alloying alloying behavior grain size

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Phase Transformation in Al/Zn Multilayers during Mechanical alloying

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Acta Metallurgica Sinica(English Letters) 2023年第10期36卷 1709-1718页

作者： Chen Chen Junjie Yu Jingyu Lu Jian Zhang Xuan Su Chen-Hao Qian Yulin Chen Weixi Ji Manping Liu Department of mechanical Engineering Jiangnan UniversityWuxi214122China Jiangsu Key Laboratory of Advanced Food Manufacturing Equipment and Technology Jiangnan UniversityWuxi214122China School of Materials Science and Engineering Jiangsu UniversityZhenjiang212013China

In this work,Mechanical alloying of the alternating stacked pure Al and Zn thin foils was accomplished via high-pressure torsion(HPT).In the alloyed Al-Zn system,an exotic phase transformation from hexagonal close-packed(HCP)to face-centered cubic(FCC)was identified.The atomic-scale evolution process and underlying mechanism of phase transformation down to atomic scale are provided by molecular dynamics simulation and high-resolution transmission electron microscopy.The HCP→FCC phase transformation was attributed to the sliding of Shockley partial dislocations generated at the Al-Zn grain boundaries,which resulted in an[2110][011]and(0001)/(111)orientation relationship between the two phases.This work provides a new approach for the in-depth study of the solid phase transformation of Al-Zn alloys and also shed lights on understanding the mechanical properties of the HPT processed Al-Zn alloys.

关键词： High-pressure torsion Phase transformation Al/Zn multilayers Mechanical alloying

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Evaluation of the microstructure,thermal and mechanical properties of Cu/SiC nanocomposites fabricated by Mechanical alloying

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International Journal of Minerals,Metallurgy and Materials 2021年第3期28卷 475-486页

作者： Essam B.Moustafa Mohammed A.Taha mechanical Engineering Departments Faculty of EngineeringKing Abdulaziz UniversityJeddah 21589Saudi Arabia Solid State Physics Department National Research CentreEl Buhouth St.Dokki12622 GizaEgypt

Nano-sized silicon carbide(SiC:0wt%,1wt%,2wt%,4wt%,and 8wt%)reinforced copper(Cu)matrix nanocomposites were manufactured,pressed,and sintered at 775 and 875℃in an argon atmosphere.X-ray diffraction(XRD)and scanning electron microscopy were performed to characterize the microstructural evolution.The density,thermal expansion,mechanical,and electrical properties were studied.XRD analyses showed that with increasing SiC content,the microstrain and dislocation density increased,while the crystal size decreased.The coefficient of thermal expansion(CTE)of the nanocomposites was less than that of the Cu matrix.The improvement in the CTE with increasing sintering temperature may be because of densification of the microstructure.Moreover,the mechanical properties of these nanocomposites showed noticeable enhancements with the addition of SiC and sintering temperatures,where the microhardness and apparent strengthening efficiency of nanocomposites containing 8wt%SiC and sintered at 875℃were 958.7 MPa and 1.07 vol%^(−1),respectively.The electrical conductivity of the sample slightly decreased with additional SiC and increased with sintering temperature.The prepared Cu/SiC nanocomposites possessed good electrical conductivity,high thermal stability,and excellent mechanical properties.

关键词： copper matrix nanocomposites silicon carbide coefficient of thermal expansion elastic moduli electrical conductivity Mechanical alloying

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Effect of sintering temperature on phase evolution of Al86Ni6Y4.5Co2La1.5 bulk amorphous composites synthesized via Mechanical alloying and spark plasma sintering

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Progress in Natural Science:Materials International 2019年第1期29卷 32-40页

作者： Ashutosh Sahu Ram Sajeevan Maurya Tapas Laha Department of Metallurgical and Materials Engineering Indian Institute of Technology Department of Metallurgical and Materials Engineering National Institute of Technology

Al86Ni6Y4.5Co2La1.5amorphous powders were synthesized by Mechanical alloying for 200 h. Subsequent consolidation was performed via spark plasma sintering in the temperature range of 250 ℃ to 500 ℃ at the pressure of 500 MPa. The role of viscous flow on densification was investigated by studying the viscosity change of the amorphous phase at different consolidation temperatures. The decrease in viscosity at higher sintering temperatures resulted in better particle bonding and densification of consolidated samples. The formation of only FCC Al was observed in the consolidated samples at sintering temperatures ≤ 300 ℃ and the intermetallic phases formed at temperatures ≥ 400 ℃. The mechanical properties of the bulk samples were measured by Vickers microhardness and nanoindentation tests. The testing results showed that the average values of microhardness, nanohardness and elastic modulus of the sample consolidated at 500 ℃ were 3.06 ± 0.14 GPa,4.85 ± 1.14 GPa and 89.53 ± 9.25 GPa, respectively. The increase in hardness and elastic modulus of the higher temperature consolidated samples is attributed to the improvement in particle bonding, densification and distribution of various hard intermetallic phases in the amorphous matrix.

关键词： Al based glassy alloy Mechanical alloying Spark plasma sintering Intermetallic phase Viscosity

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Effect of Milling Tools on the Microstructure and Property of Cu-Based Composites Prepared by Mechanical alloying

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Acta Metallurgica Sinica(English Letters) 2017年第12期30卷 1155-1162页

作者： Ruo-Shan Lei Ming-Pu Wang College of Materials Science and Engineering China Jiliang University School of Materials Science and Engineering Central South University

Cu and Nb powders were used as starting materials to produce Cu-Nb and Cu-NbC-WC composites by Mechanical alloying. X-ray diffraction, scanning electron microscopy, transmission electron microscopy observations and microhardness measurements have been used to study the effects of milling tools on the phase, microstructure and property of the composites. The results revealed that a single-phase nanocrystalline solid solution was obtained using stainless steel vials and balls （Alloy 1）. Nevertheless, Cu-7 wt% Nb powders milled by tungsten carbon vials and balls exhibited an amorphous phase （Alloy 2）. The as-milled powders were then vacuum hot-pressing sintered. The microstructure of sintered Alloy 1 consisted of Nb nanoparticles and Cu nanograins. Instead, Alloy 2 showed a microstructure with NbC nanoparticles and WC submicron-sized particles dispersed throughout the Cu matrix. Furthermore, Alloy 2 （～ 322 HV） had a higher microhardness than Alloy 1 （～ 302 HV）.

关键词： Mechanical alloying Cu-based composite mechanical property Nanostructured materials

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Mechanical alloying behavior of Nb–Ti–Si-based alloy made from elemental powders by ball milling process

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Rare Metals 2017年第3期36卷 174-182页

作者： Li-Jing Zhang Xi-Ping Guo State Key Laboratory of Solidification Processing Northwestern Polytechnical UniversityXi'an 710072China

Nb-Ti-Si-based alloy powders were prepared by Mechanical alloying （MA） of elemental particles.The evolutions of morphology,size,phase constituents,crystallite size,lattice strain,composition and internal microstructure,etc.,of the alloy powders were analyzed by X-ray diffraction （XRD）,scanning electron microscopy （SEM）,energy-dispersive spectroscopy （EDS）,laser particle size analyzer and transmission electron microscope （TEM） analyses.The alloy particles are gradually refined and their shapes become globular with the increase in milling time.The diffraction peaks of Nb solid solution （Nbss） phase shift toward lower 2θ angles during ball milling from 2 to 5 h,and after that Nbss diffraction peaks shift toward higher 2θ angles with the increase in milling time from 5 to 70 h,which is mainly attributed to the alteration of the lattice parameter of Nbss powders due to the solution of the alloying element atoms into Nb lattice to form Nbss.During ball milling process,the decrease in crystallite size and increase in lattice strain of Nbss powders lead to continuous broadening of their diffraction peaks.A typical lamellar microstructure is formed inside the powder particles after ball milling for 5 h and becomes more refined and homogenized with the increase in milling time.After 40-h-ball milling,the typical lamellar microstructure disappears and a very homogeneous microstructure is formed instead.This homogeneous microstmcture is proved to be composed of only supersaturated Nbss phase.

关键词： Mechanical alloying Nb-Ti-Si-based alloy Powder morphology Phase constituents MicrostructureSupersaturated Nb solid solution

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Preparation and hydrogen storage properties of nanocrystalline TiFe synthesized by Mechanical alloying

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Progress in Natural Science:Materials International 2017年第1期27卷 149-155页

作者： V.Yu.Zadorozhnyy G.S.Milovzorov S.N.Klyamkin M.Yu.Zadorozhnyy D.V.Strugova M.V.Gorshenkov S.D.Kaloshkin National University of Science and Technology “MISIS” Department of Chemistry M.V. Lomonosov Moscow State University

In this research, the mechanism of Mechanical alloying（MA） synthesis of TiFe intermetallic compound（IMC）from individual components Ti and Fe has been studied. The partition coefficient of the apparent diffusion and the reaction rate constant during MA solid-state synthesis of the TiFe intermetallic compound in a planetary ball mill have been estimated. The results indicate that the apparent diffusion coefficient is close to 10;cm;/s that is approximately one order higher than the conventional high temperature diffusion coefficient. The reaction rate constant is close to 1.75·10;. The relation between the structure and the hydrogen storage properties of MA synthesized IMC TiFe have been briefly discussed.

关键词： Mechanical alloying Intermetallic compound TiFe Hydrogen storage Apparent diffusion coefficient Reaction rate constant

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Fabrication of Bulk (Fe,Cr)_3Al/Al_2O_3 Intermetallic Matrix Nanocomposite Through Mechanical alloying and Sintering

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Acta Metallurgica Sinica(English Letters) 2016年第10期29卷 911-919页

作者： Sayyed Erfan Aghili Mohammad Hossein Enayati Fathallah Karimzadeh Department of Materials Engineering Isfahan University of Technology

In the present study, （Fe,Cr）3Al/20 vol% A1203 nanocomposite was prepared through mechanochemical reactions during ball milling and successfully bulked using a combination of cold isostatic press and sintering at 1400℃ for 1 h. Two processing approaches were utilized to produce （Fe,Cr）3A1/A1203 nanocomposite： The first was milling of Fe, Cr, AI and Fe203, while the second one was milling of Fe, Cr, Al and Cr203, both in stoichiometric condition, to synthesize （Fe,Cr）3Al/20 vol% Al2O3. Structural changes of powder particles during Mechanical alloying were studied by X-ray diffraction. The microstructure and the morphology of powder particles and bulk samples were also studied by scanning electron microscopy and transmission electron microscopy. Microstructural analysis showed that mechanochemical reactions took place during milling, and nanometric Al2O3 was uniformly distributed in the matrix. The results also showed that the second approach required a considerably higher milling time to produce （Fe,Cr）3Al/Al2O3 nanocomposite, as compared to the first one. For this reason, bulk samples were produced from the synthesized nanocomposite in the first approach. The microstructure of the sintered samples consisted of a network structure of （Fe,Cr）3Al and Al2O3 phases with superior mechanical properties.

关键词： Iron aluminide Mechanical alloying Nanocomposite Mechanochemical treatment

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Wear and mechanical characterization of Mg-Gr self-lubricating composite fabricated by Mechanical alloying

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Journal of Magnesium and Alloys 2019年第2期7卷 283-290页

作者： Azzat Esam Abdulqader Al-maamari AKMAsif Iqbal Dewan Muhammad Nuruzzaman Faculty of mechanical and Manufacturing Engineering University Malaysia Pahang26600PekanPahangMalaysia

In this research,the wear and mechanical responses of pure magnesium-graphite(Mg-Gr)composite have been investigated aiming to get the optimum composition of reinforcement.The composite materials were fabricated by Mechanical alloying.The percentage of graphite reinforcement was chosen as 3,5,7 and 10 wt.%to identify its potential for self-lubricating property under dry sliding conditions.The mechanical properties including hardness,tensile strength and flexural strength of the composites and the base material were tested.The wear tests were conducted by using a pin-on-disc tribometer.The results show that the mechanical properties decrease with increasing graphite content as compared to that of the base material.The wear rate and average coefficient of friction decrease with the addition of graphite and was found to be minimum at 5 wt.%graphite reinforcement.The addition of 5 wt.%graphite in the composite exhibits superior wear properties as compared to that of the matrix material and other compositions of the Mg-Gr composites.

关键词： Metal-matrix composites(MMCs) Characterization mechanical properties Wear Mechanical alloying

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