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Manufacture and Cytotoxicity of a lead-free piezoelectric ceramic as a Bone Substitute—Consolidation of Porous Lithium Sodium Potassium Niobate by Cold Isostatic Pressing

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International Journal of Oral Science 2009年第2期1卷 99-104页

作者： Qi Wang Jun Yang Wu Zhang Roxanne Khoie Yi-ming Li Jian-guo Zhu Zhi-qing Chen State Key Laboratory of Oral Diseases West China College of Stomatology Sichuan University Chengdu China College of Materials Science and Engineering Sichuan University Chengdu China Center for Dental Research School of Dentistry Loma Linda University Loma Linda USA

Aim The piezoelectric properties and cytotoxicity of a porous lead-free piezoelectric ceramic for use as a direct bone substitute were investigated. Methodology Cold isostatic pressing （CIP） was applied to fabricate porous lithium sodium potassium niobate （Li0.06Na0.5K0.44） NbO3 specimens using a pore-forming method. The morphologies of the CIP-processed specimens were characterized and compared to those of specimens made by from conventional pressing procedures. The effects of the ceramic on the attachment and proliferation of osteoblasts isolated from the cranium of 1-day-old Sprague- Dawley rats were examined by a scanning electron microscopy （SEM） and metbylthiazol tetrazolium （MTT） assay. Results The results showed that CIP enhanced piezoelectricity and biological performance of the niobate specimen, and also promoted an extracellular matrix-like topography of it. In vitro studies showed that the CIP-enhanced material had positive effects on the attachment and proliferation of osteoblasts. Conclusion Niobate ceramic generated by CIP shows a promise for being a piezoelectric composite bone substitute.

关键词： lead-free piezoelectric ceramic cold isostatic pressing (CIP) cytocompatibility osteoblast

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Synthesis and Electrical Properties of Li-modified Bi_(0.5)Na_(0.5)TiO_3-BaTiO_3 lead-free piezoelectric ceramics

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Journal of Materials Science & Technology 2009年第6期25卷 777-780页

作者： Yunweu Liao Dingquan Xiao Institute of Applied Chemistry China West Normal University Nanchong 637002 China Department of Materials Science Sichuan University Chengdu 610064 China

lead-free piezoelectric ceramics （1-y）Bi0.5（Na1-xLix）0.5TiO3-yBaTiO3 with x=0-0.125 and y=0.02-0.12 were fabricated by a solid-state reaction process, and their dielectric, piezoelectric and ferroelectric properties were investigated. The results show that the addition of Li^＋ significantly improves the sintering performance and piezoelectric properties of the ceramics. X-ray diffraction （XRD） patterns indicate that the ceramics possess pure perovskite structure. At room temperature, the ceramics provide high piezoelectric charge constant d33 （up to 210 pC/N）, high planar electromechanical coupling factor kp （34.5%）, large remanent polarization Pr （up to 40 μC/cm^2）, and low coercive field Ec （3.0 kV/mm）, which indicates that （1-y）Bi0.5（Na1-xLix）0.5TiO3-yBaTi03 is a good lead-free piezoelectric ceramic.

关键词： lead-free piezoelectric ceramic Bi0.5Na0.5TiO3 Microstructure piezoelectricity

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Origin of high mechanical quality factor in CuO-doped （K, Na）NbO3-based ceramics

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Frontiers of Materials Science 2014年第2期8卷 165-175页

作者： Wen-Feng LIANG Ding-Quan XIAO Jia-Gang WU Wen-Juan WU Jian-Guo ZHU Department of Materials Science Sichuan University Chengdu 610064 China CAEP Key Laboratory of Neutron Physics Mianyang 621900 China Institute of Nuclear Physics and Chemistry China Academy of Engineering Physics Mianyang 621900 China

The origin of a high mechanical quality in CuO-doped （K, Na）NbO3-based ceramics is addressed by considering the correlations between the lattice positions of Cu ions and the hardening effect in K0.48Na0.52＋xNbO3-0.01CuO ceramics. The Cu ions simultaneously occupy K/Na and Nb sites of these ceramics with x = 0 and 0.02, only occupy the K/Na site of the ceramics with x= -0.02, and mostly form a secondary phase of the ceramics with x = -0.05. The Cu ions lead to the hardening of ceramics with an increase of Ec and Qm by only occupying the K/Na site, together with the formation of double hysteresis loops in un-poled compositions. A defect model is proposed to illuminate the origin of a high Qm value, that is, the domain stabilization is dominated by the content of relatively mobile O2- ions in the ceramics, which has a weak bonding with CUK/Na defects.

关键词： lead-free piezoelectric ceramic (K, Na)NbO3 (KNN) mechanism of hard-ening effect mechanical quality factor Qm domain stabilization

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