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Enhanced helium ion irradiation tolerance in a Fe-Co-Ni-Cr-Al-Ti high-entropy alloy with l12 nanoparticles

Journal of Materials Science & Technology 2023年第12期143卷 169-177页

作者： Y.l.Zhao F.l.Meng T.Yang J.H.luan S.F.liu G.M.Yeli W.T.lin W.H.liu X.J.liu C.T.liu J.J.Kai School of Materials Science and Engineering Harbin Institute of Technology(Shenzhen)Shenzhen 518055China School of Materials Science and Engineering Southern University of Science and TechnologyShenzhen 518055China Department of Materials Science and Engineering Mechanical Behavior Division of Shenyang National Laboratory for Materials ScienceCity University of Hong KongHong KongChina Department of Mechanical Engineering City University of Hong KongHong KongChina Institute of Nuclear&New Energy Technology Tsinghua UniversityBeijing 100084China

l12-strengthened high entropy alloys(HEAs)with excellent room and high-temperature mechanical prop-erties have been proposed as promising candidates as structural materials for advanced nuclear systems.However,knowledge about their radiation response is fairly limited.In the present work,a novel HEA with a high density of l12 nanoparticles was irradiated with He ion at 500°C.Transmission electron microscope(TEM)and atom probe tomography(APT)were employed to study the evolution of mi-crostructural stability and radiation-induced segregation.Similar to the single-phase FeCoNiCr HEA,the main microstructural features were numerous large faulted dislocation loops and helium bubbles.While the irradiation resistance of the present l12-strengthened HEA is much improved in terms of reduced bubble size,which could be attributed to the considerable He trapping efficiency of the coherent pre-cipitate/matrix interface and the enhanced capability of the interface for damage elimination when the matrix channel width is narrow.APT analysis revealed that an inverse-Kirkendall-mechanism-dominated radiation-induced segregation(RIS)occurs around bubbles,where a significant Co enrichment and Ni de-pletion can be clearly observed.In addition,the competing dynamics of ballistic mixing and elemental clustering that raised from the irradiation-enhanced diffusion in a highly supersaturated matrix,along with the low precipitation nucleation barrier due to the small lattice misfit,lead to a dynamical pre-cipitation dissolution and re-precipitation appears under irradiation.Such a promising phenomenon is expected to promote a potential self-healing effect and could in turn provide a sustainable irradiation tolerance over the operational lifetime of a reactor.

关键词： l12 nanoparticles High-entropy alloy Helium bubble Phase stability Radiation-induced segregation

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