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Highly oriented MXene/polyvinyl alcohol films prepared by scalable layer-by-layer blade coating for efficient electromagnetic interference shielding and infrared stealth

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Nano Research 2024年第6期17卷 5651-5660页

作者： Jingyu Dong Zhaoyang Li Congqi Liu Bing Zhou Chuntai Liu uezhan Feng State Key Laboratory of Structural Analysis Optimization and CAE Software for Industrial EquipmentNational Engineering Research Center for Advanced Polymer Processing TechnologyZhengzhou UniversityZhengzhou 450002China Shangqiu Normal University Shangqiu 476000China

Controlling the orientation of two-dimensional MXene within layered films is essential to optimize or tune their mechanical properties and electromagnetic interference shielding(EMI)performance,but achieving the high orientation MXene layers on an industrial scale remains a challenging goal.In this paper,a scalable layer-by-layer blade coating(LbLBC)method was employed to fabricate highly oriented MXene/polyvinyl alcohol(PVA)films.During the LbLBC process,MXene/PVA colloid suffered a strong shearing effect,which induced the ordered alignment of MXene nanosheets along the direction of the blade movement.The orientation of MXene can be effectively adjusted by changing the scraping gap of LbLBC,achieving a maximum Herman orientation factor f of 0.81.As a result,the mechanical properties and EMI performance of the as-prepared MXene/PVA films are in direct proportion to their orientation,with the optimal values of tensile strength of 145.5 MPa,fracture strain of 19.6%,toughness of 17.7 MJ·m^(−3),and EMI shielding effectiveness of 36.7 dB.Furthermore,the inherently low mid-infrared(mid-IR)emissivity of MXene,combined with the densely oriented structure affords the composite films with IR stealth,resulting in a substantial decrease from 150 to 66.1℃in the radiative temperature of a surface.Conclusively,these scalable MXene/PVA films exhibit remarkable potential for integration into the next generation of multifunctional protective camouflage materials.

关键词： MXene nanosheets densely oriented structure layer-by-layer blade coating electromagnetic interference shielding infrared stealth

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Performance of the Multilayer Film for infrared stealth based on VO2 Thermochromism

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Journal of Thermal Science 2024年第4期33卷 1312-1324页

作者： LI Yaru WANG Fuqiang ZHANG Aoyu FU Zhichang SU Ronghua GAO Tengfei WANG Zhen GUO Jicheng ORDOS Institute of Technology School of New Energy Harbin Institute of Technology at Weihai School of Energy Science and Engineering Harbin Institute of Technology Defense Engineering Institute AMSPLA

With the development of detection and identification technology,infrared stealth is of great value to realize anti-reconnaissance detection of military targets.At present,infrared stealth materials generally have deficiency,such as complex structure,inconvenient radiation regulation and cumbersome preparation steps,which greatly limit the practical application of infrared stealth materials.In view of the above deficiency of infrared stealth materials,we proposed a kind of multilayer film for infrared stealth using VO2thermochromism based on the temperature response mechanism of tuna to adjust its color,and through the intelligent reversible radiation regulation mechanism to meet the infrared stealth requirements of tanks in different actual scenes.The results show that when the temperature increases from 300 K to 373 K,the peak emissivity of the film decreases from 94% to 20% in the 8-14 μm band after structural optimization,which can realize the infrared stealth of the high temperature target in the 8-14 μm band.The average emissivity of the multilayer film for infrared stealth at3-5μm and 8-14μm band can be reduced to 34% and 27% at 373 K,and the peak emissivity at 5-8 μm band can reach 65%,realizing dual-band infrared stealth in the 3-5 μm and 8-14 μm bands and heat dissipation in the 5-8μm band.The multilayer film for infrared stealth based on VO2thermochromism designed by the authors can meet the characteristics of simple film structure,convenient radiation regulation and simple preparation.

关键词： vanadium dioxide multilayer film infrared stealth thermal management

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Ni Flower/MXene-Melamine Foam Derived 3D Magnetic/Conductive Networks for Ultra-Efficient Microwave Absorption and infrared stealth

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Nano-Micro Letters 2022年第4期14卷 142-157页

作者： Haoran Cheng Yamin Pan Xin Wang Chuntai Liu Changyu Shen Dirk W.Schubert Zhanhu Guo Xianhu Liu Key Laboratory of Advanced Material Processing&Mold(Ministry of Education) National Engineering Research Center for Advanced Polymer Processing TechnologyCollege of Materials Science and EngineeringZhengzhou UniversityZhengzhou 450002People’s Republic of China Institute of Polymer Materials Friedrich-Alexander-University Erlangen-NurembergMartensstr.791058 ErlangenGermany Integrated Composites Laboratory(ICL) Department of Chemical&Biomolecular EngineeringUniversity of TennesseeKnoxvilleTN 37996USA

The development of multifunctional and efficient electromagnetic wave absorbing materials is a challenging research hotspot.Here,the magnetized Ni flower/MXene hybrids are successfully assembled on the surface of melamine foam(MF)through electrostatic self-assembly and dip-coating adsorption process,realizing the integration of microwave absorption,infrared stealth,and flame retardant.Remarkably,the Ni/MXene-MF achieves a minimum reflection loss(RLmin)of−62.7 dB with a corresponding effective absorption bandwidth(EAB)of 6.24 GHz at 2 mm and an EAB of 6.88 GHz at 1.8 mm.Strong electromagnetic wave absorption is attributed to the three-dimensional magnetic/conductive networks,which provided excellent impedance matching,dielectric loss,magnetic loss,interface polarization,and multiple attenuations.In addition,the Ni/MXene-MF endows low density,excellent heat insulation,infrared stealth,and flame-retardant functions.This work provided a new development strategy for the design of multifunctional and efficient electromagnetic wave absorbing materials.

关键词： Ni-MXene/Melamine foam Microwave absorption Heat insulation infrared stealth Flame-retardant

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Multifunctional protective aerogel with superelasticity over−196 to 500℃

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Nano Research 2022年第9期15卷 7797-7805页

作者： Bo-Wen Liu Min Cao Yi-Ying Zhang Yu-Zhong Wang Hai-Bo Zhao The Collaborative Innovation Center for Eco-Friendly and Fire-Safety Polymeric Materials(MoE) National Engineering Laboratory of Eco-Friendly Polymeric Materials(Sichuan)State Key Laboratory of Polymer Materials EngineeringCollege of ChemistrySichuan UniversityChengdu 610064China

Protective materials that possess superelasticity and multifunctionality over a broad temperature range are urgently needed in various advanced applications.However,under harsh work conditions,the performance of current materials may largely deteriorate to lose protective functionality.Herein,we report a bidirectionally oriented multi-walled carbon nanotubes(MWCNTs)-reinforced chitosan carbon aerogel(CS-MWCNT)that possesses superelasticity,high electromagnetic interference shielding,thermal insulation,and infrared stealth at both low temperatures(such as liquid nitrogen)and high temperatures(such as alcohol flames).Highly oriented lamellar arch structures combined with an MWCNTs-reinforced carbon skeleton act as elastic segments to disperse the stress during compression and endow CS-MWCNT with the ability to recover to almost the original size after being compressed at−196-500℃.The lamellar structures make CS-MWCNT thermally insulating and infrared stealth with a low thermal conductivity of~0.03 W/(m·K).Furthermore,a high electromagnetic interference(EMI)shielding effect of 64 dB is realized via an absorption-dominant EMI shielding mechanism derived from the successive inherently conductive carbon lamella,and the EMI shielding performance is largely maintained after treatment under extreme conditions like low temperature,high temperature,as well as cyclic compression.This work provides a new strategy for the development of temperature-invariant multifunctional aerogels for harsh environment applications.

关键词： superelasticity electromagnetic interference shielding heat insulation infrared stealth extreme environment

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Coupling of Epsilon-Near-Zero Mode to Mushroom-Type Metamaterial for Optimizing infrared Suppression and Radiative Cooling

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Photonic Sensors 2023年第2期13卷 76-88页

作者： Jiacheng LI Shuang LIU Shenglan WU Yong LIU Zhiyong ZHONG State Key Laboratory of Electronic Thin Films and Integrated Devices School of Optoelectronic Science and EngineeringUniversity of Electronic Science and Technology of ChinaChengdu 611731China School of Electronic Science and Engineering University of Electronic Science and Technology of ChinaChengdu 611731China

We report a complementary metal oxide semiconductor(CMOS)compatible metamaterial-based spectrally selective absorber/emitter(MBSSAE)for infrared(IR)stealth,which has the low absorption/emissivity in the IR atmospheric transmission window(3μm-5μm,8μm-14μm)and ultra-high and broadband absorption/emissivity in the IR non-atmospheric window(5μm-8μm).We propose a novel method for the broadband absorption/emissivity in 5μm-8μm with incorporation of an epsilon-near-zero(ENZ)material between the top patterned aluminum(Al)disks layer and the silicon oxide(SiO_(2))spacer layer.With an appropriate design,the peaks in the IR atmospheric transmission window can be suppressed while the peak intensity in the non-atmospheric window remains high.The optimized MBSSAE has an average absorption/emissivity less than 10%in 8μm-14μm and less than 6%in 3μm-5μm.And the average absorption/emissivity in 5μm-8μm is approximately over 64%.This proposed scheme may introduce the opportunities for the large-area and low-cost infrared stealth coating,as well as for the radiative cooling,spectral selective thermal detector,optical sensor,and thermophotovoltaic applications.

关键词： Metamaterials infrared stealth ENZ mode Rabi splitting broadband thermal emitter

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Preparation of ZAO powder and investigation on its infrared emissivity

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Journal of Harbin Institute of Technology(New Series) 2010年第4期17卷 588-592页

作者：武晓威冯玉杰刘延坤 School of Municipal and Environmental Engineering Harbin Institute of Technology College of Geographical Sciences Harbin Normal University

According to the basic infrared stealth mechanism of low infrared emissivity powders,the ZAO powder materials were prepared by liquid coprecipitation method,and the starting materials were Zn( NO3) 6H2O and Al( NO3) 39H2O. The process parameters were obtained,and the relationship between technology parameters and infrared emissivity was investigated. The temperature of thermal treatment,crystal structure and surface micrograph of ZAO powder was analyzed by the help of TG-DTA,XRD and SEM. The infrared stealth performance of ZAO powder was studied by IR-2 emissivity spectroscopy. Results showed that the infrared emissivity was the lowest when pH was 8. 0,calcination temperature was 1100 ℃,calcination time was 2 h,and the Al2O3doping content was 3% ( mass percentage) . The crystal structure of doped ZAO powder was lead-zinc, and there exists distortion of crystal lattice in nanocrystalline ZnO. The average particle size was 10 μm. The lowest infrared emissivity reached to 0. 61 at between 8 μm and 14 μm. It means that the ZAO powders will be excellent infrared stealthy materials.

关键词： ZAO infrared stealth semiconductor material emissivity

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