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A general synthesis of inorganic nanotubes as high-rate anode materials of sodium ion batteries

Journal of Energy Chemistry 2023年第2期77卷 369-375,I0010页

作者： Chunting Wang Ningyan Cheng Zhongchao Bai Qinfen Gu Feier Niu Xun Xu Jialin Zhang Nana Wang Binghui Ge Jian Yang Yitai Qian Shixue Dou Key Laboratory of Colloid and Interface Chemistry Ministry of EducationSchool of Chemistry and Chemical EngineeringShandong UniversityJinan 250100ShandongChina Key Laboratory of Structure and Functional Regulation of Hybrid Materials of Ministry of Education Institutes of Physical Science and Information TechnologyAnhui UniversityHefei 230601AnhuiChina College of Mechanical and Electronic Engineering Shandong University of Science and TechnologyQingdao 266590ShandongChina Australian Synchrotron 800 Blackburn RoadClaytonVIC 3168Australia College of Chemistry and Materials Engineering Anhui Science and Technology UniversityBengbu 233000AnhuiChina Institute for Superconducting and Electronic Materials University of Wollongong Innovation Campus Innovation Campus Squires WayWollongongNew South Wales 2500Australia Institute of Energy Materials Science(IEMS) University of Shanghai for Science and TechnologyShanghai 200093China

Ino rganic tubular materials have an exceptionally wide range of applications,yet developing a simple and universal method to controllably synthesize them remains *** this work,we report a vaporphase-etching hard-template method that can directly fabricate tubes on various thermally stable oxide and sulfide *** synthesis method features the introduction of a vapor-phase-etching process to greatly simplify the steps involved in preparing tubular materials and avoids complicated postprocessing ***,the in-situ heating transmission electron microscopy(tem)technique is used to observe the dynamic formation process of TiO_(2-x) tubes,indicating that the removal process of the Sb2S3 templates first experienced the Rayleigh instability,then vapor-phase-etching *** used as an anode for sodium ion batteries,the TiO_(2-x) tube exhibits excellent rate performance of134.6 mA h g^(-1) at the high current density of 10 A g^(-1) and long-term cycling over 7000 ***,the full cell demonstrates excellent cycling performance with capacity retention of 98%after 1000 cycles,indicating that it is a promising anode material for *** method can be expanded to the design and synthesis of other thermally-stable tubular materials such as ZnS,MoS_(2),and SiO_(2).

关键词： Tubular materials in-situ heating tem Sodium ion batteries TiO_(2) Hard template methods

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