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Two-step hydrothermal conversion of biomass waste to humic acid using hydrochar as intermediate

Frontiers of Environmental Science & Engineering 2023年第10期17卷 17-26页

作者： Yuchao Shao Jun Zhao Yuyang Long Wenjing Lu School of Environment Tsinghua UniversityBeijing 100084China Department of Biology Institute of Bioresource and AgricultureHong Kong Baptist UniversityHong Kong 999077China Zhejiang Provincial Key Laboratory of Solid Waste Treatment and Recycling Instrumental Analysis CenterSchool of Environmental Science and EngineeringZhejiang Gongshang UniversityHangzhou 310012China

Converting biomass materials to humic acid is a sustainable method for humic acid production and achieve biomass valorization. A two-step hydrothermal treatment method was adopted in this study to produce humic acid from corn stalks. In the first step of the process, hydrochar was prepared at different hydrothermal temperatures and pH values. Their chemical properties were then analyzed, and the hydrochar-derived humic acids were produced under alkaline hydrothermal conditions (denoted as HHAalk). The hydrochar, prepared under high temperature (200 °C) and strong acidic (pH 0) conditions, achieved high HHAalk yields (i.e., 67.9 wt% and 68.8 wt% calculated based on weight of hydrochar). The sources of HHAalk formation were as follows: 1) production in the hydrochar preparation stage, and 2) increment under the alkaline hydrothermal treatment of hydrochar. The degree of hydrochar unsaturation was suggested as an indicator for evaluating the hydrochar humification potential under alkaline hydrothermal conditions. This study provides an important reference for the preparation of suitable hydrochar with high hydrothermal humification potential.

关键词： Biowaste Hydrochar Humic acid hydrothermal parameter Unsaturation

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