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Development in oxide metallurgy for improving the weldability of high -strength low-alloy steel-Combined deoxidizers and microalloying elements

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International Journal of Minerals,Metallurgy and Materials 2024年第6期31卷 1263-1284页

作者： Tingting Li Jian Yang State Key Laboratory of Advanced Special steel School of Materials Science and EngineeringShanghai UniversityShanghai 200444China

The mechanisms of oxide metallurgy include inducing the formation of intragranular acicular ferrite(IAF)using micron-sized inclusions and restricting the growth of prior austenite grains(PAGs)by nanosized particles during welding.The chaotically oriented IAF and refined PAGs inhibit crack initiation and propagation in the steel,resulting in high impact toughness.This work summarizes the com-bined effect of deoxidizers and alloying elements,with the aim to provide a new perspective for the research and practice related to im-proving the impact toughness of the heat affected zone(HAZ)during the high heat input welding.Ti complex deoxidation with other strong deoxidants,such as Mg,Ca,Zr,and rare earth metals(REMs),can improve the toughness of the heat-affected zone(HAZ)by re-fining PAGs or increasing IAF contents.However,it is difficult to identify the specific phase responsible for IAF nucleation because ef-fective inclusions formed by complex deoxidation are usually multiphase.Increasing alloying elements,such as C,Si,Al,Nb,or Cr,con-tents can impair HAZ toughness.A high C content typically increases the number of coarse carbides and decreases the potency of IAF formation.Si,Cr,or Al addition leads to the formation of undesirable microstructures.Nb reduces the high-temperature stability of the precipitates.Mo,V,and B can enhance HAZ toughness.Mo-containing precipitates present good thermal stability.VN or V(C,N)is ef-fective in promoting IAF nucleation due to its good coherent crystallographic relationship with ferrite.The formation of the B-depleted zone around the inclusion promotes IAF formation.The interactions between alloying elements are complex,and the effect of adding dif-ferent alloying elements remains to be evaluated.In the future,the interactions between various alloying elements and their effects on ox-ide metallurgy,as well as the calculation of the nucleation effects of effective inclusions using first principles calculations will become the focus of oxide metallurgy.

关键词： oxide metallurgy technology heat affected zone high-strength low-alloy steel intragranular acicular ferrite microalloying element

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Multi-performance evaluation of high-throughput accelerated corrosion test for high-strength low-alloy 921A steel

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Journal of Iron and steel Research(International) 2024年第5期31卷 1260-1278页

作者： Cong-cong Du Ming-hua Qin Zhan-fang Wu Dong-ling Li Lei Zhao Xiang-yang Li Hai-zhou Wang Beijing Advanced Innovation Center for Materials Genome Engineering National Center for Materials Service SafetyUniversity of Science and Technology BeijingBeijing100083China China Iron and steel Research Institute Group Co. Ltd.Beijing100081China Beijing Advanced Innovation Center for Materials Genome Engineering Central Iron and Steel Research InstituteBeijing100081China

The corrosion behavior of high-strength low-alloy 921A steel in a simulated marine atmospheric environment was studied using a high-throughput experimental method.The corrosion behavior,corrosion morphology,and corrosion products of 921A steels were analyzed using various techniques,including corrosion mass loss method,polarization curve,white-light interferometry,scanning electron microscopy,energy-dispersive spectrometry,microbeam X-ray fluorescence spectrometry,X-ray diffraction technique,and X-ray photoelectron spectroscopy.The test results indicated that 921A steel exhibits better corrosion resistance than Q450NQR1 steel in simulated harsh atmospheric environments,as evidenced by a lower corrosion mass loss rate throughout the corrosion tests.The corrosion products of both steels consisted ofα-FeOOH,Fe_(3)O_(4),andγ-FeOOH,withα-FeOOH being more prevalent in the rust layer of 921A steel than in Q450NQR1 steel.The inner rust layer of 921A steel also exhibited an appositional enrichment region of Cr,Ni,Mo,and V,leading to its superior corrosion resistance compared to that of Q450NQR1 steel.The efficacy of high-throughput accelerated corrosion experimental methods was highlighted for evaluating the corrosion resistance of steel materials in harsh environmental conditions.The findings suggest that 921A steel exhibits better corrosion resistance compared to Q450NQR1 steel and has the potential to be more suitable in harsh marine atmospheric environments.The characterization of the rust layer structures and composition reveals the parallel enrichment of certain elements in the inner rust layer of 921A steel,which enhances its corrosion resistance.

关键词： Atmospheric corrosion high-throughput experimental method high-strength low-alloy steel Corrosion characteristics Rust layer Element enrichment

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Effect of oxide inclusions on MnS precipitates and tensile mechanical property of high-strength low-alloy steel

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Journal of Iron and steel Research(International) 2024年第5期31卷 1210-1220页

作者： Xiao-yong Gao Hong Wei Li-feng Zhang School of Mechanical Engineering Yanshan UniversityQinhuangdao066004HebeiChina School of Materials Science and Engineering Yanshan UniversityQinhuangdao066004HebeiChina School of Mechanical and Materials Engineering North China University of TechnologyBeijing100144China

The key role of oxide inclusions on the microstructure and mechanical property of a high-strength low-alloy steel was investigated.The field emission scanning electron microscope equipped with energy-dispersive spectrometry was used to characterize MnS precipitates.Oxide inclusions play an important role in the shape control of MnS precipitates.More oxides fovored to decrease the size and the aspect ratio of MnS precipitates.With less oxide inclusions in the steel,approximately over 16.7%MnS precipitates were with aspect ratio a>5 and pure MnS precipitates accounted for 75.9%in number.However,with more oxide inclusions in the steel,only 7.4%MnS precipitates were with a>5 and pure MnS precipitates accounted for 60.1%in number.Refinement of MnS by oxide inclusions improved the strength and inhibited the anisotropy.More oxide inclusions in the steel increased the yield strength and tensile strength of the steel in both longitudinal and transverse directions,and lowered the anisotropy of the mechanical property.

关键词： high-strength low-alloy steel MnS Oxide inclusion Mechanical property Anisotropy

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Effect of trace boron on corrosion resistance of rust layer of high-strength low-alloy steel in 3.5 wt.% NaCl solution

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Journal of Iron and steel Research(International) 2023年第10期30卷 2080-2090页

作者： Yan-hui Hou Ze-kun Xu Guang-qiang Li The State Key Laboratory of Refractories and Metallurgy Wuhan University of Science and TechnologyWuhan 430081HubeiChina Key Laboratory for Ferrous Metallurgy and Resources Utilization of Ministry of Education Wuhan University of Science and TechnologyWuhan 430081HubeiChina

The influence mechanism of trace boron on the corrosion resistance of high-strength low-alloy(HSLA)steel in a simulated marine environment was studied by combining first-principles calculation with experiment.The effect of boron on the corrosion properties and corrosion morphology of the rust layer formed on the surface of HSLA steel was studied by means of corrosion weightlessness method,polarization curve,scanning electron microscopy(SEM)and X-ray diffraction(XRD)technique.The mass loss measurements and polarization curves revealed that the corrosion resistance of HSLA steel is improved by adding trace boron.XRD and SEM results show that the rust layer is produced byα-FeOOH(the main protective phase),Fe_(3)O_(4) andγ-FeOOH,and boron contributes to stability ofα-FeOOH.Based on the first-principles calculation,the solid solution of B atom in the corrosion product is beneficial to the fixation of Cl atom and to the reduction of the corrosion of Cl atom to the steel matrix.

关键词： Boron high-strength low-alloy steel Corrosion resistance NaCl solution Rust layer First-principles calculation

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Effects of final rolling temperature and coiling temperature on precipitates and microstructure of high-strength low-alloy pipeline steel

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Journal of Iron and steel Research(International) 2022年第8期29卷 1236-1244页

作者： Ya-dong Wang Zheng-hua Tang Su-fen Xiao Charles WSiyasiya Tao Wei Department of Materials Science and Engineering Sichuan UniversityChengdu 610065SichuanChina Department of Materials Science and Metallurgical Engineering University of PretoriaPretoria 0028South Africa

The strength-to-weight ratio is an important property of high-strength low-alloy(HSLA)steel in pipeline,whose precipitation strengthening can be improved.The final rolling temperature(FRT)and coiling temperature(CT)are the key process parameters in the control of precipitates and microstructure.Continuous cooling rate was fixed at 10℃/s,and the effects of deformation and coiling temperatures on precipitates and microstructure of Ti-Nb microalloyed HSLA steel were investigated through thermo-mechanical controlled processing on Gleeble 3500.The microstructure is mainly acicular ferrite with high density dislocation and several microns scale.The size and volume fraction of the precipitates were studied under transmission electron microscopy.The results showed that the diameter of the precipitates was in the range between 4 and 240 nm.The optimized combination of parameters is FRT of 820℃and CT of 550℃,and the volume fraction of precipitates obtained under this process is 0.59%.

关键词： Precipitate Thermo-mechanical controlled processing Final rolling temperature Coiling temperature high-strength low-alloy steel (Ti,Nb)C

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Determining role of heterogeneous microstructure in lowering yield ratio and enhancing impact toughness in high-strength low-alloy steel

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International Journal of Minerals,Metallurgy and Materials 2021年第5期28卷 816-825页

作者： Yi-shuang Yu Bin Hu Min-liang Gao Zhen-jia Xie Xue-quan Rong Gang Han Hui Guo Cheng-jia Shang Collaborative Innovation Center of steel Technology University of Science and Technology BeijingBeijing 100083China Institute of Advanced Materials and Technology University of Science and Technology BeijingBeijing 100083China State Key Laboratory of Metal Material for Marine Equipment and Application Anshan 114021China

Here we present a novel approach of intercritical heat treatment for microstructure tailoring,in which intercritical annealing is introduced between conventional quenching and tempering.This induced a heterogeneous microstructure consisting of soft intercritical ferrite and hard tempered martensite,resulting in a low yield ratio(YR)and high impact toughness in a high-strength low-alloy steel.The initial yielding and subsequent work hardening behavior of the steel during tensile deformation were modified by the presence of soft intercritical ferrite after intercritical annealing,in comparison to the steel with full martensitic microstructure.The increase in YR was related to the reduction in hardness difference between the soft and hard phases due to the precipitation of nano-carbides and the recovery of dislocations during tempering.The excellent low-temperature toughness was ascribed not only to the decrease in probability of microcrack initiation for the reduction of hardness difference between two phases,but also to the increase in resistance of microcrack propagation caused by the high density of high angle grain boundaries.

关键词： heterogeneous microstructure yield ratio impact toughness intercritical heat treatment high-strength low-alloy steel

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Interface reaction of high-strength low-alloy steel with Al-43.4Zn-1.6Si(wt.%)metallic coating

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Journal of Iron and steel Research(International) 2019年第12期26卷 1304-1314页

作者： Wang-jun Peng Guang-xin Wu Yi Cheng Jie-yu Zhang State Key Laboratory of Advanced Special steel Shanghai UniversityShanghai 200072China Shanghai Key Laboratory of Advanced Ferrometallurgy Shanghai UniversityShanghai 200072China School of Materials Science and Engineering Shanghai UniversityShanghai 200072China

The microstructure,elemental distribution,phase composition,and thickness of intermetallic layers between high-strength low-alloy steel(H420)/mild carbon steel(DC51)and Al–43.4Zn–1.6Si(wt.%)(galvalume,GL)alloy were comparatively investigated.The experimental results reveal that the interfacial reaction layer was composed of Fe2Al5,Fe4Al13,and Al8Fe2Si intermetallic compounds.Moreover,the growth curves of the Fe2Al5 and Fe4Al13 intermetallic layers fit the parabolic law well,and the total thickness of the intermetallic layers of H420+GL was almost the same as that of DC51+GL.However,the thickness of the Fe2Al5 layer in H420+GL was thinner than that in DC51+GL.In addition,first-principle calculations were performed to explore the effect of Mn on the growth of the Fe2Al5 intermetallic phase,and the results indicate that Mn substitution in Fe2Al5 removes electronic charge from the Al atoms,thus decreasing the thickness of the Fe2Al5 interface layer.

关键词： high-strength low-alloy steel Mild carbon steel Al–43.4Zn–1.6Si(wt.%)alloy Interface reaction

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Visualization of microstructural factors resisting the crack propagation in mesosegregated high-strength low-alloy steel

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Journal of Materials Science & Technology 2020年第7期42卷 75-84页

作者： Shuxia Wang Chuanwei Li Lizhan Han Haozhang Zhong Jianfeng Gu Institute of Materials Modification and Modeling School of Materials Science and EngineeringShanghai Jiao Tong UniversityShanghai200240China Shanghai Key Laboratory of Materials Laser Processing and Modification Shanghai Jiao Tong UniversityShanghai200240China Collaborative Innovation Center for Advanced Ship and Deep Sea Exploration Shanghai Jiao Tong UniversityShanghai200240China Materials Genome Initiative Center Shanghai Jiao Tong UniversityShanghai200240China

While relationship between fracture mechanism and homogeneous microstructures has been fully understood,relationship between fracture mechanism and inhomogeneous microstructures such as the mesosegregation receives less attention as it deserves.Fracture mechanism of the high-strength low-alloy(HSLA)steel considering the mesosegregation was investigated and its corre s ponding micro structure was characterized in this paper.Mesosegregation re fers to the inhomogeneous distribution of alloy elements during casting solidification,and leads to the formation of positive segregation zones(PSZ)and negative segregation zones(NSZ)in ingots.The fracture surface of impact sample exhibits the quasi-cleavage fracture at-21℃,and is divided into ductile and brittle fracture zone.Meanwhile,the PSZ and NSZ spread across ductile and brittle fracture zone randomly.In ductile fracture zone,micro-voids fracture mechanism covers the PSZ and NSZ,and higher deformation degree is shown in the PSZ.In brittle fracture zone,secondary cleavage cracks are observed in both PSZ and NSZ,but present bigger size and higher quantity in the NSZ.However,some regions of the PSZ still present micro-voids fracture mechanism in brittle fracture zone.It reveals that the microstructures in the PSZ exhibit a higher resistance ability to crack propagation than that in the NSZ.All observations above provide a better visualization of the microstructural factors that resist the crack propagation.It is important to map all information regarding the fracture mechanism and mesosegregation to allow for further acceptance and industrial use.

关键词： high-strength low-alloy steel Heavy forgings Mesosegregation Inhomogeneous microstructures Fracture mechanism

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Effect of nanosized NbC precipitates on hydrogen-induced cracking of high-strength low-alloy steel

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International Journal of Minerals,Metallurgy and Materials 2021年第2期28卷 249-256页

作者： En-dian Fan Shi-qi Zhang Dong-han Xie Qi-yue Zhao Xiao-gang Li Yun-hua Huang Institution for Advanced Materials and Technology University of Science and Technology BeijingBeijing 100083China Key Laboratory of Advanced Materials(MOE) School of Materials Science and EngineeringTsinghua UniversityBeijing 100084China Ningbo Institute of Material Technology&Engineering Chinese Academy of SciencesNingbo 315201China

We investigated the effect of nanosized NbC precipitates on hydrogen-induced cracking(HIC)of high-strength low-alloy steel by conducting slow-strain-rate tensile tests(SSRT)and performing continuous hydrogen charging and fracture analysis.The results reveal that the HIC resistance of Nb-bearing steel is obviously superior to that of Nb-free steel,with the fractured Nb-bearing steel in the SSRT exhibiting a smaller ratio of elongation reduction(Iδ).However,as the hydrogen traps induced by NbC precipitates approach hydrogen saturation,the effect of the precipitates on the HIC resistance attenuate.We speculate that the highly dispersed nanosized NbC precipitates act as irreversible hydrogen traps that hinder the accumulation of hydrogen at potential crack nucleation sites.In addition,much like Nb-free steel,the Nb-bearing steel exhibits both H-solution strengthening and the resistance to HIC.

关键词： nanosized NbC precipitates high-strength low-alloy steel hydrogen-induced cracking slow-strain-rate tensile,hydrogen charging

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strengthening and toughening mechanism of a Cu-bearing high-strength low-alloy steel with refined tempered martensite/bainite(M/B)matrix and minor inter-critical ferrite

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Journal of Iron and steel Research(International) 2021年第4期28卷 464-478页

作者： Fei Zhu Feng Chai Xiao-bing Luo Zheng-yan Zhang Cai-fu Yang Department of Structural steels Central Iron and Steel Research InstituteBeijing 100081China

The microstructure–mechanical property relationship of a Cu-bearing low-carbon high-strength low-alloy steel,subjected to a novel multistage heat treatment including quenching(Q),lamellarization(L)and tempering(T),is presented.Yield strength of 989.5 MPa and average toughness at-80℃of 41 J were obtained in this steel after quenching and tempering(QT)heat treatments.Specimen QLT gained a little lower yield strength(982.5 MPa),but greatly enhanced average toughness at-80℃(137 J).To further clarify the strengthening and toughening mechanisms in specimen QLT,parameters of microstructural characteristic and crack propagation process were compared and analyzed for specimens Q,QL,QT and QLT.The microstructure of tempered martensite/bainite(M/B)in specimen QT changed to refined tempered M/B matrix mixed with minor IF(inter-critical ferrite)in specimen QLT.Cu-rich precipitates existed in tempered M/B for both specimens QT and QLT,as well as in IF.Compared with QT,adding a lamellarization step before tempering made the effective grains of specimen QLT refined and also led to coarser Cu-rich precipitates in tempered M/B matrix.The weaker strengthening effect of coarser Cu-rich precipitates should be a key reason for the slightly lower yield strength in specimen QLT than in specimen QT.No austenite was found in all specimens Q,QL,QT and QLT.Specimen QLT showed purely ductile fracture mode at-80℃due to the refined effective grains.The greatly improved toughness is mainly attributed to the enhanced energy of crack propagation.The combination of refined microstructure,softened matrix and deformation of minor'soft'IF during crack propagation led to the most superior toughness of specimen QLT among all specimens.

关键词： high-strength low-alloy steel Multistage heat treatment low-temperature toughness strengthening mechanism Grain refinement Crack propagation

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