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Highly Thermoconductive,Strong Graphene‑Based Composite Films by Eliminating Nanosheets Wrinkles

Nano-Micro Letters 2024年第1期16卷 328-340页

作者： Guang Xiao Hao Li Zhizhou Yu Haoting Niu Yagang Yao College of Engineering and Applied Sciences Jiangsu Key Laboratory of Artificial Functional Materialsand Collaborative Innovation Center of Advanced MicrostructuresNational Laboratory of Solid State MicrostructuresNanjing UniversityNanjing 210093People’s Republic of China Institute of Laser Manufacturing Henan Academy of SciencesZhengzhou 450052People’s Republic of China Center for Quantum Transport and Thermal Energy Science School of Physics and TechnologyNanjing Normal UniversityNanjing 210023People’s Republic of China

Graphene-based thermally conductive composites have been proposed as effective thermal management materials for cooling high-power electronic devices.However,when flexible Graphene nanosheets are assembled into macroscopic thermally conductive composites,capillary forces induce shrinkage of Graphene nanosheets to form wrinkles during solution-based spontaneous drying,which greatly reduces the thermal conductivity of the composites.Herein,Graphene nanosheets/aramid nanofiber(GNS/ANF)composite films with high thermal conductivity were prepared by in-plane stretching of GNS/ANF composite hydrogel networks with hydrogen bonds andπ-πinteractions.The in-plane mechanical stretching eliminates Graphene nanosheets wrinkles by suppressing inward shrinkage due to capillary forces during drying and achieves a high in-plane orientation of Graphene nanosheets,thereby creating a fast in-plane heat transfer channel.The composite films(GNS/ANF-60 wt%)with eliminated Graphene nanosheets wrinkles showed a significant increase in thermal conductivity(146 W m^(−1)K^(−1))and tensile strength(207 MPa).The combination of these excellent properties enables the GNS/ANF composite films to be effectively used for cooling flexible LED chips and smartphones,showing promising applications in the thermal management of high-power electronic devices.

关键词： Graphene Aramid nanofiber Wrinkles elimination In-plane stretching Thermal conductivity

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Self-Healing MXene-and Graphene-Based Composites:Properties and Applications

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Nano-Micro Letters 2023年第7期15卷 165-192页

作者： Atefeh Zarepour Sepideh Ahmadi Navid Rabiee Ali Zarrabi Siavash Iravani Department of Biomedical Engineering Faculty of Engineering and Natural SciencesIstinye University34396 IstanbulTürkiye Department of Medical Biotechnology School of Advanced Technologies in MedicineShahid Beheshti University of Medical SciencesTehran 19857-17443Iran Cellular and Molecular Biology Research Center Shahid Beheshti University of Medical SciencesTehran 19857-17443Iran Centre for Molecular Medicine and Innovative Therapeutics Murdoch UniversityPerthWA 6150Australia School of Engineering Macquarie UniversitySydneyNSW 2109Australia Faculty of Pharmacy and Pharmaceutical Sciences Isfahan University of Medical SciencesEsfahān 81746-73461Iran

Today,self-healing Graphene-and MXene-based composites have attracted researchers due to the increase in durability as well as the cost reduction in long-time applications.Different studies have focused on designing novel self-healing Graphene-and MXenebased composites with enhanced sensitivity,stretchability,and flexibility as well as improved electrical conductivity,healing efficacy,mechanical properties,and energy conversion efficacy.These composites with self-healing properties can be employed in the field of wearable sensors,supercapacitors,anticorrosive coatings,electromagnetic interference shielding,electronic-skin,soft robotics,etc.However,it appears that more explorations are still needed to achieve composites with excellent arbitrary shape adaptability,suitable adhesiveness,ideal durability,high stretchability,immediate self-healing responsibility,and outstanding electromagnetic features.Besides,optimizing reaction/synthesis conditions and finding suitable strategies for functionalization/modification are crucial aspects that should be comprehensively investigated.MXenes and Graphene exhibited superior electrochemical properties with abundant surface terminations and great surface area,which are important to evolve biomedical and sensing applications.However,flexibility and stretchability are important criteria that need to be improved for their future applications.Herein,the most recent advancements pertaining to the applications and properties of self-healing Graphene-and MXene-based composites are deliberated,focusing on crucial challenges and future perspectives.

关键词： MXenes Graphene Self-healing materials Electromagnetic interference shielding Wearable sensors

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Generation of mode‑locked states of conventional solitons and bright‑dark solitons in Graphene mode‑locked fber laser

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Frontiers of Optoelectronics 2023年第2期16卷 71-80页

作者： Zixiong Li Mingyu Li Xinyi Hou Lei Du Lin Xiao Tianshu Wang Wanzhuo Ma Department of Optical Engineering School of Opto-Electronic EngineeringChangchun University of Science and TechnologyChangchun 130022China

This paper proposes a mode-locked fber laser based on Graphene-coated microfber.The total length of the fber laser resonant cavity is 31.34 m.Under the condition of stable output of bright-dark soliton pairs from the fber laser,dual-wavelength tuning is realized by adjusting the polarization controller(PC),and the wavelength tuning range is 11 nm.Furthermore,the efects of polarization states on bright-dark solitons are studied.It is demonstrated that the mode-locking state can be switched between conventional solitons and bright-dark solitons in the Graphene mode-locked fber laser.Bright-dark soliton pairs with diferent shapes and nanosecond pulse width can be obtained by adjusting the PC and pump power.

关键词： Fiber laser Graphene Conventional soliton Bright-dark soliton pairs

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MXene‑Graphene Composites:A Perspective on Biomedical Potentials

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Nano-Micro Letters 2022年第8期14卷 112-123页

作者： Ebrahim Mostafavi Siavash Iravani Stanford Cardiovascular Institute Stanford University School of MedicineStanfordCA 94305USA Department of Medicine Stanford University School of MedicineStanfordCA 94305USA Faculty of Pharmacy and Pharmaceutical Sciences Isfahan University of Medical SciencesIsfahanIran

MXenes,transition metal carbides and nitrides with Graphene-like structures,have received considerable attention since their first discovery.On the other hand,Graphene has been extensively used in biomedical and medicinal applications.MXene and Graphene,both as promising candidates of two-dimensional materials,have shown to possess high potential in future biomedical applications due to their unique physicochemical properties such as superior electrical conductivity,high biocompatibility,large surface area,optical and magnetic features,and extraordinary thermal and mechanical properties.These special structural,functional,and biological characteristics suggest that the hybrid/composite structure of MXene and Graphene would be able to meet many unmet needs in different fields;particularly in medicine and biomedical engineering,where high-performance mechanical,electrical,thermal,magnetic,and optical requirements are necessary.However,the hybridization and surface functionalization should be further explored to obtain biocompatible composites/platforms with unique physicochemical properties,high stability,and multifunctionality.In addition,toxicological and long-term biosafety assessments and clinical translation evaluations should be given high priority in research.Although very limited studies have revealed the excellent potentials of MXene/Graphene in biomedicine,the next steps should be toward the extensive research and detailed analysis in optimizing the properties and improving their functionality with a clinical and industrial outlook.Herein,different synthesis/fabrication methods and performances of MXene/Graphene composites are discussed for potential biomedical applications.The potential toxicological effects of these composites on human cells and tissues are also covered,and future perspectives toward more successful translational applications are presented.The current state-of-the-art biotechnological advances in the use of MXene-Graphene composites,as well as their developmental challenges and future p

关键词： Graphene MXene Composites Hybrid structures Biocompatibility Cancer theranostics Biomedical engineering

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Copper acetate-facilitated transfer-free growth of high-quality Graphene for hydrovoltaic generators

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National Science Review 2022年第7期9卷 71-79页

作者： Jingyuan Shan Sunmiao Fang Wendong Wang Wen Zhao Rui Zhang Bingzhi Liu Li Lin Bei Jiang Haina Ci Ruojuan Liu Wen Wang Xiaoqin Yang Wenyue Guo Mark H.Rümmeli Wanlin Guo Jingyu Sun Zhongfan Liu Center for Nanochemistry (CNC) Beijing Science and Engineering Center for Nanocarbons Beijing National Laboratory for Molecular Sciences College of Chemistry and Molecular Engineering Peking University Academy for Advanced Interdisciplinary Studies Peking University Key Laboratory for Intelligent Nano Materials and Devices of the Ministry of Education State Key Laboratory of Mechanics and Control of Mechanical Structures Institute of Nanoscience Nanjing University of Aeronautics and Astronautics Department of Physics and Astronomy University of Manchester School of Materials Science and Engineering China University of Petroleum (East China) College of Energy Soochow Institute for Energy and Materials Innovations (SIEMIS)Jiangsu Provincial Key Laboratory for Advanced Carbon Materials and Wearable Energy TechnologiesSoochow University Beijing Graphene Institute (BGI)

Direct synthesis of high-quality Graphene on dielectric substrates without a transfer process is of vital importance for a variety of applications.Current strategies for boosting high-quality Graphene growth,such as remote metal catalyzation,are limited by poor performance with respect to the release of metal catalysts and hence suffer from a problem with metal residues.Herein,we report an effective approach that utilizes a metal-containing species,copper acetate,to continuously supply copper clusters in a gaseous form to aid transfer-free growth of Graphene over a wafer scale.The thus-derived Graphene films were found to show reduced multilayer density and improved electrical performance and exhibited a carrier mobility of8500 cm~2 V-1s-1.Furthermore,droplet-based hydrovoltaic electricity generator devices based on directly grown Graphene were found to exhibit robust voltage output and long cyclic stability,in stark contrast to their counterparts based on transferred Graphene,demonstrating the potential for emerging energy harvesting applications.The work presented here offers a promising solution to organize the metal catalytic booster toward transfer-free synthesis of high-quality Graphene and enable smart energy generation.

关键词： chemical vapor deposition Graphene copper acetate hydrovoltaic electricity generator transfer-free growth

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Transfer-free chemical vapor deposition Graphene for nitride epitaxy: challenges, current status and future outlook

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Science China Chemistry 2024年第3期67卷 824-840页

作者： Xiang Gao Senlin Li Jingfeng Bi Kaixuan Zhou Meng Li Zhongfan Liu Jingyu Sun College of Energy Soochow Institute for Energy and Materials InnovationsSUDA-BGI Collaborative Innovation CenterKey Laboratory of Advanced Carbon Materials and Wearable Energy Technologies of Jiangsu ProvinceSoochow UniversitySuzhou 215006China Beijing Graphene Institute Beijing 100095China Xiamen Silan Advanced Compound Semiconductor Co.Ltd. Xiamen 361026China

Graphene, a two-dimensional material with outstanding electrical and mechanical properties, has attracted considerable attention in the field of semiconductor technologies due to its potential use as a buffer layer for the epitaxial Ⅲ-nitride growth. In recent years, significant progress has been made in the chemical vapor deposition growth of Graphene on various insulating substrates for the nitride epitaxy, which offers a facile, inexpensive, and easily scalable methodology. However, certain challenges are still present in the form of producing high-quality Graphene and achieving optimal interface compatibility with Ⅲ-nitride materials.In this review, we provide an overview of the bottlenecks associated with the transferred Graphene fabrication techniques and the state-of-the-art techniques for the transfer-free Graphene growth. The present contribution highlights the current progress in the transfer-free Graphene growth on different insulating substrates, including sapphire, quartz, SiO_(2)/Si, and discusses the potential applications of transfer-free Graphene in the Ⅲ-nitride epitaxy. Finally, it includes the prospects of the transfer-free Graphene growth for the Ⅲ-nitride epitaxy and the challenges that should be overcome to realize its full potential in this field.

关键词： Transfer-free chemical vapor deposition Graphene for nitride epitaxy challenges current status and future outlook Graphene

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Nb_(2)O_(5) nanocrystals decorated Graphene composites as anode materials for high-performance dual-ion batteries

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Nano Research 2024年第3期17卷 1535-1541页

作者： Lei Wang Fei Huang Guoyin Zhu Zhihui Dai Jiangsu Collaborative Innovation Center of Biomedical Functional Materials Jiangsu Key Laboratory of Biofunctional MaterialsSchool of Chemistry and Materials ScienceNanjing Normal UniversityNanjing 210023China Institute of Advanced Materials and Flexible Electronics(IAMFE) School of Chemistry and Materials ScienceNanjing University of Information Science&TechnologyNanjing 210044China School of Chemistry and Molecular Engineering Nanjing Tech UniversityNanjing 211816China

Niobium oxide(Nb_(2)O_(5))is a promising material in photocatalytic,solar cell,electronic like electron field emitters,and especially lithium-ion batteries(LIBs)because of its adjustable morphologies,controllable crystal type,stable structure,and environmental friendliness.However,its low electrical conductivity lowers the rate performance and limits the practical applications in LIBs.Herein,we present a one-step solid-state synthesis of orthogonal Nb_(2)O_(5) nanocrystals/Graphene composites(Nb_(2)O_(5)/G)as high-performance anode materials in LIBs.Benefiting from the nanoscale crystalline structure Nb_(2)O_(5) and highly-conductive Graphene substrate,the as-prepared Nb_(2)O_(5)/G exhibits excellent electrochemical performances.Impressively,a reversible structural phase transition between orthogonal Nb_(2)O_(5) and tetragonal Li1-xNbO_(2)(0Graphene composite anode and a comprehension of its electrochemical reaction mechanism.

关键词： niobium oxide Graphene anode dual-ion batteries graphite intercalation

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Graphene and Graphene-based materials in axonal repair of spinal cord injury

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Neural Regeneration Research 2022年第10期17卷 2117-2125页

作者： Shi-Xin Wang Yu-Bao Lu Xue-Xi Wang Yan Wang Yu-Jun Song Xiao Wang Munkhtuya Nyamgerelt School of Basic Medical Sciences Lanzhou UniversityLanzhouGansu ProvinceChina The Second Clinical Medical College Lanzhou UniversityLanzhouGansu ProvinceChina Department of Spine Surgery The Third Affiliated HospitalSun Yat-sen UniversityGuangzhouGuangdong ProvinceChina Key Laboratory of Evidence-Based Medicine and Knowledge Translation of Gansu Province LanzhouGansu ProvinceChina

Graphene and Graphene-based materials have the ability to induce stem cells to differentiate into neurons,which is necessary to overcome the current problems faced in the clinical treatment of spinal cord injury.This review summarizes the advantages of Graphene and Graphene-based materials(in particular,composite materials)in axonal repair after spinal cord injury.These materials have good histocompatibility,and mechanical and adsorption properties that can be targeted to improve the environment of axonal regeneration.They also have good conductivity,which allows them to make full use of electrical nerve signal stimulation in spinal cord tissue to promote axonal regeneration.Furthermore,they can be used as carriers of seed cells,trophic factors,and drugs in nerve tissue engineering scaffolds to provide a basis for constructing a local microenvironment after spinal cord injury.However,to achieve clinical adoption of Graphene and Graphene-based materials for the repair of spinal cord injury,further research is needed to reduce their toxicity.

关键词： axonal regeneration Graphene Graphene oxide nerve axon regeneration reduced Graphene oxide spinal cord contusions spinal cord injury spinal cord trauma

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Light-modulated Graphene-based φ_(0) Josephson junction and -φ_(0) to φ_(0) transition

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Chinese Physics B 2024年第2期33卷 476-481页

作者：程任翔于苗汪洪曹德亮李兴鳌戚凤华周兴飞 New Energy Technology Engineering Laboratory of Jiangsu Province School of ScienceNanjing University of Posts and TelecommunicationsNanjing 210023China School of Electronic and Information Engineering Jinling Institute of TechnologyNanjing 211169China School of Electronic Engineering Nanjing Xiaozhuang UniversityNanjing 211171China

We investigate the chiral edge states-induced Josephson current–phase relation in a Graphene-based Josephson junction modulated by the off-resonant circularly polarized light and the staggered sublattice potential.By solving the Bogoliubov–de Gennes equation,a φ_(0) Josephson junction is induced in the coaction of the off-resonant circularly polarized light and the staggered sublattice potential,which arises from the fact that the center of-mass wave vector of Cooper pair becomes finite and the opposite center of-mass wave vector to compensate is lacking in the nonsuperconducting region.Interestingly,when the direction of polarization of light is changed,-φ_(0) to φ_(0) transition generates,which generalizes the concept of traditional 0–πtransition.Our findings provide a purely optical way to manipulate a phase-controllable Josephson device and guidelines for future experiments to confirm the presence of Graphene-based φ_(0)Josephson junction.

关键词： Graphene circularly polarized light staggered sublattice potential φ_(0)Josephson junction

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Graphene enables equiatomic FeNiCrCoCu high-entropy alloy with improved TWIP and TRIP effects under shock compression

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Journal of Materials Science & Technology 2024年第3期170卷 186-199页

作者： Hongcai Xie Zhichao Ma Wei Zhang Hongwei Zhao Luquan Ren School of Mechanical and Aerospace Engineering Jilin UniversityChangchun 130025China Key Laboratory of CNC Equipment Reliability Ministry of Education Jilin UniversityChangchun 130025China Key Laboratory of Bionic Engineering Ministry of Education Jilin UniversityChangchun 130025China Weihai Institute for Bionics-Jilin University Weihai 264400China Institute of Structured and Architected Materials Liaoning Academy of MaterialsShenyang 110167China

Graphene(Gr)reinforced high-entropy alloy(HEA)matrix composites are expected as potential candidates for next-generation structural applications in light of outstanding mechanical properties.A deep comprehension of the underlying deformation mechanisms under extreme shock loading is of paramount importance,however,remains lacking due to experimentally technical limitations in existence.In the present study,by means of nonequilibrium molecular dynamics simulations,dynamic deformation behaviors and corresponding mechanisms in equiatomic FeNiCrCoCu HEA/Gr composite systems were investigated in terms of various shock velocities.The resistance to dislocation propagation imparted by Gr was corroborated to encourage the elevated local stress level by increasing the likelihood of dislocation interplays,which facilitated the onset of twins and hexagonal close-packed(HCP)martensite laths.Meanwhile,the advent of Gr was demonstrated to endow the HEA with an additional twinning pathway that induced a structural conversion from HCP to parent face-centered cubic(FCC)inside HCP martensite laths,different from the classical one that necessitated undergoing the intermediate procedure of extrinsic stacking fault(ESF)evolution.More than that,by virtue of an increase in flow stress,the transformation-induced plasticity(TRIP)effect was validated to be additionally evoked as the predominant strain accommodation mechanism at higher strains on the one hand,but which only assisted plasticity in pure systems,and on the other hand,can also act as an auxiliary regulation mode together with the twinning-induced plasticity(TWIP)effect under intermediate strains,but with enhanced contributions relative to pure systems.One may expect that TRIP and TWIP effects promoted by introducing Gr would considerably inspire a synergistic effect between strength and ductility,contributing to the exceptional shock-resistant performance of FeNiCrCoCu HEAs under extreme regimes.

关键词： Molecular dynamics High-entropy alloy Graphene TRIP TWIP Shock

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