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High-response n-butanol gas sensor based on ZnO/In_(2)O_(3) heterostructure

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Rare Metals 2023年第1期42卷 198-209页

作者： Zhen-Yu Yuan Fan Yang Hong-Min Zhu Fan-Li Meng Medhat Ibrahim College of Information Science and Engineering Northeastern UniversityShenyang110819China Spectroscopy Department National Research CentreGiza12622Egypt

In this study,ZnO/In_(2)O_(3)-heterostructured nanosheets were prepared using a one-step hydrothermal *** effects of ZnO content on the gas-sensing performance were discussed,with ZnO/In_(2)O_(3)-2 exhibiting the highest performance among the prepared *** response of ZnO/In_(2)O_(3)-2 to n-butanol was 302 at 26℃,which was 11.93 times higher than that of pure In_(2)O_(3).Among the eight tested gases,ZnO/In_(2)O_(3)-2 displayed the highest response to ***,the lower detection limit of the ZnO/In_(2)O_(3)nanosheets was reduced from 10×10^(-6)to 0.1×10^(-6)(for pure In_(2)O_(3)nanosheets)toward *** is because the doping of Zn2+increases the number of oxygen vacancies on the sensor surface and allows the formation of an n-n heterostructure between ZnO and In_(2)O_(3),which increases the initial resistance of the sensor.

关键词： High-response N-N heterostructure N-butanol gas sensor

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Borophene gas sensor

Nano Research 2022年第3期15卷 2537-2544页

作者： Chuang Hou Guoan Tai Yi Liu Xiang Liu The State Key Laboratory of Mechanics and Control of Mechanical Structures and Laboratory of Intelligent Nano Materials and Devices of Ministry of Education College of Aerospace EngineeringNanjing University of Aeronautics and AstronauticsNanjing 210016China

High-performance gas sensing devices have been extensively studied in industrial production,clinical medicine and environmental *** the materials used to fabricate gas sensors,two-dimensional(2D)materials are viewed as favorable candidate sensing materials because of their high surface-to-volume ratios,abundant surface activity,defect ***,gas sensors based on the previously reported 2D materials have some disadvantages such as poor air-stability and slow dynamic ***,borophene,as a unique 2D material,has been theoretically predicted to have excellent gas sensing characteristic,especially for nitrogen dioxide(NO_(2)).However,the gas sensing property of borophene has not been still reported ***,we report that a chemiresistive sensor device based on borophene shows high sensitivity,fast response,high selectivity,good flexibility and long-time *** is found that the sensor has a low experimental detection limit of around 200 ppb,a large detection range from 200 ppb to 100 ppm,and fast response time of 30 s and recovery time of 200 s at room temperature,which are remarkably superior to those of reported 2D *** underlying NO_(2) sensing mechanism of borophene is revealed by first-principles *** line with theoretical predication,it has also been confirmed experimentally that the borophene-based sensor has a unique selectivity to NO_(2) compared with other common ***,the sensor also displays superior flexibility and stability under different bending *** study shows excellent electronic and sensing characteristic of borophene,which indicates that it has great potential application value in high-performance sensing and detection in the future.

关键词： borophene gas sensor charge transfer wearable application density functional theory

Enhancement of the Sensitivity of gas sensor Based on Microstructure Optical Fiber

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Photonic sensors 2015年第4期5卷 312-320页

作者： Monir MORSHED Md. Imran HASAN S. M. Abdur RAZZAK Department of lnformation and Communication Technology Mawlana Bhashani Science and Technology University Tangail-1902 Bangladesh Department of Electronics & Telecommunication Engineering Rajshahi University of Engineering & Technology Rajshahi-6204 Bangladesh Department of Electrical & Electronic Engineering Rajshahi University of Engineering & Technology Rajshahi-6204 Bangladesh

This paper proposes the design and characterization of microstructure optical fiber for gas sensing applications. The aim is to detect toxic and colorless gases over a wide transmission band covering 0.80 gm to 2.00gm wavelength. Numerical investigation is carried out by using the finite element method （FEM）. The numerical study shows that sensitivity of the proposed sensor is moderately increased by introducing four non-circular holes around the defected core of photonic crystal fiber and the confinement loss is also reduced. Furthermore, we confirm that increasing the diameter of central air core and size of the non-circular holes can improve the relative sensitivity and the confinement loss is reduced by increasing the diameter of air holes in the cladding. The enhancement of the relative sensitivity is more than 27.58% （0.1323 to 0.1688） at the wavelength 2=1.33gm that is the absorption line of methane （CH4） and hydrogen fluoride （HF） gases. The confinement loss of the fiber is 1.765x 10-8dB/m.

关键词： Confinement loss gas sensor hollow core photonic crystal fiber microstrucmre fiber relativesensitivity

Porous γ-Fe_(2)O_(3) nanoparticle decorated with atomically dispersed platinum: Study on atomic site structural change and gas sensor activity evolution

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Nano Research 2021年第5期14卷 1435-1442页

作者： Qiheng Li Zhi Li Qinghua Zhang Lirong Zheng Wensheng Yan Xiao Liang Lin Gu Chen Chen Dingsheng Wang Qing Peng Yadong Li Department of Chemistry Tsinghua UniversityBeijing100084China School of Physical Sciences University of Chinese Academy of SciencesBeijing100190China Beijing Synchrotron Radiation Facility Institute of High Energy PhysicsChinese Academy of SciencesBeijing100049China National Synchrotron Radiation Laboratory(NSRL) University of Science and Technology of ChinaHefei230029China

Decorating semi-conducting metal oxide with noble metal has been recognized as a viable approach to improve the sensitivity of gas sensor. However, conventional method which relys on noble metal nanoparticles is confronted with drawback of significantly increased cost. To maximize the atom efficiency and reduce the cost for practical industrial application, designing sensor material with noble metal isolated single atom sites (ISAS) doping is a desired option. Here, we report an atomically dispersed platinum on one-dimensional arranged porous γ-Fe2O3 nanoparticle composites as highly efficient ethanol gas sensor. The optimized sample (Pt1-Fe2O3-ox) exhibited a high response (Ra/Rg = 102.4) and good selectivity to ethanol gas. It is demonstrated only the Pt single atom sites with high valance can effectively promote the adsorption capacity to ethanol and consequently enhance the sensitivity of sensing process by changing the electrical structure of Fe2O3 support. This work indicates the single atom sites could play a vital role in improving the performance of conventional metal oxides gas sensors and pave way for the exploration of ISAS-enhanced gas sensor for other volatile organic compounds (VOCs).

关键词： isolated single atom sites structure-activity relationship gas sensor nanocomposites

Berlin Green Framework‑Based gas sensor for Room‑Temperature and High‑Selectivity Detection of Ammonia

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Nano-Micro Letters 2021年第4期13卷 146-158页

作者： Tingqiang Yang Lingfeng Gao Wenxuan Wang Jianlong Kang Guanghui Zhao Delong Li Wen Chen Han Zhang Institute of Microscale Optoelectronics Collaborative Innovation Centre for Optoelectronic Science and TechnologyKey Laboratory of Optoelectronic Devices and Systems of Ministry of Education and Guangdong ProvinceCollege of Physics and Optoelectronic EngineeringShenzhen Key Laboratory of Micro‑Nano Photonic Information TechnologyGuangdong Laboratory of Artificial Intelligence and Digital Economy(SZ)Shenzhen UniversityShenzhen 518060People’s Republic of China State Key Laboratory of Advanced Technology for Materials Synthesis and Processing School of Materials Science and EngineeringWuhan University of TechnologyWuhan 430070People’s Republic of China Research Center for Materials Genome Engineering Wuhan University of TechnologyWuhan 430070People’s Republic of China

Ammonia detection possesses great potential in atmosphere environmental protection,agriculture,industry,and rapid medical ***,it still remains a great challenge to balance the sensitivity,selectivity,working temperature,and response/recovery *** this work,Berlin green(BG)framework is demonstrated as a highly promising sensing material for ammonia detection by both density functional theory simulation and experimental gas sensing *** in BG framework offers abundant active sites for ammonia absorption,and the absorbed ammonia transfers sufficient electron to BG,arousing remarkable enhancement of *** BG framework shows remarkable response to ammonia at 50–110°C with the highest response at 80°C,which is jointly influenced by ammonia’s absorption onto BG surface and insertion into BG *** sensing performance of BG can hardly be achieved at room temperature due to its high *** of conductive Ti3CN MXene overcomes the high resistance of pure BG framework,and the simply prepared BG/Ti3CN mixture shows high selectivity to ammonia at room temperature with satisfying response/recovery speed.

关键词： Berlin green framework gas sensor Ammonia Room temperature High selectivity

Room temperature gas sensor based on tube-like hydroxyapatite modified with gold nanoparticles

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Journal of Central South University 2016年第1期23卷 18-26页

作者：罗兰兰刘咏谭彦妮李会霞张青李昆 State Key Laboratory of Powder Metallurgy Central South University

The main goal of this work is to explore the possibility of using Au-modified hydroxyapatite(HA) as a potential sensor material. Tube-like HA structure was fabricated with the aid of a Nafion N-117 cation exchange membrane and gold(Au) nanoparticles were added by a hydrothermal method. The morphology, structure and composition were characterized by scanning electron microscopy(SEM), transmission electron microscopy(TEM), X-ray diffraction(XRD), and X-ray photoelectron spectroscopy(XPS). The gas sensing properties were also investigated. Results show that Au nanoparticles are dispersed into the HA powder, which is tube-like, with rough inner and outer surfaces. Compared with pure HA, Au-modified HA exhibits improved sensing properties for NH_3. 5%(mass fraction) Au-modified HA shows the highest response with relatively short response/recovery time. The response is up to 79.2% when the corresponding sensor is exposed to 200×10^(-6) NH_3 at room temperature, and the response time and recovery time are 20 s and 25 s, respectively. For lower concentration, like 50×10^(-6), the response is still up to 70.8%. Good selectivity and repeatability are also observed. The sensing mechanism of high response and selectivity for NH_3 gas was also discussed. These results suggest that Au-HA composite is a promising material for NH_3 sensors operating at room temperature.

关键词： gas sensor Au nanoparticles hydroxyapatite gas selectivity ammonia gas

Air-stable,all-dry transferred ReS_(2)/gase heterostructure-based NO_(2)gas sensor

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Journal of Materials Science & Technology 2024年第1期168卷 79-87页

作者： A.Venkatesan Hyeyoon Ryu Anupom Devnath Hyungyu Yoo Seunghyun Lee Department of Electronic Engineering Kyung Hee UniversityYongin-Si 17104South Korea Department of Electronics and Information Convergence Engineering Kyung Hee UniversityYongin-Si 17104South Korea

Two-dimensional(2D)materials have gained considerable attention in chemical sensing owing to their naturally high surface-to-volume ***,the poor response time and incomplete recovery re-strict their application in practical,high performance gas *** this work,we fabricated air-stable ReS_(2)/gase heterostructure-based NO_(2)gas sensors with excellent gas sensing response,recovery,selectiv-ity and a low limit of detection(LOD)toward nitrogen dioxide(NO_(2)).The ReS_(2)/gase heterostructure was prepared via mechanical exfoliation and an all-dry transfer *** the sensing measurements,temperature-dependant transport measurements were carried *** Schottky Barrier Height(SBH)of the ReS_(2)/gase heterostructure was calculated and the corresponding transport mechanisms were *** fabricated gas sensors showed a significant response enhancement with full reversibility to-ward ppm-level NO_(2)(response of∼17%at 3 ppm,a LOD of∼556 ppb)at an operating temperature of(33°C).In particular,the total response and recovery time of the ReS_(2)/gase was revealed to be less than 4 min(∼38 s and∼174 s,respectively)for the 250 ppm concentration,which is one of the best response and recovery time toward ppm-level NO_(2).The excellent sensing performances and recovery characteris-tics of the ReS_(2)/gase structure are attributed to its efficient charge separation,unique interlayer coupling and desirable band *** atomically thin,ultrasensitive gas sensor that operates at room tem-perature is a strong technological contender to conventional metal oxide gas sensors,which often require elevated temperatures.

关键词： 2D materials All-dry transfer gas sensor Van der Waals heterostructure ReS_(2)/gase gas sensing response Transition metal dichalcogenide

Achieving highly-efficient H2S gas sensor by flower-like SnO_(2)–SnO/porous GaN heterojunction

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Chinese Physics B 2023年第2期32卷 193-200页

作者：刘增都灵张少辉边昂方君鹏邢晨阳李山汤谨诚郭宇锋唐为华 College of Integrated Circuit Science and Engineering Nanjing University of Posts and TelecommunicationsNanjing 210023China National and Local Joint Engineering Laboratory for RF Integration and Micro-Packing Technologies Nanjing University of Posts and TelecommunicationsNanjing 210023China School of Electronic and Information Engineering Jinling Institute of TechnologyNanjing 211169China Institute of Microscale Optoelectronics Shenzhen UniversityShenzhen 518060China Key Laboratory of Luminescence and Optical Information of Ministry of Education Institute of Optoelectronic TechnologyBeijing Jiaotong UniversityBeijing 100044China School of Integrated Circuits Tsinghua UniversityBeijing 100044China Key Laboratory of Optoelectronic Devices and Systems of Ministry of Education College of Physics and Optoelectronic EngineeringShenzhen UniversityShenzhen 518060China State Key Laboratory of Information Photonics and Optical Communications School of ScienceBeijing University of Posts and TelecommunicationsBeijing 100876China

A flower-like SnO_(2)–SnO/porous Ga N(FSS/PGaN) heterojunction was fabricated for the first time via a facile spraying process, and the whole process also involved hydrothermal preparation of FSS and electrochemical wet etching of GaN,and SnO_(2)–SnO composites with p–n junctions were loaded onto PGaN surface directly applied to H_(2)S sensor. Meanwhile,the excellent transport capability of heterojunction between FSS and PGaN facilitates electron transfer, that is, a response time as short as 65 s and a release time up to 27 s can be achieved merely at 150℃ under 50 ppm H_(2)S concentration, which has laid a reasonable theoretical and experimental foundation for the subsequent PGaN-based heterojunction gas *** lowering working temperature and high sensitivity(23.5 at 200 ppm H2S) are attributed to the structure of PGaN itself and the heterojunction between SnO_(2)–SnO and PGaN. In addition, the as-obtained sensor showed ultra-high test *** simple design strategy of FSS/PGaN-based H_(2)S sensor highlights its potential in various applications.

关键词： gas sensor SnO_(2)–SnO porous GaN heterojunction

Sensing mechanism of Ag/α-MoO_(3) nanobelts for H_(2)S gas sensor

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Rare Metals 2021年第6期40卷 1545-1553页

作者： Shi-Kai Shen Xin-Lei Cui Chuan-Yu Guo Xin Dong Xian-Fa Zhang Xiao-Li Cheng Li-Hua Huo Ying-Ming Xu School of Electrical Engineering Suihua UniversitySuihua 152000China Key Laboratory of Functional Inorganic Material Chemistry Ministry of Education of the People’s Republic of ChinaHeilongjiang UniversityHarbin 150080China Key Laboratory for Polymeric Composite and Functional Materials of Ministry of Education Guangdong Engineering Technology Research Center for High-Performance Organic and Polymer Photoelectric Functional FilmsSchool of ChemistrySun Yat-Sen UniversityGuangzhou 510275China

Sensing mechanism is still a big problem in the field of gas ***-depth study of the sensing mechanism can provide better ideas for the design of sensing materials,and it is also more conducive to the improvement in gas-sensing *** this work,Ag/α-MoO_(3) material was obtained by loading Ag in α-MoO_(3) nanobelts prepared by hydrothermal *** material was characterized by field electron scanning electron microscopy(SEM),high-resolution transmission electron microscopy(HRTEM),X-ray diffraction(XRD) and X-ray photoelectron spectroscopy(XPS).Comparing the gas sensing properties of α-MoO_(3) and Ag/α-MoO_(3),it is found that Ag effectively improves the selectivity of the material to H_(2)S at 133℃.The response of the 5 wt% Ag/α-MoO_(3) sensor to 100 × 10-6 hydrogen sulfide(H_(2)S) is 225 and the detection limit is 100 ×10^(-9).The sensing mechanism was verified by gas chromatography and mass spectrometer(GC-MS),XPS and Fourier transform infrared spectroscopy(FTIR).

关键词： Ag/α-MoO_(3) Nanobelt gas sensor Hydrogen sulfide Sensing mechanism