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Effect of Filler Composition on the Brazing of Alumina to copper Using Ultrasonic Wave

Journal of Materials Science & Technology 2003年第z1期19卷 176-178页

作者： Khalid M. HAFEZ Masaaki NAKA Joining & Welding Research Institute Osaka University Ibaraki Osaka 567-0047 Japan Joining & Welding Research Institute Osaka University Ibaraki Osaka 567-0047 Japan

An ultrasonic wave was applied during brazing of alumina to Cu. First alumina was metallized by applying ultrasonicwave in braze bath. Then the metallized alumina was brazed with Cu using the same filler alloy. The filler used wereZn-Al alloys and Zn-Sn Alloys. The weight percent of Al in filler was ranging between 0, 5%, 10%, *** weight percent of tin in filler was ranging between 0, 30%, 60% and 91%, respectively. The joining mechanismwas investigated by measuring the joining strength, hardness and analyzing the microstructure at interface of thejoint. The shear strength and microstructure of the joint strongly depend on the filler composition. The effect ofultrasound was derived primarily from acoustic cavitations, impact and friction of the filler against alumina *** improved the wetting between alumina and the filler, and reflected to improve the joint strength. Anotherultrasonic advantage as to reduce of the joining temperature, that reduced the thermal stress in the braze joint.

关键词： Alumina, copper, Ultrasonic waves, Fracture stress, Microstructure, Brazing

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Synthesis,characterization,properties and crystal structure of heterometallic 1D coordination polymers {[CuLZn·CuLZn(H_2O)]·H_2O}_n

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Science China Chemistry 2006年第4期49卷 338-344页

作者： TAO Ruojie1, LI Fu’an1, ZANG Shuangquan1, CHENG Yanxiang2 & NIU Jingyang1 1. Chemistry and Chemical Engineering College of Henan University, Kaifeng 475001, China 2. Changchun Institute of Applied Chemistry, Chinese Academy of Sciences, Changchun 130022, China 1. Chemistry and Chemical Engineering College of Henan University Kaifeng 475001 China 2. Changchun Institute of Applied Chemistry Chinese Academy of Sciences Changchun 130022 China

copper-zinc heterometallic 1D chain coordination polymer has been synthesized and characterized by elemental analysis, and IR spectra etc. The crystal structure was determined by single-crystal X-ray diffraction analyses. The title complex is 1D chain coordination polymer with the chemical formula {[CuLZn·CuLZn(H2O)]·H2O}n, where H4L=N-(2-hydroxybenzamido)-N’-(3-carboxy- lsalicylidene)ethylenediamine. Its structural unit is comprosed of two tetranuclear cycles formed by two dissymmetrical tetranuclear units. These units polymerized each other to form 1D chain coordi- nation polymer.

关键词： copper, zinc, heterometallic coordination polymer, crystal structure.

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