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Enhancing micro-scale SiOx anode durability:Electro-mechanical strengthening of binder networks via anchoring carbon nanotubes with carboxymethyl cellulose

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Journal of Energy Chemistry 2025年第2期101卷 23-33页

作者： Chaeyeon Ha Jin Kyo Koo Jun Myoung Sheem Young-Jun Kim SKKU Advanced Institute of Nano Technology (SAINT) Sungkyunkwan University Department of Nano Science and Technology Sungkyunkwan University Advanced Center for Convergence Energy Storage System Sungkyunkwan University SKKU Institute of Energy Science and Technology (SIEST) Sungkyunkwan University

With the increasing prevalence of lithium-ion batteries（LIBs） applications,the demand for high-capacity next-generation materials has also *** currently considered a promising anode material due to its exceptionally high capacity for ***,the significant volumetric changes of SiOxduring cycling and its initial Coulombic efficiency（ICE） complicate its use,whether alone or in combination with graphite *** this study,a three-dimensional conductive binder network with high electronic conductivity and robust elasticity for graphite/SiOxblended anodes was proposed by chemically anchoring carbon nanotubes and carboxymethyl cellulose binders using tannic acid as a chemical *** addition,a dehydrogenation-based prelithiation strategy employing lithium hydride was utilized to enhance the ICE of *** combination of these two strategies increased the CE of SiOxfrom 74% to87% and effectively mitigated its volume expansion in the graphite/SiOxblended electrode,resulting in an efficient electron-conductive binder *** led to a remarkable capacity retention of 94% after30 cycles,even under challenging conditions,with a high capacity of 550 mA h g-1and a current density of 4 mA ***,to validate the feasibility of utilizing prelithiated SiOxanode materials and the conductive binder network in LIBs,a full cell incorporating these materials and a single-crystalline Ni-rich cathode was *** cell demonstrated a～27.3% increase in discharge capacity of the first cycle(～185.7 mA h g-1) and exhibited a cycling stability of 300 ***,this study reports a simple,feasible,and insightful method for designing high-performance LIB electrodes.

关键词： Lithium-ion batteries SiO x anode Blended anode Carbon nanotubes carboxymethyl cellulose Conductive binder network

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Efficient remediation of different concentrations of Cr-contaminated soils by nano zero-valent iron modified with carboxymethyl cellulose and biochar

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Journal of Environmental Sciences 2025年第1期147卷 474-486页

作者： Lihong Xie Qiyan Ma Qingjun Chen Yiyang Liu Pengfei Guo Jinlan Zhang Guilan Duan Aijun Lin Tingting Zhang Shangyi Li Department of Environmental Science and Engineering College of Chemical EngineeringBeijing University of Chemical TechnologyBeijing 100029China China National Petroleum and Chemical Planning Institute Beijing 100013China State Key Laboratory of Urban and Regional Ecology Research Center for Eco-Environmental SciencesChinese Academy of SciencesBeijing 100085China

Nano zero-valent iron(nZVI)is widely used in soil remediation due to its high ***,the easy agglomeration,poor antioxidant ability and passivation layer of Fe-Cr coprecipitates of nZVI have limited its application scale in Cr-contaminated soil remediation,especially in high concentration of Cr-contaminated ***,we found that the carboxymethyl cellulose on nZVI particles could increase the zeta potential value of soil and change the phase of *** with the presence of biochar,97.0%and 96.6%Cr immobilization efficiency through CMC-nZVI/BC were respectively achieved in high and low concentrations of Cr-contaminated soils after 90-days *** addition,the immobilization efficiency of Cr(VI)only decreased by 5.1%through CMC-nZVI/BC treatment after 10 weeks aging in air,attributing to the strong antioxidation *** for the surrounding Crcontaminated groundwater,the Cr(VI)removal capacity of CMC-nZVI/BC was evaluated under different reaction conditions through column experiments and COMSOL ***-nZVI/BC could efficiently remove 85%of Cr(VI)in about 400 hr when the initial Cr(VI)concentration was 40 mg/L and the flow rate was 0.5 mL/*** study demonstrates that uniformly dispersed CMC-nZVI/BC has an excellent remediation effect on different concentrations of Cr-contaminated soils.

关键词： carboxymethyl cellulose Nanoscale zero-valent iron Biochar Cr-contaminated soils

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Dyes adsorption using a synthetic carboxymethyl cellulose-acrylic acid adsorbent

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Journal of Environmental Sciences 2014年第5期26卷 1203-1211页

作者： Genlin Zhang Lijuan Yi Hui Deng Ping Sun School of Chemistry and Chemical Engineering Key Laboratory for Green Processing of Chemical Engineering of Xinjiang Bingtuan Shihezi University

Removal of noxious dyes is gaining public and technological attention. Herein grafting polymerization was employed to produce a novel adsorbent using acrylic acid and carboxymethyl cellulose for dye removal. Scanning electron microscopy and Fourier-transform infrared spectroscopy verified the adsorbent formed under optimized reaction conditions. The removal ratio of adsorbent to Methyl Orange, Disperse Blue 2BLN and malachite green chloride reached to 84.2%, 79.6% and 99.9%, respectively. The greater agreement between the calculated and experimental results suggested that pseudo second-order kinetic model better represents the kinetic adsorption data. Equilibrium adsorptions of dyes were better explained by the Temkin isotherm. The results implied that this new cellulose-based absorbent had the universaiity for removal of dyes through the chemical adsorption mechanism.

关键词： adsorption dye grafting polymerization carboxymethyl cellulose acrylic acid

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Effect of carboxymethyl cellulose(CMC) Functionalization on Dispersion, Mechanical, and Corrosion Properties of CNT/Epoxy Nanocomposites

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Chinese Journal of Polymer Science 2023年第8期41卷 1277-1286,I0010页

作者： Da-Wei Zhang Leonard Chia Ying Huang Department of Civil Construction and Environmental EngineeringNorth Dakota State UniversityFargo 58108USA

Carbon nanotube(CNT)/epoxy nanocomposites have a great potential of possessing many advanced ***,the homogenization of CNT dispersion is still a great challenge in the research field of *** study applied a novel dispersion agent,carboxymethyl cellulose(CMC),to functionalize CNTs and improve CNT dispersion in *** effectiveness of the CMC functionalization was compared with mechanical mixing and a commonly used surfactant,sodium dodecylbenzene sulfonate(Na DDBS),regarding dispersion,mechanical and corrosion properties of CNT/epoxy nanocomposites with three different CNT concentrations(0.1%,0.3%and 0.5%).The experimental results of Raman spectroscopy,particle size analysis and transmission electron microscopy showed that CMC functionalized CNTs reduced CNT cluster sizes more efficiently than Na DDBS functionalized and mechanically mixed CNTs,indicating a better CNT *** peak particle size of CMC functionalized CNTs reduced as much as 54%(0.1%CNT concentration)and 16%(0.3%CNT concentration),compared to mechanical mixed and Na DDBS functionalized *** of the better dispersion,it was found by compressive tests that CNT/epoxy nanocomposites with CMC functionalization resulted in 189%and 66%higher compressive strength,224%and 50%higher modulus of elasticity than those with mechanical mixing and Na DDBS functionalization respectively(0.1%CNT cencentration).In addition,electrochemical corrosion tests also showed that CNT/epoxy nanocomposites with CMC functionalization achieved lowest corrosion rate(0.214 mpy),the highest corrosion resistance(201.031Ω·cm^(2)),and the lowest porosity density(0.011%).

关键词： CNT/epoxy composites carboxymethyl cellulose Dispersion Mechanical properties Corrosion properties

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Synthesis and characterization of carboxymethyl cellulose/organic montmorillonite nanocomposites and its adsorption behavior for Congo Red dye

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Water Science and Engineering 2013年第3期6卷 272-282页

作者： Min-min WANG Li WANG College of Material Science and Art Design Inner Mongolia Agricultural University

A series of carboxymethyl cellulose/organic montmorillonite （CMC/OMMT） nanocomposites with different weight ratios of carboxymethyl cellulose （CMC） to organic montmorillonite （OMMT） were synthesized under different conditions. The nanocomposites were characterized by the Fourier transform infrared （FT-IR） spectrophotometer, X-ray diffraction （XRD） method, transmission electron microscope （TEM）, scanning electron microscope （SEM）, and thermal gravimetric （TG） analysis. The results showed that the introduction of CMC may have different influences on the physico-chemical properties of OMMT and intercalated-exfoliated nanostructures were formed in the nanocomposites. The effects of different reaction conditions on the adsorption capacity of samples for Congo Red （CR） dye were investigated by controlling the amount ofhexadecyl trimethyl ammonium bromide （CTAB）, the weight ratio of CMC to OMMT, the reaction time, and the reaction temperature. Results from the adsorption experiment showed that the adsorption capacity of the nanocomposites can reach 171.37 rag/g, with the amount of CTAB being 1.0 cation exchange capacity （CEC） of MMT, the weight ratio of CMC to OMMT being l：l, the reaction time being 6 h, and the reaction temperature being 60~C. The CMC/OMMT nanocomposite can be used as a potential adsorbent to remove CR dye from an aqueous solution.

关键词： carboxymethyl cellulose organic montmorillonite nanocomposite adsorption,Congo Red dye

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Characterization of carboxymethyl cellulose Made from Bamboo Harvesting Residues

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Journal of Renewable Materials 2022年第12期10卷 3229-3241页

作者： Shuangyan Zhang Shun Yang Chuangui Wang Weiyi Su Huangfei Lv Yuanyuan Li School of Forestry and Landscape Architecture Anhui Agricultural UniversityHefei230036China

Bamboo harvesting residues are wastes by-products of bamboo industries that contain holocellulose for about 63.14%to 70.71%,which often be discarded,incinerated or *** this study,carboxymethyl cellulose was prepared from bamboo harvesting residues(bamboo-branch and bamboo-tip)as raw *** chemical composition of bamboo harvesting residues,the viscosity and degree of substitution of carboxymethyl cellulose were *** cellulose obtained was further characterized and compared by means of FTIR,SEM,XRD and *** showed that under the optimized identical conditions,the viscosity and degree of substitution of carboxymethyl cellulose from bamboo-branch and bamboo-tip were 6.0 and 78.9 mPa·s,0.75 and 0.89,*** cellulose obtained from bamboo-tip displayed a lower crystallinity and a better thermal stability as compared to synthetic carboxymethyl cellulose obtained from bamboo-branch and bamboo-culm.

关键词： Bamboo harvesting residues bamboo-branch bamboo-tip carboxymethyl cellulose characterization

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EFFECT OF METAL IONIC SPECIES AT MINERAL SURFACES ON THE ADSORPTION OF carboxymethyl cellulose

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Journal of Wuhan University of Technology(Materials Science) 1994年第1期9卷 118-124页

作者：曾宪滨邓小莉刘奇 Wuhan Univ of Tech. China

In this research it was shown that mineral surface metal-lic sites played a decisive role in carboxymethyl cellulose (CMC) adsorp-tion, and surface hydrophobicity alone did not have significant effects. Both the carboxymethyl groups and the hydroxyl groups of the CMC par-ticipated in the interaction with mineral surface, with the carboxymethyl groups interacting with metal and metal hydroxyl species, and hydroxyl groups interacting with metal hydroxide species, respectively.

关键词： carboxymethyl cellulose mechanisms of adsorption polysaccharide

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Characterization of synbiotic films based on carboxymethyl cellulose/β-glucan and development of a shelf life prediction model

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Food Bioscience 2023年第1期51卷 762-772页

作者： Sahar Seyedzadeh-Hashemi Vahid Mofid Seyede Marzieh Hosseini Seyed Mohammad Taghi Gharibzahedi Amir Mohammad Mortazavian Saeedeh Shojaee-Aliabadi Department of Food Science and Technology Faculty of Nutrition Sciences and Food TechnologyNational Nutrition and Food Technology Research InstituteShahid Beheshti University of Medical SciencesTehranIran Institute of Materials Science Faculty of EngineeringKiel University24143KielGermany Institute of Chemistry Technische Universitat BerlinStraße des 17.Juni 12410623BerlinGermany

carboxymethyl cellulose(CMC)/β-glucan(BG)-based films(100:0,75:25,50:50,25:75)were developed and characterized to extend the survivability of Lactobacillus acidophilus LA-5 and establish a shelf life prediction *** incorporation of inulin(IL,2%and 4%)into the CMC matrix was also *** containing 2%IL and 50%BG were selected to develop probiotic films due to their suitable physicomechanical and barrier ***-transform infrared(FT-IR)spectroscopy spectra and scanning electron microscopy(SEM)images showed good compatibility between prebiotics and CMC films *** tensile strength and water vapor permeability(WVP)of films reduced by prebiotics addition,their oxygen barrier and extensibility were significantly *** viability of probiotic cells was observed in film containing BG;at 4℃(8.3 Log CFU/g),10℃(8.06 Log CFU/g)and 25℃(7.37 Log CFU/g),and under simulated gastrointestinal conditions(7.87 Log CFU/g).This new edible film would be inspiring for future bioactive-loaded packaging.

关键词： Biodegradable film carboxymethyl cellulose β-glucan Inulin Probiotic viability Shelf life prediction Simulated digestion

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Screening the synergy of sodium dodecylbenzenesulfonate and carboxymethyl cellulose for surfactant-polymer flooding

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Petroleum Research 2022年第3期7卷 308-317页

作者： Suriatie Mat Yusuf Radzuan Junin Mohd Akhmal Muhamad Sidek Augustine Agi Mohd Fazril Irfan Ahmad Fuad Nor Roslina Rosli Norazah Abd Rahman Effah Yahya Nor Adilah Muhamad Soffian Wong Muhammad Hazim Mustaza Department of Petroleum Engineering School of Chemical and Energy EngineeringFaculty of EngineeringUniversiti Teknologi Malaysia81310Johor BahruMalaysia Institute for Oil and Gas Universiti Teknologi Malaysia81310Johor BahruMalaysia School of Chemical Engineering College of EngineeringUniversiti Teknologi MARA40450Shah AlamSelangorMalaysia

carboxymethyl cellulose(CMC)has emerged in oil and gas industries as a superior substitution to the conventional HPAM and xanthan gum(XG)for high viscosity polymer flooding *** this study,the combined effect of conventional surfactant,sodium dodecylbenzenesulfonate(SDBS)and CMC for potential surfactant-polymer(SP)flooding in enhanced oil recovery(EOR)has been ***,SDBS–CMC interaction and the functional groups present in CMC were appropriately *** presence of various C–O bonds signifies the existence of carboxymethyl group which greatly influence the rheological properties of CMC *** behaviour of SDBS–CMC was characterized by their viscosity,shear rate,solubilization,wettability,and surface *** flooding utilizing SDBS-CMC was performed and compared to commercial SDBS-XG SP *** results indicate several SDBS-CMC combinations are favourable for EOR *** viscosity shows direct relationship with CMC ***,at any given SDBS concentrations,significant increment was observed at 0.3 wt%and ***,the trend displayed inconclusive relation to SDBS *** of the SDBS-CMC combinations generate Winsor III emulsions particularly at CMC of 0.2 and 0.3 wt%,while Type II were observed in few *** CMC concentrations increased the contact angle,while gradual reductions were observed with SDBS *** gradual reduction in surface tension was highly influenced by the addition of CMC rather than SDBS.A novel combination of 0.3 wt%SDBS and 0.4 wt%CMC possessed an encouraging criterion in term of viscosity,solubilization,and surface tension reduction for EOR *** experiment from several SDBS-CMC combinations proved to recover additional oil ranging 16.4–20.2%of oil initially in place(OIIP).The trend in incremental oil recovery is similar to that of when utilising SDBS-XG.

关键词： carboxymethyl cellulose Sodium dodecylbenzenesulfonate Enhanced oil recovery Surfactant-polymer flooding

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Absorption Capability Comparison of Two Kinds of Super Absorbent Resins from carboxymethyl cellulose

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Journal of Beijing Institute of Technology 2007年第1期16卷 98-102页

作者：李杰丁彩霞栾昌曲鹏飞马骊芳 School of Materials Science and Engineering Beijing Institute of Technology Beijing 100081China

The two kinds of super absorbent resins from carboxymethyl cellulose were synthesized with the potassium persulphate and methylenebisacrylamide as initiator and cross linker respectively by radical polymerization in aqueous solution. Thestructures of the two resins were characterized with Fourier transform infrared spectroscopy FTIR, scanning electron miscroscopy （SEM）, and environment scanning electron miscroscopy （ESEM）, the results indicate that the fibriform of the carboxymethyl cellulose （CMC） is disappeared and the crusslink networks in eopolymer of carboxymethyl cellulose-graft-polyacrylic acid（CMC-g-PAA） are denser than that of eopolymer of carboxymethyl cellulose-graft-poly （acrylic acid-co-N-vinyl Pyrrolidone）（CMC-g- PAA-co-PVP）. The comparison between the two resins in absorption capacities is that CMC-g-PAA is better in the water-keep capability being heated, while CMC-g-PAA-co-PVP is better in the water absorbency and salt resistance.

关键词： super absorbent resin carboxymethyl cellulose acrylic acid N-vinyl pyrrolidone absorption capability

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