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Remote synthesis of Layered Double Hydroxide Nanosheets Through the automatic Chemical Robot

Chemical Research in Chinese Universities 2022年第1期38卷 217-222页

作者： WANG Zelin LIU Guihao SHEN Tianyang TAN Ling ZHAO Yufei SONG Yu-Fei CNPC Research Institute of Safety and Environmental Technology Beijing 102206P.R.China State Key Laboratory of Chemical Resource Engineering Beijing University of Chemical TechnologyBeijing 100029P.R.China Beijing Advanced Innovation Center for Soft Matter Science and Engineering Beijing University of Chemical TechnologyBeijing 100029P.R.China

As a family of two-dimensional functional materials, layered double hydroxides(LDHs) have the characteristics of adjustable lamellar element type and proportion, variable interlamellar anion, controllable particle size and thickness, providing a robust platform for photo/electro/thermal-catalysis. With the continuous progress of materials science, the synthesis of LDHs is becoming more and more refined. Herein, to achieve the fine preparation of LDHs materials, especailly for the no-chemical/material researchers, we successfully assembled the automatic synthesis device and wrote corresponding computer software to control this device, and the automatic synthesis of bulk and monolayer LDHs nanosheets on a laboratory scale can be realized. This work paves a new labor-saving way for the fine synthesis of LDHs nanostructures, further improving the development of LDHs-based materials.

关键词： Layered double hydroxide automatic synthesis Monolayer Single-atom catalyst

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Automated and remote synthesis of poly(ethylene glycol)-mineralized ZIF-8 composite particles via a synthesizer assisted by femtosecond laser micromachining

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Chinese Chemical Letters 2022年第1期33卷 497-500页

作者： Miao Wu Lingling Xia Yucen Li Difeng Yin Jianping Yu Wenbo Li Ning Wang Xin Li Jiwei Cui Wei Chu Ya Cheng Ming Hu School of Physics and Electronic Science East China Normal UniversityShanghai 200241China State Key Laboratory of Precision Spectroscopy School of Physics and Electronic ScienceEast China Normal UniversityShanghai 200241 China XXL–The Extreme Optoelectromechanics Laboratory School of Physics and Electronic ScienceEast China Normal UniversityShanghai 200241 China State Key Laboratory of High Field Laser Physics and CAS Center for Excellence in Ultra-intense Laser Science Shanghai Institute of Optics and Fine Mechanics(SIOM)Chinese Academy of Sciences(CAS)Shanghai 201800China University of Chinese Academy of Sciences Beijing 100049China Key Laboratory of Colloid and Interface Chemistry of the Ministry of Education School of Chemistry and Chemical EngineeringShandong UniversityJi'nan 250100China

Mineralization of the ZIF-8 in the presence of biomacromolecules has been demonstrated to be a general way for making bioentities@ZIFs *** ZIF-8 crystals permit controlled storage and utilization of the bioentities,thus can benefit drug delivery,cold-chain breaking *** the increasing needs on personal care and distributed manufacturing,automated synthesis controlled by a computer becomes the next *** this work,we designed an automatic synthesis system to prepare PEG mineralized ZIF-8 composite *** system is based on flow chemistry with the microfluidic chips fabricated by femtosecond laser *** particles were synthesized and monitored ***,this synthesizer could be extended for fabrication of vaccine particles under remote control through internet.

关键词： ZIF-8 automatic synthesis Remote synthesis MOFs Vaccine particles Microfluidic chip Flow chemistry

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