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Process optimization of an industrial acetic acid dehydration progress via heterogeneous azeotropic distillation

Chinese Journal of Chemical Engineering 2018年第8期26卷 1631-1643页

作者： Xiuhui Huang Zeqiu Li Ying Tian School of Energy and Power Engineering University of Shanghai for Science and Technology School of Optical-Electrical and Computer Engineering University of Shanghai for Science and Technology

The simulated process model of the HAc dehydration process under actual overloaded condition was conducted by amending the model of standard condition in our previous work using the process data collected from actual production. Based on the actual process model, the operation optimization analysis of each plant(HAc dehydration column, decanter and NPA recycle column) was conducted using Residue Curve Maps(RCMs),sensitivity analysis and software optimization module. Based on the optimized parameters, the influence of feed impurity MA and the temperature of decanter on the separating effect and energy consumption of the whole process were analyzed. Then the whole process operation optimizing strategy was proposed with the objective that the total reboiler duty Q Total of C-1 and C-3 reaches the minimum value, keeping C-1 and C-3 at their optimized separation parameters obtained above, connecting all the broken recycle and connection streams, and using the temperature of D-1 as operation variable. The optimization result shows that the total reboiler duty Q Total of the whole process can reach the minimum value of 128.32 × 10~6 k J·h^(-1) when the temperature of decanter is 352.35 K, and it can save 5.94 × 10~6 k J·h^(-1), about 2.56 t·h^(-1) low-pressure saturated vapor.

关键词： acetic acid dehydration Azeotropic distillation Process simulation Operation optimization

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Simulation and Analysis on Multiple Steady States of an Industrial acetic acid dehydration System

引用

Chinese Journal of Chemical Engineering 2011年第6期19卷 983-989页

作者：李绍军黄定伟 Key Laboratory of Advanced Control and Optimization for Chemical Processes （East China University of Science and Technology） Ministry of Education Shanghai 200237 China

In this work, an industrial acetic acid dehydration system via heterogeneous azeotropic distillation is simulated by Aspen Plus software. Residue curves are used to analyze the distillating behavior, and appropriate operating region of the system is determined. Based on steady states simulation, a sensitivity analysis is carried out to detect the output multiple steady states in the system. Different solution branches are observered when the flow rates of the feed stream and the organic reflux stream are selected as manipulated variables. The performance of the column under different steady states is different. A method is oroposed to achieve the desired steady state.

关键词： acetic acid dehydration heterogeneous azeotropic distillation residue curve multiple-steady states

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