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Influence of γ' precipitate on deformation and fracture during creep in PM nickel-based superalloy

Progress in Natural Science:Materials International 2021年第2期31卷 303-309页

作者： Zichao Peng Jinwen Zou Jie Yang Gaofeng Tian Xuqing Wang Science and Technology on Advanced High Temperature Structural Materials Laboratory Beijing Institute of Aeronautical MaterialsAECC

FGH96 is a powder metallurgy nickel based superally used for turbine disk of aero-engines. In the present study FGH96 alloy with four different γ’ precipitate microstructures were produced via solution heat-treatment with different cooling rates, and the maximum cooling rate reached 400°C/min which was a super cooling rate for Nickel-based superalloy. The creep tests were conducted for PM FGH96 alloy under the testing condition of 704°C and 690 MPa. The relationship between the creep properties and the distribution of γ’ precipitate was established. The creep mechanism was analyzed by using TEM and ACTEM, and the dislocation movement was studied at the atomic scale. The creep strain rate was calculated through a physically based crystal slip model established based on crystal plasticity. The calculated results were consistent with the test ones, illustrating the validity of the model. The fracture mechanism was also investigated, and the results showed that the creep cracks generated on the surface due to the oxidation. It was observed that the cracks propagated in different ways depending on the different average diameters of γ’ precipitate. With the decrease of the average γ’ precipitate size,the critical shearing stress increased and the resistance of the dislocation slipping increased. The fracture mechanism for the primary stage transformed from intragranular to intergranular due to the change of dislocation slipping.

关键词： PM FGH96 superalloy Microtwinning γ′ precipitate Fracture mechanism Physically-based creep model

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Heat Treatment of a Candidate Material for 700 ℃ A-USC Power Plants

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Journal of Iron and Steel Research(International) 2015年第2期22卷 150-156页

作者： Yan CHONG Zheng-dong LIU Andy GODFREY Lu WANG Wei LIU Yu-qing WENG School of Materials Science and Engineering Tsinghua University Central Iron and Steel Research Institute

The preliminary chemical composition optimization and heat treatment parameters of Inconel 740H were investigated systematically. Six heats of experimental alloys （designated as heat 401 to heat 406） with varied chemi- cal compositions were subjected to standard heat treatment at four different solution temperatures. Due to its superi- or combination of strength, ductility, and toughness together with its minor mechanical property changes at different solution temperatures, heat 405 was chosen as an optimized one to conduct further heat treatment investigations. The evolution of grain size with solution temperature for heat 405 was studied and the optimal solution temperature was determined. After solution treatment at the optimal temperature, four different cooling rates were applied to investi- gate the effect of cooling rate on the size distribution modal and mean radius of the γ′ precipitates. No bi-modal size distribution of γ′ precipitates was found for all cooling rates and water cooling was recommended for Inconel 740H. In addition, the effect of pre-aging at 800 ℃ for 16 h on the microstrueture of Inconel 740H aged for a long time was studied. It is found that pre-aging at 800 ℃ would result in bi-modal size distribution of γ′ precipitates after long time aging at 750 ℃ compared with mono modal size distribution in samples without pre-aging, which might be caused by the difference in initial size distribution modal before Ostwald ripening of γ′ precipitates in samples with and without pre-aging at 800 ℃.

关键词： Inconel 740H heat treatment grain size γ′ precipitate mechanical property

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