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Importance of oxygen-containing functionalities and pore structures of biochar in catalyzing pyrolysis of homologous poplar

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Chinese Journal of Chemical Engineering 2024年第1期65卷 200-211页

作者： Li Qiu Chao Li Shu Zhang Shuang Wang Bin Li Zhenhua Cui Yonggui Tang Obid Tursunov Xun Hu School of Material Science and Engineering University of JinanJinan 250022China Joint International Research Laboratory of Biomass Energy and Materials College of Materials Science and EngineeringNanjing Forestry UniversityNanjing 210037China School of Energy and Power Engineering Jiangsu UniversityZhenjiang 212013China shandong BASAN Graphite New Material Plant Zibo 255311China Department of Power Supply and Renewable Energy Sources National Research University TIIAMETashkent 100000Uzbekistan

Biochar and bio-oil are produced simultaneously in one pyrolysis process,and they inevitably contact and may interact,influencing the composition of bio-oil and modifying the structure of *** this sense,biochar is an inherent catalyst for *** this study,in order to investigate the influence of functionalities and pore structures of biochar on its capability for catalyzing the conversion of homologous volatiles in bio-oil,three char catalysts(600C,800C,and 800AC)produced via pyrolysis of poplar wood at 600 or 800℃or activated at 800℃,were used for catalyzing pyrolysis of homologous poplar wood at 600℃,*** results indicated that the 600C catalyst was more active than 800C and 800AC for catalyzing cracking of volatiles to form more gas(yield increase by 40.2%)and aromatization of volatiles to form more light or heavy phenolics,due to its abundant oxygen-containing functionalities acting as active *** developed pores of the 800AC showed no such catalytic effect but could trap some volatiles and allow their further conversion via sufficient ***,the interaction with the volatiles consumed oxygen on 600C(decrease by 50%),enhancing the aromatic degree and increasing thermal *** dominance of deposition of carbonaceous material of a very aromatic nature over 800C and 800AC resulted in net weight gain and blocked micropores but formed additional *** in situ diffuse reflectance infrared Fourier transform spectroscopy characterization of the catalytic pyrolysis indicated superior activity of 600C for removal of -OH,while conversion of the intermediates bearing C=O was enhanced over all the char catalysts.

关键词： Poplar wood Catalytic pyrolysis Char catalyst Volatile-char interaction Bio-oil

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Global adaptive output-feedback tracking with prescribed performance for uncertain nonlinear systems

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Science China(Information Sciences) 2024年第5期67卷 150-164页

作者： Yuan WANG Yungang LIU School of Control Science and Engineering Shandong University

At present, one typical control strategy for guaranteeing transient and steady-state performance is funnel control and prescribed performance control. The strategy features completely discarding the system nonlinearities, even if they are completely known and available. Such an intrinsic feature requires the controller to produce a larger control effect to eliminate the negative impact caused by the high nonlinearities, leading to a conservative controller. In this paper, we fully take advantage of known information on nonlinearities in control design, instead of completely discarding it as done in funnel control. Particularly, we leverage adaptive techniques(i.e., high-gain dynamic compensation) to deal with unknown system nonlinearities. Meanwhile, we integrate the tools of output feedback, tracking control, and the performance *** such, an adaptive output-feedback scheme is developed for global tracking with spatiotemporal performance specifications: arbitrarily given tracking accuracy and accuracy-ensured time. A simulation example supports the developed approach.

关键词： uncertain nonlinear systems output feedback prescribed performance unknown control direction dynamic high gain global tracking

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TBBPA rather than its main derivatives enhanced growth of endometrial cancer via p53 ubiquitination

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Journal of Environmental Sciences 2024年第3期137卷 82-95页

作者： Hongyan Yu Jingxu Zhang Jing Liu Ruonan Pan Yu Wang Xiaoting Jin Rifat Zubair Ahmed Yuxin Zheng Department of Occupational Health and Environmental Health School of Public HealthQingdao UniversityQingdao 266071China State Key Laboratory of Environmental Chemistry and Ecotoxicology Research Center for Eco-Environmental SciencesChinese Academy of SciencesBeijing 100085China Department of Genetics University of KarachiKarachi 75270Pakistan

Tetrabromobisphenol A(TBBPA)and its derivatives widely exist in various environments and *** the available data indicate that TBBPA exposure is highly associated with the increased incidence of endometrial cancer(EC),the effects of TBBPA and its main derivatives on EC proliferation and the involved crucial mechanism remain *** present study aimed to investigate the effects of TBBPA and its derivatives under environmental concentrations on the proliferation of EC,and the crucial mechanism on the progression of EC caused by bromine fame retardants *** this research,TBBPA and two of the most common TBBPA derivatives including TBBPA bis(2-hydroxyethyl ether)(TBBPABHEE)and TBBPA bis(dibromopropyl ether)(TBBPA-BDBPE)were screened for their capacities in induced EC proliferation and explored the related mechanism by in vitro cell culture model and in vivo mice *** environmental concentrations,TBBPA promoted the proliferation of EC,the main derivatives of TBBPA(TBBPA-BHEE and TBBPA-BDBPE)did not present the similar facilitation *** ubiquitination degradation of p53 was crucial in TBBPA induced EC proliferation,which resulted in the increase of downstream cell cycle and decrease of *** further molecular docking result suggested the high affinity between TBBPA and ubiquitinated *** finding revealed the effects of TBBPA and its derivatives on EC proliferation,thus providing novel insights into the underlying mechanisms of TBBPA-caused EC.

关键词： Tetrabromobisphenol A(TBBPA) Endometrial cancer(EC) Derivatives Ubiquitin proteases p53

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Hydrodynamic analysis of carbon nanotube clusters in distributor-less conical fluidized beds with step-by-step scaling

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Chinese Journal of Chemical Engineering 2024年第3期67卷 117-125页

作者： Tianle Zhang Wenjuan Bai Qianpeng Dong Dianming Chu Lianlian Wang Yan He shandong Engineering Laboratory for Preparation and Application of High-performance Carbon-Materials College of Electromechanical EngineeringQingdao University of Science and TechnologyQingdao 266061China shandong Dazhan Nano Materials Co. Ltd.Binzhou 256220China

As a high-performance material with great application potential,the application of carbon nanotubes has been limited by their production volume.A distributor-less conical fluidized bed is the main equipment used in the industrial production of carbon *** improve the production volume and product quality of carbon nanotubes,the study of fluidized-bed-diameter scaling is *** different diameters of distributor-less conical fluidized beds were established,and then the particle behavior and bubble characteristics of carbon nanotube clusters at these bed diameters were ***-series and wavelet analysis methods were used to analyze the pressure-fluctuation signals inside the fluidized *** showed that the distributor-less design caused the airflow to break through the middle of the bed,which did not change with the change in bed *** powder-bridging phenomenon of carbon nanotube clusters in a 100-mm-diameter fluidized bed was related to the special microstructure of carbon nanotube *** frequency of pressure fluctuations in the bed decreased nonlinearly with increasing bed *** study can guide the design and scale-up of distributor-less conical fluidized beds,especially for the scale-up of carbon nanotube production equipment,which can contribute to the improvement of carbon nanotubes’capacity and quality in industrial production.

关键词： Carbon nanotubes Fluidized bed Multiphase flow Scale-up Multiscale

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Enhanced Temporal Correlation for Universal Lesion Detection

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Computer Modeling in Engineering & Sciences 2024年第3期138卷 3051-3063页

作者： Muwei Jian Yue Jin Hui Yu School of Computer Science and Technology Shandong University of Finance and EconomicsJinanChina School of Information Science and Technology Linyi UniversityLinyiChina School of Creative Technologies University of PortsmouthPortsmouthUK

Universal lesion detection(ULD)methods for computed tomography(CT)images play a vital role in the modern clinical medicine and intelligent *** is well known that single 2D CT slices lack spatial-temporal characteristics and contextual information compared to 3D CT ***,3D CT blocks necessitate significantly higher hardware resources during the learning ***,efficiently exploiting temporal correlation and spatial-temporal features of 2D CT slices is crucial for ULD *** this paper,we propose a ULD network with the enhanced temporal correlation for this purpose,named *** designed TCE module is applied to enrich the discriminate feature representation of multiple sequential CT ***,we employ multi-scale feature maps to facilitate the localization and detection of lesions in various *** experiments are conducted on the DeepLesion benchmark demonstrate that thismethod achieves 66.84%and 78.18%for FS@0.5 and FS@1.0,respectively,outperforming compared state-of-the-art methods.

关键词： Universal lesion detection computational biology medical computing deep learning enhanced temporal correlation

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Effect of solution treatment on the microstructure,phase transformation behavior and functional properties of NiTiNb ternary shape memory alloys fabricated via laser powder bed fusion in-situ alloying

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International Journal of Extreme Manufacturing 2024年第4期6卷 202-223页

作者： Rui Xi Hao Jiang Guichuan Li Zhihui Zhang Huiliang Wei Guoqun Zhao Jan Van Humbeeck Xiebin Wang Key Laboratory for Liquid-Solid Structural Evolution and Processing of Materials(Ministry of Education) Shandong UniversityJingshi Road 17923Jinan 250061People's Republic of China Department of Materials Engineering University of Leuven(KU Leuven)Kasteelpark Arenberg 44 bus 2450Heverlee B3001Belgium Key Laboratory of Bionic Engineering(Ministry of Education) Jilin UniversityRenmin Street 5988Changchun 130025People's Republic of China School of Mechanical Engineering Nanjing University of Science and TechnologyXiaolingwei Street 200Nanjing 210094People's Republic of China

Post-heat treatment is commonly employed to improve the microstructural homogeneity and enhance the mechanical performances of the additively manufactured metallic *** this work,a ternary(NiTi)91Nb9(at.%)shape memory alloy was produced by laser powder bed fusion(L-PBF)using pre-alloyed NiTi and elemental Nb *** effect of solution treatment on the microstructure,phase transformation behavior and mechanical/functional performances was *** in-situ alloyed(NiTi)91Nb9 alloy exhibits a submicron cellular-dendritic structure surrounding the supersaturated B2-NiTi *** high-temperature(1273 K)solution treatment,Nb-rich precipitates were precipitated from the supersaturated *** fragmentation and spheroidization of the NiTi/Nb eutectics occurred during solution treatment,leading to a morphological transition from mesh-like into rod-like and *** of theβ-Nb phases occurred with increasing holding *** martensite transformation temperature increases after solution treatment,mainly attributed to:(i)reduced lattice distortion due to the Nb expulsion from the supersaturated B2-NiTi,and(ii)the Ti expulsion from theβ-Nb phases that lowers the ratio Ni/Ti in the B2-NiTi matrix,which resulted from the microstructure changes from non-equilibrium to equilibrium *** thermal hysteresis of the solutionized alloys is around 145 K after 20%pre-deformation,which is comparable to the conventional NiTiNb alloys.A short-term solution treatment(*** 1273 K for 30 min)enhances the ductility and strength of the as-printed specimen,with the increase of fracture stress from(613±19)MPa to(781±20)MPa and the increase of fracture strain from(7.6±0.1)%to(9.5±0.4)%.Both the as-printed and solutionized samples exhibit good tensile shape memory effects with recovery rates>90%.This work suggests that post-process heat treatment is essential to optimize the microstructure and improve the mechanical performances of the L-PBF in-situ allo

关键词： shape memory alloy NiTiNb laser powder bed fusion in-situ alloying heat treatment

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Mechanism Exploration of Euphorbia fischeriana Steud. for Liver Cancer Based on Aspartic Acid Identification in Metabolomics

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Chinese Journal of Integrative Medicine 2024年第6期30卷 507-514页

作者： ZHAO Jing TIAN Xin-chen ZHANG Jia-qi HUANG Chen SUN Yan QIAO Sen JIANG Shu-long Clinical Medical Laboratory Center Jining First People’s HospitalJiningShandong Province272000China Cheeloo College of Medicine Shandong UniversityJinan250000China

Objective:To investigate the anti-liver cancer effects and aspartic acid(Asp)-related action mechanism of Euphorbia fischeriana Steud.(LD).Methods:The mice model of liver cancer was established by injection of H22 *** 5 days,mice were randomly divided into model group,sorafenib group(20 mg/kg),LD high-dose(LDH,1.36 g/kg) group,LD medium-dose(LDM,0.68 g/kg) group,and LD low-dose(LDL,0.34 g/kg)group,10 mice each *** were intragastrically administered to the mice once daily for 10 days,*** weight,tumor size and tumor weight were *** index was *** changes of liver cancer tissues were evaluated by hematoxylin and eosin staining and TUNEL *** chromatography-mass spectrometer was used to analyze different metabolites between the model and LDH ***:After LD treatment,tumor weight,tumor size and hepatic index were reduced compared with the model *** and karyorrhexis of tumor cells were ***,61 differential metabolites(18 up-regulated,43 down-regulated) were affirmed and 20 pathways of KEGG(P<0.05) were *** addition,Bel-7402,HepG2 and H22 cell viabilities were significantly increased after adding Asp into the *** then,the cell proliferation effect induced by Asp was ameliorated by ***:The anti-liver cancer efficacy of LD extract was validated in H22 mice model,and inhibition of Asp level might be the underlying mechanism.

关键词： liver cancer Euphorbia fischeriana Steud. aspartic acid metabolomics

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In situ embedded bismuth nanoparticles among highly porous carbon fibers for efficient carbon dioxide reduction

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Rare Metals 2024年第9期43卷 4312-4320页

作者： Wei-Jian Guo Ao Zhou Wen-Wen Cai Jin-Tao Zhang Key Laboratory for Colloid and Interface Chemistry (Ministry of Education) School of Chemistry and Chemical EngineeringShandong University

Electrocatalysis provides an optimal approach for the conversion of carbon dioxide(CO2) into high-value chemicals, thereby presenting a promising avenue toward achieve carbon neutrality. However, addressing the selectivity and stability challenges of metal catalysts in electrolytic reduction remains a daunting task. In this study, the electrospinning method is employed to fabricate porous carbon nanofibers loaded with bismuth nanoparticles with the help of in situ pyrolysis. The porous carbon nanofibers as conductive support would facilitate the dispersion of bismuth active sites while inhibiting their aggregation and promoting the mass transfer, thus enhancing their electrocatalytic activity and stability. Additionally, nitrogen doping induces electron delocalization in bismuth atoms through metal-support interactions, thus enabling efficient adsorption of intermediates for improving selectivity based on the theoretical calculation. Consequently, Bi@PCNF-500 exhibits the exceptional selectivity and stability across a wide range of potential windows. Notably, its faradaic efficiency(FE) of formate reaches 92.7% in H-cell and94.9% in flow cell, respectively, with good electrocatalytic stability. The in situ characterization and theoretical calculations elucidate the plausible reaction mechanism to obtain basic rules for designing efficient electrocatalyst.

关键词： Carbon dioxide reduction Electron delocalization N-doping Porous carbon nanofiber

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Overview of enhancing biological treatment of coal chemical wastewater:New strategies and future directions

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Journal of Environmental Sciences 2024年第1期135卷 506-520页

作者： Weiwei Ma Xiaoqi Zhang Hongjun Han Xueqing Shi Qiaoping Kong Tong Yu Fei Zhao School of Environmental and Municipal Engineering Qingdao University of TechnologyQingdao 266520China State Key Laboratory of Urban Water Resource and Environment Harbin Institute of TechnologyHarbin 150090China

Coal chemical wastewater(CCW)is a type of refractory industrial wastewater,and its treatment has become the main bottleneck restricting the sustainable development of novel coal chemical *** treatment is considered as an economical,effective and environmentally friendly technology for CCW ***,conventional biological process is difficult to achieve the efficient removal of refractory organics because of CCW with the characteristics of composition complexity and high ***,seeking the novel enhancement strategy appears to be a favorable solution for enhancing biological treatment efficiency of *** review focuses on presenting a comprehensive picture about the exogenous enhancement strategies for CCW biological *** performance and potential application of exogenous enhancement strategies,including co-metabolic substrate enhancement,biofilm filler enhancement,adsorption material enhancement and conductive mediator enhancement,were ***,the enhancing mechanisms of different strategies were comprehensively discussed from a biological ***,the prospects of enhancement strategies based on the engineering performance,economic cost and environmental impact(3E)evaluation were *** novel enhancement strategy based on“low carbon emissions”,“resource recycling”and“water environment security”in the context of carbon neutrality was *** together,this review provides technical reference and new direction to facilitate the regulation and optimization of typical industrial wastewater biological treatment.

关键词： Coal chemical wastewater Biological treatment Exogenous enhancement Refractory organics 3E evaluation

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Experimental Study on Consolidation Properties of Hydrate-Bearing Fine-Grained Sediments Collected from the Shenhu Area of the Northern South China Sea

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Journal of Ocean University of China 2024年第4期23卷 981-990页

作者： WEI Ruchun LIU Lele JIA Chao DONG Xiao BU Qingtao ZHANG Yongchao LIU Changling WU Nengyou School of Water Conservancy and Environment University of JinanJinan 250022China shandong Engineering Research Center of Marine Exploration and Conservation Ocean University of ChinaQingdao 266100China Key Laboratory of Gas Hydrate Ministry of Natural ResourcesQingdao Institute of Marine GeologyQingdao 266237China Institute of Marine Science and Technology Shandong UniversityQingdao 266232China

Mechanical properties of hydrate-bearing fine-grained sediments are crucial to effectively mitigate environmental risks caused by artificial and natural decomposition of natural gas hydrates,and the decomposition can induce laterally confined *** explore the effect of natural gas hydrates on laterally confined compression properties,consolidation tests are conducted on remolded hydrate-free and hydrate-bearing samples by using natural fine-grained sediments collected from the northern South China Sea as the host sediments,and empirical equations are developed based on the analyses of consolidation *** results show that vertical loading induces a reduction in void ratio,and the reduction increases with decreasing hydrate saturation when samples are subjected to the same vertical stress *** compression index of samples is about 0.53 whether there is hydrate or not,but the yield stress of samples increases sharply with increasing hydrate saturation once beyond the critical *** coefficient of volume compression and the coefficient of consolidation of hydrate-bearing samples both increase firstly and then decrease to a relative stable level with increasing vertical stress,and the transition occurs at 200 *** average consolidation degree with elapsed time increases rapidly under low vertical stresses,slowly under median vertical stresses,and under high vertical stresses,the consolidation increases a little faster but still slower than those under low vertical stresses.

关键词： natural gas hydrate stiffness compression index hydraulic permeability geohazard

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