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Microstructure evolution and shape memory behaviors of Ni_(47)Ti_(44)Nb_(9)alloy subjected to multistep thermomechanical loading with different prestrain levels

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Journal of Materials science & Technology 2024年第4期171卷 80-93页

作者： Y.H.Zhang H.Li Z.W.Yang X.Liu Q.F.Gu State Key Laboratory of Solidification Processing School of Materials Science and EngineeringNorthwestern Polytechnical UniversityXi’an 710072China Shaanxi Key Laboratory of High-Performance Precision Forming Technology and Equipment Northwestern Polytechnical UniversityXi’an 710072China

Ni_(47)Ti_(44)Nb_(9)shape memory alloy(SMA)is a promising material in the aerospace field due to its wide transformation *** application of shape memory effect depends on multistep thermomechan-ical loading,viz.,low-temperature deformation and subsequent heating to ***-temperature deformation prestrain plays a pivotal role in shape memory properties tailoring of SMA ***,microstructure evolution and deformation mechanisms of Ni_(47)Ti_(44)Nb_(9)SMA subjected to vari-ous prestrain levels are still *** this end,microstructure evolution and shape memory behaviors of Ni_(47)Ti_(44)Nb_(9)alloy subjected to multistep thermomechanical loading with prestrain levels of 8%-16%at-28℃(M_(s)+30℃)were *** results demonstrate that the stress-strain curve of the specimen exhibits four distinct stages at a maximal prestrain of 16%.Whereas stageⅡand stageⅢend at prestrains of∼8%and∼12%,*** stageⅡ,the stress-induced martensitic transformation is accompanied by the dislocation slip of the NiTi matrix andβ-Nb *** stageⅢ,in addition to the higher density of dislocations and further growth of stress-induced martensite variants(SIMVs),(001)compound twins are introduced as a result of the(001)deformation twinning in stress-induced ***{20-1}martensite twins are gradually introduced in stageⅣ.Correspondingly,after subsequent unloading and heating,a higher density of{114}austenite twins form in the specimen with a larger prestrain of 16%.With increasing prestrain from 8%to 16%,the recoverable strainε_(re)^(T)upon heating increases first and then ***ε_(re)^(T)obtains a maximum of 7.03%at 10%prestrain and de-creases to 6.17%at 16%*** increase ofε_(re)^(T)can be attributed to the formation of new SIMVs,the further growth of existing SIMVs,and the recoverable(001)compound *** the decrease ofε_(re)^(T)is mainly associated with the irrecoverable strain by{20−1}martensite *** effe

关键词： Ni_(47)Ti_(44)Nb_(9)shape memory alloy Wide transformation hysteresis Thermomechanical loading Microstructure evolution Shape memory behaviors Stress-induced martensitic transformation Deformation twinning

Numerical analysis on seismic response and failure mechanism of articulated pile−structure system in a liquefiable site from shaking-table experiments

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Frontiers of Structural and Civil Engineering 2024年第7期18卷 1117-1133页

作者： Pengfei DOU Hao LIU Chengshun XU Jinting WANG Yilong SUN Xiuli DU Department of Hydraulic Engineering Tsinghua UniversityBeijing 100084China Key Laboratory of Urban Security and Disaster Engineering of the Ministry of Education Beijing University of TechnologyBeijing 100124China

This study investigates the seismic response and failure mode of a pile-structure system in a liquefiable site by employing a numerical simulation model combined with the shaking-table results of a soil-pile-structure dynamic *** pile and soil responses obtained from the numerical simulations agreed well with the experimental *** slopes of the dynamic shear-stress-shear-strain hysteretic curves at different positions also exhibited a decreasing trend,indicating that the shear strength of the soil in all parts of the foundation *** peak acceleration of the soil and pile was not clearly amplified in the saturated sand layer but appeared to be amplified in the top *** maximum bending moments appeared in the middle and lower parts of the pile shaft;however,the shear forces at the corresponding positions were not *** can be observed from the deformation mode of the pile-group foundation that a typical bending failure is caused by an excessive bending moment in the middle of the pile shaft if the link between the pile top and cap is articulated,and sufficient attention should be paid to the bending failure in the middle of the pile shaft.

关键词： numerical simulation soil liquefaction pile foundation shaking-table experiment seismic responses failure model

Biophotoelectrochemistry for the treatment of emerging contaminants

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science China Technological sciences 2024年第10期67卷 3051-3066页

作者： HU Jing CHEN Man GU WenZhi DENG WenEr HONG MingQiu HU AnDong YE Jie ZHOU ShunGui Fujian Provincial Key Laboratory of Soil Environmental Health and Regulation College of Resources and EnvironmentFujian Agriculture and Forestry University

Emerging contaminants(ECs) of significant concern are widely distributed throughout the environment due to various industrial practices and human activities. Given the alarming ecological threats and potential risks that ECs pose to human health and aquatic life, even at trace concentrations, it is imperative to develop innovative technologies to effectively address these challenges. The biophotoelectrochemistry(BPEC) system, which integrates microbial cells with photosensitizers for solar-tochemical conversion, holds great potential as an efficient strategy for the removal of ECs. In this review, we provide new insights into the BPEC system for the ECs treatment by systematically summarizing the classification, sources, and environmental occurrence of ECs. Additionally, we explore the research progress and degradation mechanisms in ECs removal with ***, the current challenges and future perspectives for the applications of the BPEC system in the ECs treatment are *** review aims to promote the development of BPEC technology for ECs treatment, offering a promising prospect for environmental remediation, circular economy, and clean-energy production.

关键词： emerging contaminants biophotoelectrochemistry photocatalysis biodegradation

Resource allocation for D2D-assisted haptic communications

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Digital Communications and Networks 2024年第1期10卷 63-74页

作者： Yan Wu Chao Yue Yang Yang Liang Ao College of Telecommunication Engineering Army Engineering University of PLANanjing210000China

Haptic communications is recognized as a promising enabler of extensive services by enabling real-time haptic control and feedback in remote environments,e.g.,teleoperation and autonomous *** the strict transmission requirements on reliability and latency,Device-to-Device(D2D)communications is introduced to assist haptic *** particular,the teleoperators with poor channel quality are assisted by auxiliaries,and each auxiliary and its corresponding teleoperator constitute a D2D ***,the haptic interaction and the scarcity of radio resources pose severe challenges to the resource allocation,especially facing the sporadic packet ***,the contentionbased access scheme is applied to achieve low-latency transmission,where the resource scheduling latency is omitted and users can directly access available *** this context,we derive the reliability index of D2D pairs under the contention-based access scheme,i.e.,closed-loop packet error ***,the reliability performance is guaranteed by bidirectional power control,which aims to minimize the sum packet error probability of all D2D *** game theory is introduced to solve the problem with low ***,a distributed power control algorithm based on synchronous log-linear learning is proposed to converge to the optimal Nash *** results demonstrate the superiority of the proposed learning algorithm.

关键词： Haptic communications D2D Power control Contention-based access Potential game

Graphene-anchored sodium single atoms:A highly active and stable catalyst for transesterification reaction

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Nano Research 2024年第6期17卷 4979-4985页

作者： Song-Song Peng Yao Nian Xing-Ru Song Xiang-Bin Shao Chen Gu Zhi-Wei Xing Shi-Chao Qi Peng Tan You Han Xiao-Qin Liu Lin-Bing Sun State Key Laboratory of Materials-Oriented Chemical Engineering Jiangsu National Synergetic Innovation Center for Advanced Materials(SICAM)College of Chemical EngineeringNanjing Tech University30 South Puzhu RoadNanjing 211816China School of Chemical Engineering and Technology Tianjin UniversityTianjin 300072China Haihe Laboratory of Sustainable Chemical Transformations Tianjin 300192China

Solid strong base catalysts have received considerable attention in various organic reactions due to their facile separation,neglectable corrosion,and environmental *** great progress has been made in the preparation of solid strong base catalysts,it is still challenging to avoid basic sites aggregation on support and active sites loss in reaction ***,we report a tandem redox strategy to prepare Na single atoms on graphene,producing a new kind of solid strong base catalyst(Na1/G).The base precursor NaNO_(3)was first reduced to Na2O by graphene(400℃)and successively to single atoms Na anchored on the graphene vacancies(800℃).Owing to the atomically dispersed of basicity,the resultant catalyst presents high activity toward the transesterification of methanol and ethylene carbonate to synthesize dimethyl carbonate(turnover frequency(TOF)value:125.7 h^(−1)),which is much better than the conventional counterpart Na2O/G and various reported solid strong bases(TOF:1.0-90.1 h^(−1)).Furthermore,thanks to the basicity anchored on graphene,the Na1/G catalyst shows excellent durability during *** work may provide a new direction for the development of solid strong base catalysts.

关键词： solid strong base catalyst basic sites redox graphene single Na atoms

Anti-osteosarcoma trimodal synergistic therapy using NiFe-LDH and MXene nanocomposite for enhanced biocompatibility and efficacy

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Acta Pharmaceutica Sinica B 2024年第3期14卷 1329-1344页

作者： Yani Xu Lan Yang Min Li Haozhou Shu Na Jia Yunzhen Gao Rongying Shi Xiaojia Yang Zhirong Zhang Ling Zhang Key Laboratory of Drug-Targeting and Drug Delivery System of the Education Ministry West China School of PharmacySichuan UniversityChengdu 610041China Med-X Center for Materials College of Polymer Science and EngineeringSichuan UniversityChengdu 610065China

Osteosarcoma is usually resistant to immunotherapy and,thus primarily relies on surgical resection and high-dosage ***,less invasive or toxic therapies such as photothermal therapy(PTT)and chemodynamic therapy(CDT)generally failed to show satisfactory *** multimodal therapies with proper safety profiles may provide better solutions for ***,a simple nanocomposite that synergistically combines CDT,PTT,and chemotherapy for osteosarcoma treatment was *** this composite,small 2D Ni Fe-LDH flakes were processed into 3D hollow nanospheres via template methods to encapsulate 5-Fluorouracil(5-FU)with high loading *** nanospheres were then adsorbed onto larger 2D Ti3C2MXene monolayers and finally shielded by bovine serum albumin(BSA)to form 5-FU@Ni Fe-LDH/Ti3C2/BSA nanoplatforms(5NiTiB).Both in vitro and in vivo data demonstrated that the 5-FU induced chemotherapy,Ni Fe-LDH driven chemodynamic effects,and MXene-based photothermal killing collectively exhibited a synergistic“all-in-one”anti-tumor effect.5NiTiB improved tumor suppression rate from<5%by 5-FU alone to~80.1%.This nanotherapeutic platform achieved higher therapeutic efficacy with a lower agent dose,thereby minimizing side ***,the composite is simple to produce,enabling the fine-tuning of dosages to suit different ***,the platform is versatile and efficient,with potential for further development.

关键词： Osteosarcoma NiFe-LDH MXene Chemodynamic therapy Photothermal therapy Chemotherapy 5-Fluorouracil Nanocomposite

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Enzyme-activatable disk-shaped nanocarriers augment tumor permeability for breast cancer combination therapy

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Nano Research 2024年第7期17卷 6400-6410页

作者： Hanming Zhang Honglin Gao Yicong Zhang Yikun Han Qing Lin Tao Gong Xun Sun Zhirong Zhang Ling Zhang Shiqi Huang Key Laboratory of Drug-Targeting and Drug Delivery System of the Education Ministry West China School of PharmacySichuan UniversityChengdu 610041China Med-X Center for Materials College of Polymer Science and EngineeringSichuan UniversityChengdu 610065China

Unique physiopathological characteristics of tumor tissues impose obstacles to the sufficient penetration of traditional nanomedicines,resulting in undesirable drug delivery efficacy and therapeutic ***,we constructed TRAIL-[NDHCPT]^(GAC),a synergistic hydroxycamptothecin(HCPT)and tumor necrosis factor-related apoptosis-inducing ligand(TRAIL)protein co-loaded disk-shaped nanocarrier withγ-glutamyl transpeptidase *** the novel nanodisks extravasated into the tumor interstitium,theγ-glutamyl transpeptidase overexpressed on the tumor cell membranes cleaved theγ-glutamyl portions of the nanodisk surface to produce positively charged amino *** a result,the cationic nanodisks possessed stronger tumor infiltration ability through transcytosis than anionic *** and TRAIL exerted synergistic antitumor effects with better overall therapeutic *** TRAIL-[ND-HCPT]^(GAC)system performed significantly better than free HCPT and remarkably prolonged the survival of breast tumor-bearing mice with no significant toxicity.

关键词： tumor penetration combination therapy charge reversal γ-glutamyl transpeptidase nanodisk

Effect of diagenetic variation on the static and dynamic mechanical behavior of coral reef limestone

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International Journal of Mining science and Technology 2024年第7期34卷 893-908页

作者： Linjian Ma Jiajun Deng Mingyang Wang Jianping Wang Bin Fang Jiawen Wu State Key Laboratory of Explosion&Impact and Disaster Prevention&Mitigation Army Engineering University of PLANanjing 210007China Naval Research Institute Beijing 100070China

Coral reef limestone at different depositional depths and facies differ remarkably on the textural and mineralogical characteristics,owing to the complex sedimentary *** explore the effects of pore structure and mineral composition associated with diagenetic variation on the mechanical behavior of reef limestone,a series of quasi-static and dynamic compression tests along with microscopic examinations were performed on the reef limestone at shallow and deep burial *** is revealed that the shallow reef limestone(SRL)is classified as a porous aragonite-type carbonate rock with high porosity(55.3±3.2)%and pore *** comparison,the deep reef limestone(DRL)is mainly composed of dense calcite-type calcium carbonate with low porosity(4.9±1.6)%and pore *** DRL strengthened and stiffened by the tight grain framework consistently displays much higher values of the dynamic compressive strength,elastic modulus,brittleness index,and specific energy absorption than those of the *** gap between two types of limestone further increases with an increase in strain *** appears that the failure pattern of SRL is dominated by the inherent defects like weak bonding interfaces and growth lines,revealed by the intricate fracturing network and mixed ***,although the preexisting megapores in DRL may affect the crack propagation on pore tips to a certain distance,it hardly alters the axial splitting failure of DRL under *** stress wave propagation and attenuation in SRL is primarily controlled by the reflection and diffusion caused by plenty mesopores,as well as an energy dissipation in layer-wise pore collapse and adjacent grain crushing,while the stress wave in DRL is highly hinged on the insulation and diffraction induced by the isolated *** process is accompanied by the energy dissipation behavior of inelastic deformation resulted from the pore-emanated microcracking.

关键词： Reef limestone Dynamic behavior Mineral composition Pore structure Wave propagation Energy dissipation

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Large low-field reversible magnetocaloric effect in K_(3)Gd(PO_(4))_(2) at sub-Kelvin temperature

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Journal of Rare Earths 2024年第6期42卷 1087-1092,I0003页

作者： Haojie Wang Zhaojun Mo Jianjian Gong Heng Tu Guochun Zhang Jun Shen School of Rare Earths University of Science and Technology of ChinaHefei230026China Ganjiang Innovation Academy Chinese Academy of SciencesGanzhou341119China Center for Crystal Research and Development Key Laboratory of Functional Crystals and Laser TechnologyKey Laboratory of CryogenicsTechnical Institute of Physics and ChemistryChinese Academy of SciencesBeijing100190China Department of Energy and PowerEngineering School of Mechanical EngineeringBeijing Institute of TechnologyBeijing100081China

We synthesized a potassium gadolinium phosphate K3Gd(PO_(4))_(2)with monoclinic structure(P2_(1/m))by the high-temperature solid-state reaction *** lattice constants obtained by Rietveld refinements of XRD curve are a=0.7411 nm,b=0.5624 nm,and c=0.9433 *** and magnetocaloric properties of K_(3)Gd(PO_(4))_(2)were investigated in *** magnetic phase transition temperature of K3Gd(PO_(4))2 was determined by ultra-low temperature testing to be 0.58 K.K_(3)Gd(PO_(4))2 exhibits large magnetic entropy changes(-ΔSM).The maximum-ΔSM are 20.2 and 29.4 J/(kg·K)in the magnetic field variation(ΔH)of 1 and 2 T,respectively,which are larger than that of the commercial Gd_(3)Ga_(5)O_(12)(GGG).The maximum adiabatic temperature change(ΔT_(ad))reaches 5.91 K under a magnetic field change(ΔH)of 1 T.K_(3)Gd(PO_(4))_(2)is a potential magnetic refrigeration material for obtaining sub-Kelvin temperatures.

关键词： Ultra-low temperature Magnetocaloric effect Magnetic entropy change Magnetic refrigeration Rare earths

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