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Hot Deformation Behavior and Microstructures Evolution of GNP-Reinforced Fine-Grained Mg Composites

Acta Metallurgica Sinica(English Letters) 2024年第3期37卷 407-424页

作者： Hengrui Hu Jiayu Qin Yunpeng Zhu Jinhui Wang Xiaoqiang Li Peipeng Jin Qinghai Provincial Key Laboratory of New Light Alloys Qinghai UniversityXining 810016China Qinghai Provincial Engineering Research Center of High Performance Light Metal Alloys and Forming Qinghai UniversityXining 810016China Department of Mechanical Engineering Tsinghua UniversityBeijing 100084China School of Material science and Engineering Lanzhou University of TechnologyLanzhou 730050China

Graphene nanoplates(GNPs)-reinforced magnesium matrix composites have been attracted great ***,knowledge is lack for the hot deformation behavior of GNP-reinforced magnesium(GNPs/Mg)*** this study,the fine-grained GNPs/Mg composite was fabricated by powder metallurgy process followed by *** hot deformation behavior,microstructure evolution and dynamic recrystallization(DRX)mechanism of fine-grained GNPs/Mg composite were investigated by hot compression test and electron back-scatter diffraction(EBSD).The hot compression tests of the composite were conducted at temperatures between 423 and 573 K with the strain rates from 0.001 to 1 s^(-1).The strain compensated power law equation was established to describe the hot deformation behavior of the *** stress exponent and activation energy of the composite are 7.76 and 83.23 kJ/mol,respectively,suggesting that the deformation mechanism is grain boundary slip controlled dislocation climb *** abnormally high stress exponent and activation energy are unattainable in the composite due to the fine grain size of the composites and the absence of Zener pinning and Orowan effects of GNPs *** grain size increases with the decrease in Zener-Hollomn(Z)parameter,which can be well fitted by power-law *** the increase in grain size and decrease in Z parameter,the geometrically necessary dislocation density decreases,which shows the approximately power-law relationship.A random and weak texture was formed after hot *** discontinuous dynamic recrystallization and continuous dynamic recrystallization mechanism dominated the DRX behavior at 473 K/0.001 s^(-1) and 573 K/0.001 s^(-1),respectively.

关键词： GNPs Mg composite Hot deformation behavior Constitutive equations Microstructure evolution Dynamic recrystallization

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Incorporating empirical knowledge into data-driven variable selection for quantitative analysis of coal ash content by laser-induced breakdown spectroscopy

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Plasma science and technology 2024年第7期26卷 148-156页

作者：吕一涵宋惟然侯宗余王哲 State Key Laboratory of Power System Operation and Control International Joint Laboratory on Low Carbon Clean Energy InnovationDepartment of Energy and Power EngineeringTsinghua UniversityBeijing 100084People’s Republic of China School of Energy and Electrical Engineering Qinghai UniversityXining 810016People’s Republic of China Tsinghua University Shanxi Research Institute Clean EnergyTaiyuan 030032People’s Republic of China

Laser-induced breakdown spectroscopy(LIBS)has become a widely used atomic spectroscopic technique for rapid coal ***,the vast amount of spectral information in LIBS contains signal uncertainty,which can affect its quantification *** this work,we propose a hybrid variable selection method to improve the performance of LIBS *** variables are first identified using Pearson's correlation coefficient,mutual information,least absolute shrinkage and selection operator(LASSO)and random forest,and then filtered and combined with empirical variables related to fingerprint elements of coal ash ***,these variables are fed into a partial least squares regression(PLSR).Additionally,in some models,certain variables unrelated to ash content are removed manually to study the impact of variable deselection on model *** proposed hybrid strategy was tested on three LIBS datasets for quantitative analysis of coal ash content and compared with the corresponding data-driven baseline *** is significantly better than the variable selection only method based on empirical knowledge and in most cases outperforms the baseline *** results showed that on all three datasets the hybrid strategy for variable selection combining empirical knowledge and data-driven algorithms achieved the lowest root mean square error of prediction(RMSEP)values of 1.605,3.478 and 1.647,respectively,which were significantly lower than those obtained from multiple linear regression using only 12 empirical variables,which are 1.959,3.718 and 2.181,*** LASSO-PLSR model with empirical support and 20 selected variables exhibited a significantly improved performance after variable deselection,with RMSEP values dropping from 1.635,3.962 and 1.647 to 1.483,3.086 and 1.567,*** results demonstrate that using empirical knowledge as a support for datadriven variable selection can be a viable approach to improve the acc

关键词： laser-induced breakdown spectroscopy(LIBS) coal ash content quantitative analysis variable selection empirical knowledge partial least squares regression(PLSR)

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Enlarged interlayer of separator coating enabling high-performance lithiumsulfur batteries

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Frontiers of Chemical science and Engineering 2024年第2期18卷 103-112页

作者： Yanqi Feng Hui Liu Xiaoting Liu Qiongqiong Lu School of Materials&Environment Engineering Chengdu Technological UniversityChengdu 611730China School of Materials science and Engineering Shaanxi Key Laboratory of Green Preparation and Functionalization for Inorganic MaterialsShaanxi University of Science and TechnologyXi’an 710021China Green Catalysis Center and College of ChemistryZhengzhou UniversityZhengzhou 450001China Institute of Materials Henan Key Laboratory of Advanced Conductor MaterialsHenan Academy of SciencesZhengzhou 450046China Leibniz Institute for Solid State and Materials Research(IFW) Dresden e.V.Dresden 01069Germany

Lithiumsulfur batteries have been intensively studied due to their high theoretical energy density and abundant sulfur resources. However, their commercial application is hindered by the low redox kinetics and high sulfur losses. In principle, in the design of cathodes and separators, the adsorption toward lithium-polysulfides should be enhanced and the conversion of soluble high-order lithium-polysulfides should be catalyzed. Herein, a KV_(3)O_(8)·0.75H_(2)O separator is designed as an effective lithium-polysulfides mediator in lithiumsulfur batteries. The intercalated K+ would enlarge the interlayer spacing of vanadium oxides, preventing the collapse of the layer structure and improving the electrical/ion conductivity of the interface. Moreover, the KV_(3)O_(8)·0.75H_(2)O modified separator possess a prior adsorption and high redox kinetics toward lithium-polysulfides due to the enhanced diffusion kinetics, which guarantees the high-rate capability and efficient utilization of sulfur. As a result, lithiumsulfur batteries exhibit a high capacity of 1362 mAh·g^(-1) and a long lifespan with a low capacity loss of 0.073% per cycle. This work may provide an alternative way to establish a functional separator to balance the adsorption and conversion of polysulfides during the redox back and forth.

关键词： lithium kinetics adsorption

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Performance Analysis of an Efficient Integration System of Coal-Fired Power Plant,Solar Thermal Energy and CO_(2)Capture

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Journal of Thermal science 2024年第4期33卷 1509-1522页

作者： WANG Yuhao WANG Ruilin LIU Lanhua XING Chenjian GUO Yafei YANG Qingshan YING Jiaheng SUN Jian LI Wenjia LIU Yuanyuan ZHAO Chuanwen School of Energy and Mechanical Engineering Nanjing Normal UniversityNanjing210023China China Huadian Group Co.LTD.Shanghai Branch Shanghai200120China Key Laboratory of Efficient Utilization of Low and Medium Grade Energy(Tianjin University) Ministry of Education of ChinaTianjin300350China Huadian Zhengzhou Mechanical Design Institute Company Limited Zhengzhou450046China

Coal-fired power plant is a major contributor to greenhouse gas *** post-combustion capture is a promising method for CO_(2)emission reduction but the high thermal demand is *** address this issue,solar thermal energy and CO_(2)capture are jointly integrated into the coal-fired power plant in this *** solar thermal energy is employed to meet the heat requirement of the CO_(2)capture process,thereby avoiding the electricity loss caused by self-driven CO_(2)***,the heat released from the carbonation reaction of MgO adsorbent is integrated into the steam Rankine *** partially substituting the extracted steam for feedwater heating,the electricity output of the power plant is further *** to the results from the developed model,the system could achieve a CO_(2)capture rate of 86.5%and an electricity output enhancement of 9.8%compared to the reference system,which consists of a self-driven CO_(2)capture coal-fired power plant and PV generation *** operational strategy is also optimized and the amount of CO_(2)emission reduction on a typical day is increased by 11.06%.This work shows a way to combine fossil fuels and renewable energy for low carbon emissions and efficient power generation.

关键词： CO_(2)capture parabolic trough collector solar aided coal-fired electricity generation

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Simultaneously quantifying hundreds of acylcarnitines in multiple biological matrices within ten minutes using ultrahigh-performance liquid-chromatography and tandem mass spectrometry

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Journal of Pharmaceutical Analysis 2024年第1期14卷 140-148页

作者： Jingxian Zhang Qinsheng Chen Lianglong Zhang Biru Shi Men Yu Qingxia Huang Huiru Tang State Key Laboratory of Genetic Engineering School of Life SciencesHuman Phenome InstituteZhangjiang Fudan International Innovation CenterMetabonomics and Systems Biology Laboratory at Shanghai International Centre for Molecular PhenomicsZhongshan HospitalFudan UniversityShanghai200032China Wuhan Laboratory for Shanghai Metabolome Institute(SMI)Ltd. Wuhan430000China

Acylcarnitines are metabolic intermediates of fatty acids and branched-chain amino acids having vital biofunctions and pathophysiological significances. Here, we developed a high-throughput method for quantifying hundreds of acylcarnitines in one run using ultrahigh performance liquid chromatography and tandem mass spectrometry (UPLC-MS/MS). This enabled simultaneous quantification of 1136 acylcarnitines (C0–C26) within 10-min with good sensitivity (limit of detection 0.992), accuracy (relative error 0.998) for predicting retention time (tR) of acylcarnitines with no standards and built a database of their multiple reaction monitoring parameters (tR, ion-pairs, and collision energy). Furthermore, we quantified 514 acylcarnitines in human plasma and urine, mouse kidney, liver, heart, lung, and muscle. This provides a rapid method for quantifying acylcarnitines in multiple biological matrices.

关键词： Acylcarnitine UPLC-MS/MS Quantitative structure-retention relationship Molecular phenotype

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Effects of Rosa roxburghii&edible fungus fermentation broth on immune response and gut microbiota in immunosuppressed mice

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Food science and Human Wellness 2024年第1期13卷 154-165页

作者： Dechang Xu Jielun Hu Yadong Zhong Yanli Zhang Wenting Liu Shaoping Nie Mingyong Xie State Key Laboratory of Food science and technology China-Canada Joint Laboratory of Food Science and Technology(Nanchang)Key Laboratory of Bioactive Polysaccharides of Jiangxi ProvinceNanchang UniversityNanchang 330047China

With the rise of probiotics fermentation in food industry,fermented foods have attracted worldwide *** this study,protective effects of Rosa roxburghii&edible fungus fermentation broth(REFB)on immune function and gut health in Cyclophosphamide induced immunosuppressed mice were *** showed that REFB could improve the immune organ index,and promote the proliferation and differentiation of splenic T *** addition,it attenuated intestinal mucosal damage and improved intestinal cellular *** administration also up-regulated the expression of IL-4,INF-γ,TNF-α,T-bet and GATA-3 mRNA in small ***,administration of REFB modulated gut microbiota composition and increased the relative abundance of beneficial genus,such as *** also increased the production of fecal short-chain fatty *** indicate that REFB has the potential to improve immunity,alleviate intestinal injury and regulate gut microbiota in immunosuppressed mice.

关键词： Fermented foods Immunosuppressed mice Immune response Gut microbiota Short-chain fatty acids

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Anomalous negative magnetoresistance in quantum dot Josephson junctions with Kondo correlations

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science China(Physics,Mechanics & Astronomy) 2024年第8期67卷 3-13页

作者： Mingtang Deng Chunlin Yu Guangyao Huang Rosa López Philippe Caroff Sepideh Ghalamestani Gloria Platero Hongqi Xu Institute for Quantum Information&State Key Laboratory of High Performance Computing College of Computer Science and TechnologyNational University of Defense TechnologyChangsha 410073China NanoLund and Division of Solid State Physics Lund UniversityLund S-22100Sweden China Greatwall Quantum Laboratory Changsha 410006China Institut de Física Interdisciplinària i de Sistemes Complexos IFISC Palma de Mallorca E-07122Spain Instituto de Ciencia de Materiales de Madrid Madrid 28049Spain Beijing Key Laboratory of Quantum Devices Key Laboratory for the Physics and Chemistry of Nanodevicesand Department of ElectronicsPeking UniversityBeijing 100871China Beijing Academy of Quantum Information sciences Beijing 100193China Hefei National Laboratory Hefei 230088China

The interplay between superconductivity and the Kondo effect has stimulated significant interest in condensed matter *** compete when their critical temperatures are close and can give rise to a quantum phase transition that can mimic Majorana zero ***,we have fabricated and measured Al-InSb nanowire quantum dot-Al *** the Kondo regime,a supercurrent-induced zero-bias conductance peak *** zero-bias peak shows an anomalous negative magnetoresistance(NMR)at weak magnetic *** attribute this anomalous NMR to quasiparticle trapping at vortices in the superconductor leads as a weak magnetic field is *** trapping effect lowers the quasiparticle-caused dissipation and thus enhances the Josephson *** work connects the vortex physics and the supercurrent tunneling in Kondo regimes and can help further understand the physics of Josephson quantum dot system.

关键词： quantum dot Kondo correlation InSb nanowire quasiparticle trapping

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Defective MnO2 functional separator coating as effective polysulfide mediators for lithium–sulfur batteries

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Tungsten 2024年第03期6卷 536-543页

作者： Yan-Qi Feng Qiong-Qiong Lu Hui Liu School of Materials & Environment Engineering Chengdu Technological University School of Materials science and Engineering Shaanxi Key Laboratory of Green Preparation and Functionalization for Inorganic Materials Shaanxi University of Science and Technology Institute of Materials Henan Key Laboratory of Advanced Conductor Materials Henan Academy of Sciences Institute of Materials Chemistry Leibniz Institute for Solid State and Materials Research (IFW) Dresden e.V.

Advanced energy storage systems are in urgent need nowadays due to the rising demand in mobile devices and electric vehicles [1]. Lithium–sulfur（Li–S） batteries are intensively studied due to the high theoretical specific capacity(1675 m Ah·g-1) and energy density(2600 Wh·kg-1), as well as natural abundant and environmentally friendly of sulfur.

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High-intensity spatial-mode steerable frequency up-converter toward on-chip integration

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Opto-Electronic science 2024年第4期3卷 12-20页

作者： Haizhou Huang Huaixi Chen Huagang Liu Zhi Zhang Xinkai Feng Jiaying Chen Hongchun Wu Jing Deng Wanguo Liang Wenxiong Lin Key Laboratory of Optoelectronic Materials Chemistry and Physics Fujian Institute of Research on the Structure of MatterChinese Academy of ScienceFuzhou 350002China Key Laboratory of Opto-Electronic science and technology for Medicine of Ministry of Education Fujian Provincial Key Laboratory of Photonics TechnologyCollege of Photonic and Electronic EngineeringFujian Normal UniversityFuzhou 350117China Fujian science&technology Innovation Laboratory for Optoelectronic Information of China Fuzhou 350108China College of Digital Economy Fujian Agriculture and Forestry UniversityFuzhou 350002China University of Chinese Academy of sciences Beijing 100049China.

Integrated photonic devices are essential for on-chip optical communication,optical-electronic systems,and quantum information *** develop a high-fidelity interface between photonics in various frequency domains without disturbing their quantum properties,nonlinear frequency conversion,typically steered with the quadratic(χ2)process,should be ***,another degree of freedom in steering the spatial modes during theχ2 process,with unprecedent mode intensity is proposed here by modulating the lithium niobate(LN)waveguide-based inter-mode quasi-phasematching conditions with both temperature and wavelength *** high incident light intensities(25 and 27.8 dBm for the pump and the signal lights,respectively),mode conversion at the sum-frequency wavelength with sufficient high output power(−7–8 dBm)among the TM01,TM10,and TM00 modes is realized automatically with characterized broad temperature(ΔT≥8°C)and wavelength windows(Δλ≥1 nm),avoiding the previous efforts in carefully preparing the signal or pump *** results prove that high-intensity spatial modes can be prepared at arbitrary transparent wavelength of theχ2 media toward on-chip integration,which facilitates the development of chip-based communication and quantum information systems because spatial correlations can be applied to generate hyperentangled states and provide additional robustness in quantum error correction with the extended Hilbert space.

关键词： integrated photonics LN waveguide sum-frequency generation spatial-mode steering on-chip integration

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协同Orowan绕过和攀移机制的镍基高温合金蠕变新模型

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Transactions of Nonferrous Metals Society of China 2024年第4期34卷 1167-1177页

作者：李昉袁丁玲陈康华陈送义李理中南大学粉末冶金国家重点实验室长沙410083 中南大学轻合金研究院长沙410083 湖南大学机械与车辆工程学院汽车车身先进设计制造国家重点实验室长沙410082

提出一种用于准确便捷预测析出相增强镍基高温合金稳态蠕变速率的蠕变新模型。基于析出相的空间分布,采用概率依赖的方法将位错-析出相交互作用中Orowan绕过和位错攀移机制的协同模式耦合到新的蠕变模型中。结果表明,新模型预测的稳态... 详细信息

提出一种用于准确便捷预测析出相增强镍基高温合金稳态蠕变速率的蠕变新模型。基于析出相的空间分布,采用概率依赖的方法将位错-析出相交互作用中Orowan绕过和位错攀移机制的协同模式耦合到新的蠕变模型中。结果表明,新模型预测的稳态蠕变速率与实验数据吻合很好。此外,当前模型不再依赖于可调参数;同时,确定了阈值应力与温度的定量关系。这项工作为蠕变变形过程中位错-析出相交互作用提供新思路,并为设计具有更优异蠕变性能的析出强化合金提供有效模型。

关键词：镍基高温合金蠕变模型稳态蠕变速率阈值应力

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