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High-throughput synthesis of size-controlled Pt-based catalysts

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Particuology 2023年第12期83卷 232-240页

作者： zhuoran deng Liqiang Zhao Daojian Cheng State Key Laboratory of Organic-Inorganic Composites Beijing University of Chemical TechnologyBeijing100029China College of Information Science and Technology Beijing University of Chemical TechnologyBeijing100029China

Pt catalysts are commonly used for chemical reaction processes due to its high catalytic activity and ***,the size of metal particles often has a significant impact on the performance of the metal-loaded ***,developing highly efficiently synthesis method for the size control of Pt catalysts has great development prospects and research *** this study,high-throughput size tuning of Pt-based catalysts was achieved by carbonizing the *** experimental and characterization results showed that the size of the loaded Pt nanoparticles varied with different concentrations of glucose solution during carriers carbonization *** reduction of 4-nitrophenol as a template reaction indicated that the reaction rate constant of the catalyst is approximately linear with the size of Pt ***,a laboratory-built high-throughput synthesis system was applied for the catalyst synthesis,which enhances the automation of the laboratory exploratory experiments and makes it possible to synthesize catalysts with controllable size in batches.

关键词： High-throughput synthesis Size modulation Pt-based catalysts 4-Nitrophenol reduction

镁橄榄石对油井水泥抗CO_(2)腐蚀性能的影响

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中国粉体技术 2024年第2期30卷 151-163页

作者：郑怡杰龚鹏邓卓然何鑫张春梅梅开元程小伟西南石油大学新能源与材料学院油气藏地质及开发工程全国重点实验室四川成都610500

【目的】研究镁橄榄石掺加对减轻超临界CO_(2)环境下油井水泥石的腐蚀渗透性能。【方法】以镁橄榄石粉为外掺料配制不同的油井水泥,分析温度为150℃,CO_(2)总压为50 MPa条件下镁橄榄石水泥石的抗压强度,优选出镁橄榄石粉的最佳掺量;利... 详细信息

【目的】研究镁橄榄石掺加对减轻超临界CO_(2)环境下油井水泥石的腐蚀渗透性能。【方法】以镁橄榄石粉为外掺料配制不同的油井水泥,分析温度为150℃,CO_(2)总压为50 MPa条件下镁橄榄石水泥石的抗压强度,优选出镁橄榄石粉的最佳掺量;利用渗透率、热重分析(thermo gravimetric analysis,TGA)、X射线衍射(X-Ray diffraction,XRD)和扫描电子显微镜(scanning electron microscope,SEM)进行测试,评价镁橄榄石对油井水泥石抗CO_(2)腐蚀性能的影响,分析镁橄榄石对油井水泥石抗CO_(2)腐蚀的作用机制。【结果】镁橄榄石粉的掺入不会影响油井水泥的流动度,当镁橄榄石粉的质量分数为2%时,对比腐蚀前油井水泥石的,抗压强度提高35.47%,渗透率降低0.0104 m D;腐蚀28 d后,镁橄榄石水泥石的抗压强度为空白水泥石的193.71%,且仍高于腐蚀前。【结论】镁橄榄石是一种抗CO_(2)腐蚀外加剂,能提升油井水泥的抗CO_(2)腐蚀性能。

关键词：镁橄榄石超临界二氧化碳腐蚀油井水泥石

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Microstructure Regulation and Combustion Performance Optimization of PVDF/Al Composite Powder by Non-covalent Functionalized Graphenes

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Journal of Wuhan University of Technology(Materials Science) 2024年第4期39卷 904-911页

作者：易卓然 deng Haoyuan QIN Mei 孙一 LUO Guoqiang State Key Laboratory of Advanced Technology for Materials Synthesis and Processing Wuhan University of TechnologyWuhan 430070China

Graphene prepared by non-covalent modification of sulfonated poly(ether-ether-ketone)(SPG)was combined with polyvinylidene fluoride(PVDF)/Al to improve the PVDF/Al thermal conductivity while reducing the effect of the thermal resistance at the graphene-polymer *** regulation rule of SPG with different contents on the energy release of fluorine-containing system was *** the content of SPG is 4%,the peak pressure and rise rate of SPG/PVDF/Al composite powder during ignition reach the maximum of 4845.28 kPa and 8683.58 kPa/*** the content of SPG is 5%,the PVDF/Al composite powder is completely coated by SPG,and the calorific value of the material reachs the maximum of 29.094 kJ/*** the design and micro-control of the composite powder,the calorific value of the material can be effectively improved,but the improvement of the mass release rate still depends on the graphene content and surface modification state.

关键词： energetic materials PVDF/Al composites graphene modification energy release combustion

CMOS-level mega-pixel organic camera chips made of photocrosslinked photovoltaic nanocells

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Science China Materials 2024年第9期67卷 3043-3045页

作者： Yegang Liang zhuoran Wang Guozhen Shen School of Integrated Circuits and Electronics Beijing Institute of TechnologyBeijing100081China

Organic and hybrid optoelectronics have been driving the frontiers in displays,sensing,and energy in recent decades due to their superior performance,low-cost high-yield manufacturing,and new form factor of mechanical flexibility that is promising for lightweight and wearable applications[1-3].However,the inherent vulnerability makes organic semiconductors incompatible with conventional semiconductor microfabrication,posing significant challenges in high density integration to compete with the resolution of conventional image sensors[4].

关键词： frontier driving lightweight

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Artificial hawk-eye camera for foveated, tetrachromatic, and dynamic vision

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Journal of Semiconductors 2024年第9期45卷 1-3页

作者： Wenhao Ran zhuoran Wang Guozhen Shen School of Integrated Circuits and Electronics Beijing Institute of TechnologyBeijing 100081China Institute of Flexible Electronics Beijing Institute of TechnologyBeijing 102488China

With the rapid development of drones and autonomous vehicles, miniaturized and lightweight vision sensors that can track targets are of great interests. Limited by the flat structure, conventional image sensors apply a large number of lenses to achieve corresponding functions, increasing the overall volume and weight of the system.

关键词： awk vision system.

Adaptive battery thermal management systems in unsteady thermal application contexts

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Journal of Energy Chemistry 2024年第10期97卷 650-668页

作者： Kailong Liu Qiao Peng zhuoran Liu Wei Li Naxin Cui Chenghui Zhang School of Control Science and Engineering Shandong University Information Technology Analytics & Operations Group Queen's University Belfast College of Design and Engineering National University of Singapore

With the increasing attention paid to battery technology,the microscopic reaction mechanism and macroscopic heat transfer process of lithium-ion batteries have been further studied and understood from both academic and industrial ***,as one of the key parameters in the physical fra mework of batteries,affects the performa nce of the multi-physical fields within the battery,a nd its effective control is *** the heat generation in the battery is determined by the real-time operating conditions,the battery temperature is essentially controlled by the real-time heat dissipation conditions provided by the battery thermal management *** battery thermal management systems have basic temperature control capabilities for most conventional application ***,with the current development of la rge-scale,integrated,and intelligent battery technology,the adva ncement of battery thermal management technology will pay more attention to the effective control of battery temperature under sophisticated situations,such as high power and widely varied operating *** this context,this paper presents the latest advances and representative research related to battery thermal management ***,starting from battery thermal profile,the mechanism of battery heat generation is discussed in ***,the static characteristics of the traditional battery thermal management system are ***,considering the dynamic requirements of battery heat dissipation under complex operating conditions,the concept of adaptive battery thermal management system is proposed based on specific research ***,the main challenges for battery thermal management system in practice are identified,and potential future developments to overcome these challenges are presented and discussed.

关键词： Battery safety Battery thermal management system Cooling methods Heat generation mechanism Lithium-ion batteries

Unlocking efficient energy storage via regulating ion and electron-active subunits:an(SbS)_(1.15)TiS_(2)superlattice for large and fast Na^(+)storage

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Science China Chemistry 2024年第1期67卷 336-342页

作者： Baixin Peng Tianxun Cai Shaoning Zhang Yuqiang Fang zhuoran Lv Yusha Gao Fuqiang Huang State Key Laboratory of High Performance Ceramics and Superfine Microstructure Shanghai Institute of CeramicsChinese Academy of SciencesShanghai 200050China Center of Materials Science and Optoelectronics Engineering University of Chinese Academy of SciencesBeijing 100049China School of Physical Science and Technology ShanghaiTech UniversityShanghai 200031China Beijing National Laboratory for Molecular Sciences State Key Laboratory of Rare Earth Materials Chemistry and ApplicationsCollege of Chemistry and Molecular EngineeringPeking UniversityBeijing 100871China

Alloying-type metal sulfides with high sodiation activity and theoretical capacity are promising anode materials for high energy density sodium ion ***,the large volume change and the migratory and aggregation behavior of metal atoms will cause severe capacity decay during the charge/discharge ***,a robust and conductive TiS_(2)framework is integrated with a high-capacity SbS layer to construct a single phase(SbS)_(1.15)TiS_(2)superlattice for both high-capacity and fast Na^(+)*** metallic TiS_(2)sublayer with high electron activity acts as a robust and conductive skeleton to buffer the volume expansion caused by conversion and alloying reaction between Na+and SbS ***,high capacity and high rate capability can be synergistically realized in a single phase(SbS)_(1.15)TiS_(2)*** novel(SbS)_(1.15)TiS_(2)anode has a high charge capacity of 618 mAh g^(-1)at 0.2 C and superior rate performance and cycling stability(205 mAh g^(-1)at 35 C after 2,000 cycles).Furthermore,in situ and ex situ characterizations are applied to get an insight into the multi-step reaction *** integrity of robust Na-Ti-S skeleton during(dis)charge process can be *** superlattice construction idea to integrate the Na^(+)-active unit and electron-active unit would provide a new avenue for exploring high-performance anode materials for advanced sodium-ion batteries.

关键词： (SbS)_(1.15)TiS_(2) sulfides sodium ion battery superlattice fast-charging

mtDNA-triggered pH response signal-amplified fluorescent probe for multiple cell discrimination

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Chinese Chemical Letters 2024年第3期35卷 363-368页

作者： Tianping Xia Yanxian Hou zhuoran Xia Gengwen Chen Peichen Tang Jiangli Fan Xiaojun Peng State Key Laboratory of Fine Chemicals Frontiers Science Center for Smart Materials Oriented Chemical EngineeringDalian University of TechnologyDalian 116024China Hematology Reagent R&D Department Mindray Bio-medical Electronics Co.Ltd.Shenzhen 518132China Research Institute of Dalian University of Technology in Shenzhen Shenzhen 518057China

Developing fluorescence probes with multiple responses has vital significance but remains ***,for the first time,we present a mitochondrial DNA(mtDNA)-triggered pH response signalamplified fluorescent probe(QCY-DBT)for multiple cell *** probe exhibited a large stokes shift(229 nm),excellent DNA selectivity over RNA,and ultrasensitivity of detection limit(DL;74.0 ng/mL).Thus,QCY-DBT was successfully applied to analyze multiple human peripheral blood cells and visualize mtDNA in healthy and apoptotic *** the tumor acidic environment(pH 6.0–7.0),the absorbance of QCY-DBT at 436 nm increased,and the fluorescence signal(665 nm)was amplified by mtDNA,which enabled the direct observation of tumor *** study provides help in designing smart probes with multiple responses for efficient abnormal cell detection.

关键词： Fluorescence probe Mitochondrial DNA pH response Peripheral blood cells Multiple cell detection

Deterministic and Robust Volt-var Control Methods of Power System Based on Convex Deep Learning

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Journal of Modern Power Systems and Clean Energy 2024年第3期12卷 719-729页

作者： Qing Ma Changhong deng the School of Electrical Engineering and Automation Wuhan UniversityWuhanChina

Volt-var control(VVC)is essentially a non-convex optimization problem due to the non-convexity of power flow(PF)constraints,resulting in the difficulty in obtaining the optimum without convexity *** existing second-order cone method for the convexity conversion often leads to a sharp increase in PF constraints and optimization variables,which in turn increases the optimization difficulty or even leads to optimization *** paper first proposes a deterministic VVC method based on convex deep learning power flow(DLPF).This method uses the input convex neural network(ICNN)to establish a single convex mapping between state parameters and node voltage to complete the convexity conversion while the optimization variables only correspond to reactive power equipment,which can ensure the global optimum with extremely fast computation *** cope with the impact brought by the uncertainty of distributed energy and omit the additional worst scenario search of traditional robust VVC,this paper proposes robust VVC method based on convex deep learning interval power flow(DLIPF),which continues to adopt ICNN to establish another convex mapping between state parameters and node voltage *** DLIPF with DLPF,this method decreases the modeling and optimization difficulty of robust VVC *** results on 30-bus,118-bus,and 200-bus systems prove the correctness and rapidity of the proposed methods.

关键词： Volt-var control convexity conversion convex deep learning power flow