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Quantitative investigation of nanofluid imbibition in tight oil reservoirs based on NMR technique

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Petroleum Science 2022年第5期19卷 2185-2198页

作者： Tian-Tian Zhang zhi-Ping Li Caspar Daniel Adenutsi yong-Zhou Wei Zhen-Fu Ma Qing you School of Energy Resources China University of GeosciencesBeijing10083China Beijing Key Laboratory of Unconventional Natural Gas Geological Evaluation and Development Engineering Beijing10083China Core and Rock Properties Laboratory Department of Petroleum EngineeringFaculty of Civil and Geo-EngineeringKwame Nkrumah University of Science and TechnologyKumasiGhana Binnan Oil Production Plant Shengli Oilfield CompanySINOPECBinzhou256606ShandongChina Hekou Oil Production Plant Shengli Oilfield CompanySINOPECDongying257200ShandongChina

Nanofluids have been effective chemical additives for enhanced oil recovery(EOR)in tight oil reservoirs due to their special ***,oil imbibition recoveries vary for different *** oil/water distribution in rocks during imbibition using various nanofluids was less discussed in previous *** this study,we systematically examined the imbibition efficiencies of various nanofluids at60℃.Furthermore,the migration of nanofluids and oil distribution in the rock pores were monitored using nuclear magnetic resonance(NMR).The nanofluids were prepared by dispersing silica nanoparticles and five different types of surfactants i.e.,anionic-nonionic,anionic,nonionic,amphoteric and cationic surfactants in deionized(DI)***,interfacial tension(IFT)and contact angle measurements were conducted to reveal the underlying EOR mechanisms of various *** experimental results showed that the EOR potential of the different types of nanofluids was in the order anionic-nonionic>anionic>nonionic>amphoteric>cationic>***-nonionic(sodium lauryl ether sulfate(SLES))and anionic(sodium dodecyl sulfonate(SDS))nanofluids exhibited excellent capability of wettability alteration,and increased oil recovery by 27.96%and 23.08%,respectively,compared to *** NMR results also showed that mesopores(0.1-1μm)were the dominant developed pores in the rocks,and contributed the most to imbibition *** addition,the imbibition of nanofluids initially took place in mesopores and micropores before moving into *** study provides fundamental information on the selection of nanofluids for EOR in tight oil *** study also improved the understanding of oil/water distribution during the imbibition of the proposed nanofluids.

关键词： Nanofluids Spontaneous imbibition Nuclear magnetic resonance(NMR) Oil migration Tight oil reservoir

Direct and rapid detection of serum amino acid and monoamine neurotransmitters to assist the diagnosis of panic disorder

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Science China Chemistry 2025年第01期 377-384页

作者： Shiwen Liu Xuerui Wan Meng Zhao Jiaqi Wang Weilan Wu Linlin you yonggui Yuan Qian Xu Rong Gao Key Laboratory of Environmental Medicine Engineering Ministry of Education School of Public Health Southeast University Key Laboratory of Modern Toxicology of Ministry of Education Department of Hygienic Analysis and Detection School of Public HealthNanjing Medical University Department of Psychosomatics and Psychiatry Zhongda Hospital School of Medicine Southeast University

The measurement of amino acid and monoamine neurotransmitters（NTs） in serum plays a central role in the identification and monitoring of clinical panic disorder（PD）. However, the strong polarity and chemical heterogeneity of NTs make direct extraction and rapid detection extremely challenging. Herein, we developed a strategy that integrated solid phase extraction based on magnetic Fe3O4coated with polydopamine（Fe3O4@PDA） and direct analysis of mass spectrometry in real time（DART-MS） for quantification of 10 NTs. We systematically investigated the optimal conditions of this strategy to achieve good accuracy and precision. Compared with existing magnetic solid phase extraction methods for NTs detection in biological samples, this strategy could adsorb more targets while having similar adsorption efficiencies, and the total process time was reduced by an average of 69.42%. We rapidly determined the metabolic abnormality of 6 types of NTs in the serum of PD patients and demonstrated their diagnostic accuracy. In addition, an outstanding feature of PD in which tryptophan was more metabolized by the KYN pathway and the 5-hydroxytryptamine pathway was inhibited could be elucidated by this strategy. Our results highlighted the potential ability of Fe3O4@PDA coupled with DART-MS to assist in the clinical diagnosis of PD.

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Viscosity and structure relationship with equimolar substitution of CaO with MgO in the CaO–MgO–Al_(2)O_(3)–SiO_(2)slag melts

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International Journal of Minerals,Metallurgy and Materials 2025年第1期32卷 70-79页

作者： yong Hou Shuo Zhang Jie Dang Jia Guo Hanghang Zhou Xuewei Lü College of Materials Science and Engineering Chongqing UniversityChongqing 400044China Chongqing Key Laboratory of Vanadium-Titanium Metallurgy and New Materials Chongqing UniversityChongqing 400044China

Currently,the Al_(2)O_(3)content in the high-alumina slag systems within blast furnaces is generally limited to 16wt%–18.5wt%,making it challenging to overcome this *** most studies that concentrated on managing the MgO/Al_(2)O_(3)ratio or basicity,this paper explored the effect of equimolar substitution of MgO for CaO on the viscosity and structure of a high-alumina CaO-MgO-Al_(2)O_(3)-SiO_(2)slag system,providing theoretical guidance and data to facilitate the application of high-alumina *** results revealed that the viscosity first decreased and then increased with higher MgO substitution,reaching a minimum at 15mol%MgO *** transform infrared spectroscopy(FTIR)results found that the depths of the troughs representing[SiO_(4)]tetrahedra,[AlO_(4)]tetrahedra,and Si-O-Al bending became progressively deeper with increased MgO *** of the Raman spectra showed that the average number of bridging oxygens per Si atom and the X_(Q^(3))/X_(Q^(2))(X_(Q^(i))is the molar fraction of Q^(i) unit,and i is the number of bridging oxygens in a[SiO_(4)]tetrahedral unit)ratio increased from 2.30 and 1.02 to 2.52 and 2.14,respectively,indicating a progressive polymerization of the silicate structure.X-ray photoelectron spectroscopy(XPS)results highlighted that non-bridging oxygen content decreased from 77.97mol% to 63.41mol% with increasing MgO concentration,whereas bridging oxygen and free oxygen contents *** analysis demonstrated a gradual increase in the polymerization degree of the tetrahedral structure with the increase in MgO ***,bond strength is another important factor affecting the slag *** occurrence of a viscosity minimum can be attributed to the complex evolution of bond strengths of non-bridging oxygens generated during depolymerization of the[SiO_(4)]and[AlO_(4)]tetrahedral structures by CaO and MgO.

关键词： aluminosilicate viscosity structure spectroscopy

TWO-STAGE ESTIMATION FOR SEEMINGLY UNRELATED NONPARAMETRIC REGRESSION MODELS

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Journal of Systems Science & Complexity 2007年第4期20卷 509-520页

作者： Jinhong you Shangyu XIE yong ZHOU Department of Biostatistics University of North Carolina at Chapel Hill Chapel Hill NC 27599-7400 USA. Institute of Applied Mathematics Chinese Academy of Sciences Beijing 100080 China

This paper is concerned with the estimating problem of seemingly unrelated （SU） non- parametric regression models. The authors propose a new method to estimate the unknown functions, which is an extension of the two-stage procedure in the longitudinal data framework. The authors show the resulted estimators are asymptotically normal and more efficient than those based on only the individual regression equation. Some simulation studies are given in support of the asymptotic results. A real data from an ongoing environmental epidemiologie study are used to illustrate the proposed procedure.

关键词： Asymptotic normality nonparametrie model seemingly unrelated regression two-stage estimation

Comparison of four supports for adsorption of reactive dyes by immobilized Aspergillus fumigatus beads

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Journal of Environmental Sciences 2007年第4期19卷 451-457页

作者： WANG Bao-e HU yong-you School of Environmental Science and Engineering South China University of Technology Guangzhou 510640 China.

Four materials, sodium carboxymethylcellulose （Na-CMC）, sodium alginate （SA）, polyvinyl alcohol （PVA）, and chitosan （CTS）, were prepared as supports for entrapping fungus Aspergillusfumigatus. The adsorption of synthetic dyes, Reactive Brilliant Blue KN- R, and Reactive Brilliant Red K-2BP, by these immobilized gel beads and plain gel beads was evaluated. The adsorption efficiencies of Reactive Brilliant Red K-2BP and Reactive Brilliant Blue KN-R by CTS immobilized beads were 89.1% and 93.5% in 12 h, respectively. The adsorption efficiency by Na-CMC immobilized beads was slightly lower than that of mycelial pellets. But the dye culture mediums were almost completely decolorized in 48 h using the above-mentioned two immobilized beads （exceeding 95%）. The adsorption efficiency by SA immobilized beads exceeded 92% in 48 h. PVA-SA immobilized beads showed the lowest adsorption efficiency, which was 79.8% for Reactive Brilliant Red K-2BP and 92.5% for Reactive Brilliant Blue KN-R in 48 h. Comparing the adsorption efficiency by plain gel beads, Na-CMC plain gel beads ranked next to CTS ones. SA and PVA-SA plain gel beads hardly had the ability of adsorbing dyes. Subsequently, the growth of mycelia in Na-CMC and SA immobilized beads were evaluated. The biomass increased continuously in 72 h. The adsorption capacity of Reactive Brilliant Red K-2BP and Reactive Brilliant Blue KN-R by Na-CMC immobilized beads was 78.0 and 86.7 mg/g, respectively. The SEM micrographs show that the surface structure of Na-CMC immobilized bead is loose and finely porous, which facilitates diffusion of the dyes.

关键词： adsorption Aspergillus fumigatus immobilization reactive dyes

Prominent cycling reversibility and kinetics enabled by CaTiO3 protective layer on Zn metal for aqueous Zn-ion batteries

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Journal of Energy Chemistry 2025年第1期100卷 245-258页

作者： Gaeun Lee yong Nam Ahn Seongjoon So Chanwoo Park Jong-Seong Bae Taehyun Park Il Tae Kim Jaehyun Hur School of Chemical Biological and Battery Engineering Gachon University Seongnam Busan Center Korea Basic Science Institute

Aqueous Zn-ion batteries （AZIBs） have received considerable attention owing to their various advantages such as safety,low cost,simple battery assembly conditions,and high ionic ***,they still suffer from serious problems,including uncontrollable dendrite growth,corrosion,hydrogen evolution reaction （HER） from water decomposition,electrode passivation,and unexpected *** creation of a uniform artificial nanocrystal layer on the Zn anode surface is a promising strategy for resolving these ***,we propose the use of a perovskite CaTiO3（CTO） protective layer on Zn（CTO@Zn） as a promising approach for improving the performance of *** CTO artificial layer provides an efficient pathway for Zn ion diffusion towards the Zn metal because of the high dielectric constant （εr=180） and ferroelectric characteristics that enable the alignment of dipole moments and redistribute the Zn2+ions in the CTO *** avoiding the direct contact of the Zn anode with the electrolyte solution,the uneven dendrite growth,corrosion,parasitic side reactions,and HER are mitigated,while CTO retains its mechanical and chemical robustness during ***,CTO@Zn demonstrates an improved lifespan in a symmetric cell configuration compared with bare ***@Zn shows steady overpotential （～68 m V） for 1500 h at 1 mA cm-2/0.5 mA h cm-2,excelling bare ***,when paired with the V2O5-C cathode,the CTO@Zn//V2O5-C full battery delivers 148.4 mA h g-1（based on the mass of the cathode） after 300 *** study provides new insights into Zn metal anodes and the development of high-performance AZIBs.

关键词： Artificial layer Dielectric constant Zn metal anode Zinc aqueous battery

EFFICIENT ESTIMATION OF SEEMINGLY UNRELATED ADDITIVE NONPARAMETRIC REGRESSION MODELS

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Journal of Systems Science & Complexity 2013年第4期26卷 595-608页

作者： YUAN Yuan you Jinhong ZHOU yong School of Statistics and Management Shanghai University of Finance and Economics Academy of Mathematics and Systems Science Chinese Academy of Sciences

This paper is concerned with the estimating problem of seemingly unrelated(SU)nonparametric additive regression models.A polynomial spline based two-stage efficient approach is proposed to estimate the nonparametric components,which takes both of the additive structure and correlation between equations into *** asymptotic normality of the derived estimators are *** authors also show they own some advantages,including they are asymptotically more efficient than those based on only the individual regression equation and have an oracle property,which is the asymptotic distribution of each additive component is the same as it would be if the other components were known with *** simulation studies are conducted to illustrate the finite sample performance of the proposed *** the proposed procedure to a real data set is also made.

关键词： Additive structure asymptotic normality nonparametric modelling polynomial spline seemingly unrelated regression two-stage estimation.

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喷印金属微滴撞击粗糙表面的分子动力学模拟

原子与分子物理学报 2025年第4期42卷 73-80页

作者：苏仁健陈小勇游自浩桂林电子科技大学机电工程学院桂林541004 广西制造系统与先进制造技术重点实验室桂林541004

研究金属微滴撞击固体表面的行为对预测微滴形态和实现高精度的喷印制造具有重要的意义.然而,由于微纳尺度下金属微滴撞击实验的难以开展,目前涉及金属微滴撞击粗糙表面的形态变化和热毛细效应机理尚不清楚.本文采用分子动力学模拟研究... 详细信息

研究金属微滴撞击固体表面的行为对预测微滴形态和实现高精度的喷印制造具有重要的意义.然而,由于微纳尺度下金属微滴撞击实验的难以开展,目前涉及金属微滴撞击粗糙表面的形态变化和热毛细效应机理尚不清楚.本文采用分子动力学模拟研究了镓铟微滴撞击粗糙表面的动态行为,定量分析了撞击速度、粗糙结构和不同温度对微滴撞击行为的影响.结果表明:随着撞击速度的提高,微滴先后呈现沉积、弹跳和破碎飞溅三种模式,且微滴的最大铺展因子与韦伯数呈幂函数关系.此外,通过修饰基底粗糙结构发现,结构间距或高度的变化对微滴的弹跳行为存在不同的影响机制,可以有效促使或抑制微滴的弹跳行为.最后,分析得出随着温度的提高,微滴的铺展直径会变大,产生的黏性耗散也会增大.研究结果对金属微滴撞击行为的有效预测提供了理论基础.

关键词：金属微滴撞击粗糙基底分子动力学

Fracture mechanism of a laminated aluminum alloy plate during ballistic impact

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Rare Metals 2017年第9期36卷 737-745页

作者： Ming-Yuan Li Bai-Qing Xiong Guo-Jun Wang you-zhi Tong Xi-Wu Li Shu-Hui Huang zhi-Hui Li yong-An Zhang State Key Laboratory of Nonferrous Metals and Processes General Research Institute for Nonferrous MetalsBeijing 100088China Northeast Light Alloy Co. Ltd.Harbin 150060China

The multilayered 7XXX series aluminum alloy was impacted by 7.62 mm ogival projectiles at velocities ranging from 787 to 851m·s^（-1）. The deformed microstructure under various impacting velocities and fracture surfaces of different sections were investigated at different physical scales to determine the process of *** microscopy（OM）,electron back-scattered diffraction（EBSD） and scanning electron microscopy（SEM） were used in the investigation. The results show that crater is constrained in the 7B52 front layer and two types of adiabatic shear bands which are transformed bands and deformed bands and different types of cracks are *** fracture is the significant failure mode of 7B52 front layer, and the resulting delamination leads to the presence of bending tensile fracture instead of the shear *** ductile 7A01 layer blunts and deflects the spall crack tips, preventing the targets from full spall, and induces a constraint of 7A52 rear layer. The level of the constraint determines different fracture modes of 7A52 layer,accounting for the asymmetry of damage.

关键词： Laminate Aluminum Ballistic impact Spallfracture Adiabatic shear bands