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Reactive destabilization and bidirectional catalyzation for reversible hydrogen storage of liBH_(4) by novel waxberry-like nano-additive assembled from ultrafine Fe_(3)O_(4) particles

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Journal of materials science & technology 2024年第6期173卷 63-71页

作者： S.wang M.H.Wu Y.Y.zhu z.l.li Y.X.Yang Y.z.l. H.F.liu M.X.gao Department of Material science Shenzhen MSU-BIT UniversityShenzhen 518172China State Key laboratory of Silicon and Advanced Semiconductor materials&school of materials science and engineering Zhejiang UniversityHangzhou 310027China institute of Resources Utilization and Rare earth Development State Key Laboratory of Rare Metals Separation and Comprehensive UtilizationGuangdong Provincial Key Laboratory of Rare Earth Development and ApplicationGuangdong Academy of SciencesGuangzhou 510650China institute of science and technology for New energy Xi’an Technological UniversityXi’an 710021China National Supercomputing Center in Shenzhen Shenzhen 518055China

liBH_(4) containing 18.5 wt.%H_(2) is an attractive high-capacity hydrogen storage material,however,it suffers from high operation temperature and poor ***,a novel and low-cost bifunctional additive,waxberry-like Fe_(3)O_(4) secondary nanospheres assembled from ultrafine primary Fe_(3)O_(4) nanoparticles,is synthesized,which exhibits significant destabilization and bidirectional catalyzation towards(de)hydrogenation of liBH_(4).With an optimized addition of 30 wt.% waxberry-like Fe_(3)O_(4),the system initiated dehydrogenation below 100℃ and released a total of 8.1 wt.%H_(2) to 400℃.After 10 cycles,a capacity retention of 70% was achieved,greatly superior to previously reported oxides-modified *** destabilizing and catalyzing mechanisms of waxberry-like Fe_(3)O_(4) on liBH_(4) were systematically analyzed by phase and microstructural evolutions during dehydrogenation and hydrogenation cycling as well as density functional theory(DFT)*** present work provides new insights in developing advanced nano-additives with unique structural and multifunctional designs towards liBH4 hydrogen storage.

关键词： liBH_(4) Hydrogen storage Waxberry-like Fe_(3)O_(4) Destabilization Catalysis

experimental determination of the Young’s modulus of individual single-walled carbon nanotubes with single chirality

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Nano Research 2024年第8期17卷 7522-7532页

作者： Jianlin Sun Xiao zhang Yanchun wang Mingming li Xiaojun Wei Huaping liu Weiya zhou Beijing National laboratory for Condensed Matter Physics and Institute of PhysicsChinese Academy of SciencesBeijing 100190China school of Physical sciences and College of materials science and Optoelectronic technology University of Chinese Academy of SciencesBeijing 100049China Songshan lake materials laboratory Dongguan 523808China Beijing Key laboratory for Advanced Functional materials and Structure Research Beijing 100190China

One-dimensional carbon nanotube(CNT)exhibits excellent mechanical properties and is considered to be an ideal candidate material for the space ***,subtle changes in its chirality strongly affect its physical and chemical properties,including mechanical properties(such as Young's modulus,YM).Theoretical studies reveal that the YMs of perfect single-walled carbon nanotubes(SWCNTs)are in the order of TPa and related to their ***,due to the lack of SWCNTs samples with well-defined structures and the difficulties in mechanical tests on individual SWCNTs,the theoretical correlations between YM and structure of SWCNTs have not been verified and are still in debate,which directly influences the practical utilization of the excellent mechanical properties of *** this work,we have developed an experimental method to measure the YM of an individual micrometer-scale suspended CNT by atomic force microscopy.A distinct regularity is found between the YM and chirality(i.e.,chiral angle and diameter)of SWCNT in the experiment for the first *** comparing the YMs of SWCNTs with similar diameters and different chiral angles,it manifests that the SWCNT with a near zigzag configuration has a larger *** finding suggests that the effect of SWCNT’s structures on the YMs cannot be *** developed method of measuring YMs of SWCNTs will be valuable for further experimental research on the inherent physical and chemical properties of SWCNTs.

关键词： Young's modulus single-walled carbon nanotubes single chirality atomic force microscopy

Dynamically lithium-compensated polymer artificial SeI to assist highly stable lithium-rich manganese-based anode-free lithium metal batteries

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Rare Metals 2024年第6期43卷 2527-2535页

作者： Ming-Ji Peng Jin-Qiu zhou Ting-Ting Han Yang zhou Jie liu Na Xu zhen-Kang wang Wen-Bin lin Cheng-lin Yan Key laboratory of Core technology of High Specific energy Battery and Key materials for Petroleum and Chemical Industry College of EnergySoochow UniversitySuzhou 215006China light Industry instituteof electrochemical Power Sources Suzhou 215006China school of Chemistry and Chemical engineering Nantong UniversityNantong 226019China e-mail:jliu93@*** State Key laboratory of Space Power-Sources technology Shanghai Institute of Space Power-SourcesShanghai 200245China Centre energie Materiaux et TélécommunicationsInstitut National de la Recherche ScientifiqueVarennesQC J3X 1S2Canada zhangjiagang Industrial Technologies Soochow UniversitySuzhou 215006China

Owing to the unique structure,anode-free lithium metal batteries(AFlMBs)have higher energy density and lower production cost than traditional lithium metal batteries(lMBs)or lithium-ion batteries(lIBs),However,AFlMBs suffer from an inherently finite li reservoir and exhibit poor cycle stability,low Coulombic efficiency(Ce)and severe dendrite *** this work,polydiallyl lithium disulfide(PDS-li)was successfully synthesized and coated on Cu current collector by electrochemical *** PDS-li acts as an additional lithium resource to compensate for the irreversible loss of lithium during *** addition,the special structure and lithiophilicity of PDS-li contribute to lower nucleation overpotential and uniform lithium *** coupled with li-rich manganese-based(lRM)cathode of li1.2Mn0.54Ni0.13Co0.13O2,the anode-free full cell exhibits significantly improved cycle stability over 100 cycles and capacity retention of 63.3%and 57%after 80 and 100 cycles,*** believe that PDS-li can be used to ensure stable cycling performance and high-energy-density in AFlMBs.

关键词： Anode-free Artificial solid electrolyte interphase(SeI) lithium metal batteries lithium-rich cathode Finite element simulation

evidence for particle acceleration approaching PeV energies in the W51 complex

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science Bulletin 2024年第18期69卷 2833-2841页

作者： lHAASO Collaboration zhen Cao F.Aharonian Axikegu Y.X.Bai Y.W.Bao D.Bastieri X.J.Bi Y.J.Bi W.Bian A.V.Bukevich Q.Cao W.Y.Cao zhe Cao J.Chang J.F.Chang A.M.Chen e.S.Chen H.X.Chen liang Chen lin Chen long Chen M.J.Chen M.l.Chen Q.H.Chen S.Chen S.H.Chen S.z.Chen T.l.Chen Y.Chen N.Cheng Y.D.Cheng M.Y.Cui S.W.Cui X.H.Cui Y.D.Cui B.z.Dai H.l.Dai z.G.Dai Danzengluobu X.Q.Dong K.K.Duan J.H.Fan Y.z.Fan J.Fang J.H.Fang K.Fang C.F.Feng H.Feng l.Feng S.H.Feng X.T.Feng Y.Feng Y.l.Feng S.gabici B.gao C.D.gao Q.gao W.gao W.K.gao M.M.Ge l.S.Geng G.Giacinti G.H.Gong Q.B.Gou M.H.Gu F.l.Guo X.l.Guo Y.Q.Guo Y.Y.Guo Y.A.Han M.Hasan H.H.He H.N.He J.Y.He Y.He Y.K.Hor B.W.Hou C.Hou X.Hou H.B.Hu Q.Hu S.C.Hu D.H.Huang T.Q.Huang W.J.Huang X.T.Huang X.Y.Huang Y.Huang X.l.Ji H.Y.Jia K.Jia K.Jiang X.W.Jiang z.J.Jiang M.Jin M.M.Kang I.Karpikov D.Kuleshov K.Kurinov B.B.li C.M.li Cheng li Cong li D.li F.li H.B.li H.C.li Jian li Jie li K.li S.D.li W.l.li W.l.li X.R.li Xin li Y.z.l. zhe li zhuo li e.W.liang Y.F.liang S.J.lin B.liu C.liu D.liu D.B.liu H.liu H.D.liu J.liu J.l.liu M.Y.liu R.Y.liu S.M.liu W.liu Y.liu Y.N.liu Q.luo Y.luo H.K.lv B.Q.Ma l.l.Ma X.H.Ma J.R.Mao z.Min W.Mitthumsiri H.J.Mu Y.C.Nan A.Neronov l.J.Ou P.Pattarakijwanich z.Y.Pei J.C.Qi M.Y.Qi B.Q.Qiao J.J.Qin A.Raza D.Ruffolo A.Sáiz M.Saeed D.Semikoz.l.Shao O.Shchegolev X.D.Sheng F.W.Shu H.C.Song Yu.V.Stenkin V.Stepanov Y.Su D.X.Sun Q.N.Sun X.N.Sun z.B.Sun J.Takata P.H.T.Tam Q.W.Tang R.Tang z.B.Tang W.W.Tian C.wang C.B.wang G.W.wang H.G.wang H.H.wang J.C.wang Kai wang Kai wang l.P.wang l.Y.wang P.H.wang R.wang W.wang X.G.wang X.Y.wang Y.wang Y.D.wang Y.J.wang z.H.wang z.X.wang zhen wang zheng wang D.M.Wei J.J.Wei Y.J.Wei T.Wen C.Y.Wu H.R.Wu Q.W.Wu S.Wu X.F.Wu Y.S.Wu S.Q.Xi J.Xia G.M.Xiang D.X.Xiao G.Xiao Y.l.Xin Y.Xing D.R.Xiong z.Xiong D.l.Xu R.F.Xu R.X.Xu W.l.Xu l.Xue D.H.Yan J.z.Yan T.Yan C.W.Yang C.Y.Yang F.Yang F.F.Yang l.l.Yang M.J.Yang R.z.Yang W.X.Yang Y.H.Yao z.G.Yao l.Q.Yin N.Yin X.H.You z.Y.You Y.H.Yu Q.Yuan H.Yue H.D.zeng T.X.zeng W.zeng M.zha B.B.zhang F.zhang H.zhang 不详 Key laboratory of Particle Astrophysics&experimental Physics Division&Computing Center Institute of High Energy PhysicsChinese Academy of SciencesBeijing 100049China University of Chinese Academy of sciences Beijing 100049China TIANFU Cosmic Ray Research Center ChengduChina Dublin institute for Advanced Studies 31 Fitzwilliam Place2 DublinIreland Max-Planck-Institut for Nuclear Physics P.O.Box 103980Heidelberg 69029Germany school of Physical science and technology&school of Information science and technology Southwest Jiaotong UniversityChengdu 610031China school of Astronomy and Space science Nanjing UniversityNanjing 210023China Center for Astrophysics Guangzhou UniversityGuangzhou 510006China Tsung-Dao lee institute&school of Physics and Astronomy Shanghai Jiao Tong UniversityShanghai 200240China institute for Nuclear Research of Russian Academy of sciences Moscow 117312Russia Hebei Normal University Shijiazhuang 050024China University of science and technology of China Hefei 230026China State Key laboratory of Particle Detection and electronics China Key laboratory of Dark Matter and Space Astronomy&Key laboratory of Radio Astronomy Purple Mountain ObservatoryChinese Academy of SciencesNanjing 210023China Research Center for Astronomical Computing Zhejiang LaboratoryHangzhou 311121China Key laboratory for Research in galaxies and Cosmology Shanghai Astronomical ObservatoryChinese Academy of SciencesShanghai 200030China school of Physics and Astronomy Yunnan UniversityKunming 650091China Key laboratory of Cosmic Rays(Tibet University) Ministry of EducationLhasa 850000China National Astronomical Observatories Chinese Academy of SciencesBeijing 100101China school of Physics and Astronomy(zhuhai)&school of Physics(Guangzhou)&Sino-French institute of Nuclear engineering and technology(zhuhai) Sun Yat-sen UniversityZhuhai 519000&Guangzhou 510275GuangdongChina institute of Frontier and Interdisciplinary science Shandong UniversityQingdao 266237China APC UniversitéParis Cité

Theγ-ray emission from the W51 complex is widely acknowledged to be attributed to the interaction between the cosmic rays(CRs)accelerated by the shock of supernova remnant(SNR)W51C and the dense molecular clouds in the adjacent star-forming region,***,the maximum acceleration capability of W51C for CRs remains *** on observations conducted with the large High Altitude Air Shower Observatory(lHAASO),we report a significant detection ofγrays emanating from the W51 complex,with energies from 2 to 200 *** lHAASO measurements,for the first time,extend theγ-ray emission from the W51 complex beyond 100 TeV and reveal a significant spectrum bending at tens of *** combining the"π^(0)-decay bump"featured data from Fermi-lAT,the broadbandγ-ray spectrum of the W51 region can be well-characterized by a simple pp-collision *** observed spectral bending feature suggests an exponential cutoff at~400 TeV or a power-law break at~200 TeV in the CR proton spectrum,most likely providing the first evidence of SNRs serving as CR accelerators approaching the PeV ***,two young star clusters within W51B could also be theoretically viable to produce the most energeticγrays observed by *** findings strongly support the presence of extreme CR accelerators within the W51 complex and provide new insights into the origin of galactic CRs.

关键词： UHe c-ray Cosmic rays SNR W51C Star clusters

Synergetic deformation mechanisms in an Mg-zn-Y-zr alloy with intragranular lPSO structures

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Journal of Magnesium and Alloys 2023年第5期11卷 1754-1768页

作者： z.z.Peng X.H.Shao z.M.liang D.l.wang l.W.wang X.l.Ma Hebei Key laboratory of Material Near-Net Forming technology School of Materials Science and EngineeringHebei University of Science and TechnologyShijiazhuang 050018China Shenyang National laboratory for materials science Institute of Metal ResearchChinese Academy of Sciences72 Whenua RoadShenyang 110016China

Deformation kink is one of the important strengthening mechanisms of the long-period-stacking-ordered(lPSO)phase containing magnesium(Mg)alloys,while the deformation twin is generally *** optimize the mechanical properties of lPSO containing Mg alloy by simultaneously exciting kink and twin,we successfully prepared the Mg-zn-Y-zr alloy featuring intragranular lPSO phase and free grain boundary lPSO phase by *** unraveled the corresponding strengthening and toughening mechanisms through transmission electron microscopy characterization and theoretical *** high strength and good plasticity of the homogenized alloy benefit from the synergistic deformation mechanism of multiple kinking and twining in the *** the activation of kinking and twinning depends on the thicknesses of lPSO lamellae and their relative *** results may shed light on optimizing the design of Mg alloys regulating the microstructure of lPSO phases.

关键词： Mg alloy lPSO distribution Kink Twin Transmission electron microscopy

Optimization of performance of the KM2A full array using the Crab Nebula

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Chinese Physics C 2024年第6期48卷 169-178页

作者：曹臻 F.Aharonian 安琪阿西克古白云翔包逸炜 D.Bastieri 毕效军毕玉江蔡金庭曹晴曹文羽曹喆常进常劲帆陈尚明陈恩生陈亮陈林陈龙陈明君陈玛丽陈起辉陈素弘陈天禄陈阳程宁程耀东崔明阳崔树旺崔晓红崔昱东戴本忠代洪亮戴子高单增罗布 D.della Volpe 董绪强段凯凯樊军辉范一中方军方堃冯存峰封莉冯少辉丰晓婷冯有亮 S.gabici 高博高川东高林青高启高卫高伟康葛茂茂耿利斯 G.Giacinti 龚光华苟全补顾旻皓郭福来郭晓磊郭义庆郭莹莹韩毅昂何会海贺昊宁何佳银何新波何钰 M.Heller 贺远强侯博文侯超侯贤胡红波胡铨胡世聪黄代绘黄天奇黄文俊黄性涛黄晓渊黄勇黄志成季筱璐贾焕玉贾康江琨姜晓巍姜泽军金敏康明铭柯通 D.Kuleshov.K.Kurinov 李兵兵李澄李骢李丹李飞李海波李会财李华阳李军李剑李捷李凯李文龙李文莲李秀荣李昕李一卓李哲黎卓梁恩维梁云峰林苏杰刘冰刘成刘栋刘虎刘海东刘佳刘江来刘金艳刘茂元柳若愚刘四明刘伟刘怡刘以农鲁睿罗晴吕洪魁马伯强马玲玲马欣华毛基荣闵振 W.Mitthumsiri 穆慧君南云程 A.Neronov 区子维庞彬宇 P.Pattarakijwanich 裴致远齐孟尧祁业情乔冰强秦家军 D.Ruffolo A.Sáiz D.Semikoz 邵澄宇邵琅 O.Shchegolev 盛祥东舒富文宋慧超 Yu.V.Stenkin V.Stepanov 苏扬孙秦宁孙晓娜孙志斌谭柏轩唐庆文唐泽波田文武王超王昌贝王广威王洪光王惠惠王建成汪凯王利苹王玲玉王培汉王冉王为王祥高王祥玉王阳王玉东王岩谨王忠海王仲翔王振王铮韦大明魏俊杰魏永健文韬吴超勇吴含荣武莎吴雪峰吴雨生席邵强夏捷夏君集项光漫肖迪泫肖刚辛广广辛玉良邢祎熊峥徐东莲徐仁峰徐仁新徐伟立薛良闫大海颜景志颜田杨朝文杨帆杨冯帆杨何文杨佳盈杨莉莉杨明洁杨睿智杨深邦姚玉华姚志国叶一锰尹丽巧尹娜游晓浩游智勇于艳红袁强岳华曾厚敦曾婷轩曾玮查敏张彬彬张丰张海明张恒英张建立张丽霞张力张鹏飞张佩佩张瑞张少博张少如张寿山张潇张笑鹏张云峰张毅张勇赵兵赵静赵雷赵立志赵世平郑福周斌周浩周佳能周猛周平周荣周勋秀祝成光祝凤荣朱辉朱科军左雄 lHAASO Collaboration Key laboratory of Particle Astrophyics&experimental Physics Division&Computing Center Institute of High Energy PhysicsChinese Academy of SciencesBeijing 100049China University of Chinese Academy of sciences Beijing 100049China Tianfu Cosmic Ray Research Center Chengdu 610000China Dublin institute for Advanced Studies 31 Fitzwilliam Place2 DublinIreland Max-Planck-Institut for Nuclear Physics P.O.Box 10398069029 HeidelbergGermany State Key laboratory of Particle Detection and electronics China University of science and technology of China Hefei 230026China school of Physical science and technology&school of Information science and technology Southwest Jiaotong UniversityChengdu 610031China school of Astronomy and Space science Nanjing UniversityNanjing 210023China Center for Astrophysics Guangzhou UniversityGuangzhou 510006China Hebei Normal University Shijiazhuang 050024China Key laboratory of Dark Matter and Space Astronomy&Key laboratory of Radio Astronomy Purple Mountain ObservatoryChinese Academy of SciencesNanjing 210023China Tsung-Dao lee institute&school of Physics and Astronomy Shanghai Jiao Tong UniversityShanghai 200240China Key laboratory for Research in galaxies and Cosmology Shanghai Astronomical ObservatoryChinese Academy of SciencesShanghai 200030China Key laboratory of Cosmic Rays(Tibet University) Ministry of EducationLhasa 850000TibetChina National Astronomical Observatories Chinese Academy of SciencesBeijing 100101China school of Physics and Astronomy(zhuhai)&school of Physics(Guangzhou)&Sino-French institute of Nuclear engineering and technology(zhuhai) Sun Yat-sen UniversityZhuhai 519000&Guangzhou 510275China school of Physics and Astronomy Yunnan UniversityKunming 650091China Département de Physique Nucléaire et Corpusculaire Facultéde SciencesUniversitéde Genève24 Quai Ernest Ansermet1211 GenevaSwitzerland institute of Frontier and Interdisciplinary science Shandong UniversityQingdao 266237China APC Universit'e Paris Cit'eCNRS/IN2P3CEA/IRFUObservat

The full array of the large High Altitude Air Shower Observatory(lHAASO)has been in operation since July *** its kilometer-square array(KM2A),we optimized the selection criteria for very high and ultrahigh energyγ-rays using data collected from August 2021 to August 2022,resulting in an improvement in significance of the detection in the Crab Nebula of approximately 15%,compared with that of previous *** the implementation of these new selection criteria,the angular resolution was also significantly improved by approximately 10%at tens of *** aspects of the full KM2A array performance,such as the pointing error,were also calibrated using the Crab *** resulting energy spectrum of the Crab Nebula in the energy range of 10-1000 TeV are well fitted by a log-parabola model,which is consistent with the previous results from lHAASO and other experiments.

关键词： γ-ray Crab Nebula significance

effect of grain size on fatigue cracking at twin boundaries in a CoCrFeMnNi high-entropy alloy

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Journal of materials science & technology 2020年第4期39卷 1-6页

作者： A.G.wang X.H.An J.Gu X.G.wang l.l.li W.l.li M.Song Q.Q.Duan z.F.zhang X.z.l.ao school of Aerospace Mechanical&Mechatronic EngineeringThe University of Sydne0ySydneyAustralia State Key laboratory of Powder Metallurgy Central South UniversityChangsha 410083China materials Fatigue and Fracture Division Institute of Metal ResearchChinese Academy of SciencesShenyang 110016China Max-Planck-Institut für eisenforschung Max-Planck-Stra?e 140237 DüsseldorfGermany

The fatigue cracking behavior at twin boundaries(TBs)in a Co Cr Fe Mn Ni high-entropy alloy with three different grain sizes was systematically investigated under low-cycle *** of grain size,the change from slip band cracking to TB cracking occurred with increasing the difference in the Schmid factors(DSF)between matrix and ***,the required critical DSF for the transition of the dominant cracking mode decreases with decreasing grain size due to the reduced slip band spacing that increases the impingement sites on the TBs and facilitates the coalescence of defects and voids to initiate TB cracks.

关键词： High-entropy alloy Fatigue cracking Twin boundary Slip band Grain size

Comprehensive insights into the thermal and mechanical effects of metallic glasses via creep

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Journal of materials science & technology 2022年第4期99卷 39-47页

作者： z.R.Xu J.C.Qiao J.wang e.Pineda D.Crespo school of Mechanics Civil Engineering and ArchitectureNorthwestern PolytechnicalUniversityXi’an 710072China State Key laboratory of Solidification Processing Northwestern PolytechnicalUniversityXi’an 710072China Department of Physics Barcelona Research Center in Multiscale Science and TechnologyInstitute of Energy TechnologiesUniversitat Politècnica de CatalunyaBarcelona 08019Spain

evolution of deformation and relaxation behaviors of a prototypical Cu_(46)zr_(46)A_(l8)metallic glass was explored by extensive creep tests under both physical aging and cyclic *** insights into the microstructure-induced dynamic heterogeneity which accommodates creep deformation were successively revealed via experimental measurements and spectral *** annihilation of local defects within metallic glass with increasing annealing time and cyclic numbers was observed through the reduction of amplitude in both activation energy spectra and relaxation-time spectra,which were also accompanied by an ascending value of β_(KWW).It is further found that the corresponding deformation units within the metallic glass do not disappear permanently,but are recoverable over the course of cyclic *** apparent suppressed relaxation process can be gradually alleviated with increasing resuming time between two consecutive cycles,behaving differently from physical aging,which indicates a notable discrepancy between thermal treatment and mechanical treatment.

关键词： Metallic glasses Creep Physical aging Cyclic loading Relaxation-time spectrum

A method for analyzing on-line video images of crystallization at high-solid concentrations

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Particuology 2008年第1期6卷 9-15页

作者： Jian Wan Cai Y. Ma Xue z. wang institute of Particle science and engineering School of Process Environmental and Materials Engineering University of Leeds Leeds LS2 9JT UK

Recent research has demonstrated that on-line video imaging is a very promising technique for monitoring crystallization processes. The bottleneck in applying the technique for real-time closed-loop control is considered as image analysis that needs to be robust, fast and able to handle varied image qualities due to temporal variations of operating conditions such as mixing and solid concentrations. Image analysis at highsolid concentrations turns out to be extremely challenging because crystals tend to overlap or attach to each other and the boundaries between the crystals are usually ambiguous. This paper presents an image segmentation algorithm that can effectively deal with images taken at high-solid concentrations. The method segments crystals attached to each other along the mostly related concave points on the contours of crystal blocks. The detailed procedure is introduced with application to crystallization of l-glutamic acid in a hot-stage reactor.

关键词： Crystallization High-solid concentrations Image processing Multi-scale segmentation Watershed segmentation Crystal size distribution