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RF magnetron-sputtered coatings deposited from biphasic calcium phosphate targets for biomedical implant applications

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Bioactive Materials 2017年第3期2卷 170-176页

作者： K.A.prosolov K.S.popova O.A.Belyavskaya J.V.Rau K.A.Gross A.Ubelis yu.p.sharkeev Institute of Strength physics and Materials Science of SB RAS TomskAcademicheskii pr.2/4634055Russia National Research Tomsk polytechnic University TomskLenina pr.30634050Russia Istituto di Struttura della Materia Consiglio Nazionale delle Ricerche(ISM-CNR)via del Fosso del Cavaliere 10000133RomaItaly Faculty of Materials Science and Applied Chemistry Riga Technical UniversityAzenes Str.14/24RigaLV-1048Latvia University of Latvia 19Raina blvd.RigaLV-1586Latvia

Bioactive calcium phosphate coatings were deposited by radio-frequency magnetron sputtering from biphasic targets of hydroxyapatite and tricalcium phosphate,sintered at different mass%*** to Raman scattering and X-ray diffraction data,the deposited hydroxyapatite coatings have a disordered ***-temperature treatment of the coatings in air leads to a transformation of the quasi-amorphous structure into a crystalline one.A correlation has been observed between the increase in the Ca content in the coatings and a subsequent decrease in Ca in the biphasic targets after a series of deposition *** was proposed that the addition of tricalcium phosphate to the targets would led to a finer coating's surface topography with the average size of 78 nm for the structural elements.

关键词： RF-magnetron sputtering Biphasic hydroxyapatite-tricalcium phosphate targets Thin hydroxyapatite coatings plasma coatings Biocompatibility

Comparative investigations of structure and properties of micro-arc wollastonite-calcium phosphate coatings on titanium and zirconiumniobium alloy

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Bioactive Materials 2017年第3期2卷 177-184页

作者： M.B.Sedelnikova E.G.Komarova yu.p.sharkeev T.V.Tolkacheva I.A.Khlusov L.S.Litvinova K.A.yurova V.V.Shupletsova Institute of Strength physics and Materials Science of SB RAS Academicheskii pr.2/4634055TomskRussia National Research Tomsk polytechnic University Lenina pr.30634050TomskRussia Siberian State Medical University 2 Moskovsky tr.634050TomskRussia Immanuel Kant Baltic Federal University 14 A.Nevskogo st.236041KaliningradRussia

Investigation results of micro-arc wollastoniteecalcium phosphate(W-Cap)biocoatings on the pure titanium(Ti)and Zr-1wt.%Nb(Zr-1Nb)alloy were *** voltages of 150-300 V generate the micro-arc oxidation(MAO)process with the initial amplitude current of 150-550 A and 100-350 A for Ti and Zr-1Nb substrates,*** identical dependencies of changes of the coating thickness,surface roughness and adhesion strength on the process voltage were revealed for the both *** W-Cap coatings with the thickness of 10-11μm were formed on Ti and Zr-1Nb under the low process voltage of 130-150 *** wollastonite particles with the size in the range of 40-100μm were observed in such *** structure of the coatings on Ti was presented by the X-ray amorphous and crystalline *** X-ray reflexes relating to the crystalline phases of Ti and wollastonite were observed only in XRD patterns of the coatings deposited under 130-200 V on ***,the crystalline structure with phases of CaZr4(pO4)6,β-Zrp2O7,ZrO2,and Zr was detected in the coatings on ***-IRS,XRD,SEM,and TEM data confirmed that the increase of the process voltage to 300 V leads to the dissociation of the *** toxic effect of specimens on a viability,morphology and motility of human adipose-derived multipotent mesenchymal stem cells was revealed in vitro.

关键词： Micro-arc oxidation Biocoatings Calcium phosphate Wollastonite

palladium-catalyzed S_(N)2 glycosylation of phenols

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Science China Chemistry 2024年第4期67卷 1037-1038页

作者： yu Zhu p.Andrew Evans Department of Chemistry Queen’s University90 Bader LaneKingstonK7L 3N6Canada Xiangya School of pharmaceutical Sciences Central South UniversityChangsha 410013China

Glycosides are essential structural motifs present in an array of important medicines,materials,and natural products[1].Nevertheless,the chemo-and stereoselective construction of the glycosidic linkage is a long-standing challenge because relatively minor variations in the glycosyl donor or acceptor’s structure can impact stereoselectivity,thus influencing the product's functional properties.

关键词： properties palladium catalyzed

Linear-Quadratic pareto Cooperative Game for Mean-Field Backward Stochastic System

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Journal of Systems Science & Complexity 2024年第3期37卷 947-964页

作者： WANG yu School of Control Science and Engineering Shandong UniversityJinan 250061China

This paper focuses on a pareto cooperative differential game with a linear mean-field backward stochastic system and a quadratic form cost functional. Based on a weighted sum optimality method, the pareto game is equivalently converted to an optimal control problem. In the first place,the feedback form of pareto optimal strategy is derived by virtue of decoupling technology, which is represented by four Riccati equations, a mean-field forward stochastic differential equation(MF-FSDE),and a mean-field backward stochastic differential equation(MF-BSDE). In addition, the corresponding pareto optimal solution is further obtained. Finally, the author solves a problem in mathematical finance to illustrate the application of the theoretical results.

关键词： Backward stochastic differential equation linear-quadratic control mean-field pareto optimality

Novel umami peptides from two Termitomyces mushrooms and molecular docking to the taste receptor T1R1/T1R3

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Food Science and Human Wellness 2024年第2期13卷 1055-1064页

作者： Lanyun Zhang Li Zhang Jesus pérez-Moreno Lu Bin Fengming Zhang Fuqiang yu The Germplasm Bank of Wild Species Yunnan Key Laboratory for Fungal Diversity and Green DevelopmentKunming Institute of BotanyChinese Academy of SciencesKunming 650201China College of Chemical Science and Technology Yunnan UniversityKunming 650091China College of Food Science and Technology Yunnan Agricultural UniversityKunming 650201China Colegio postgraduados Campus MontecilloEdafologíaTexcoco 56230México Key Laboratory for Forest Resources Conservation and Use in the Southwest Mountains of China Southwest Forestry UniversityKunming 650224China

Wild edible Termitomyces mushrooms are popular in Southwest China and umami is important flavor qualities of edible *** study aimed to understand the umami taste of Termitomyces intermedius and Termitomyces *** umami peptides from aqueous extracts were separated using a Sephadex G-15 gel filtration *** intense umami fraction was evaluated by both sensory evaluation and electronic *** were identified as KLNDAQApK,DSTDEKFLR,VGKGAHLSGEH,MLKKKKLA,SLGFGGppGY,TVATFSSSTKpDD,AMDDDEADLLLLAM,VEDEDEKpKEK,SpEEKKEEET and *** peptides,except VEDEDEKpKEK,SpEEKKEEET and pEGADKpNK were selectively synthesized to verify their taste *** these 10 peptides had umami or salt *** 10 peptides were conducted by molecular docking to study their interaction with identified peptides and the umami taste receptor T1R1/*** these 10 peptides perfectly docked the active residues in the T1R3 *** results provide theoretical basis for the umami taste and address the umami mechanism of two wild edible Termitomyces mushrooms.

关键词： Termitomyces Non-volatile flavor compounds Umami peptides Taste characteristics Molecular docking

Approximate analytical solutions for threedimensional ascent trajectory of a solid-fuel launch vehicle with time-varying mass flow rate

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Chinese Journal of Aeronautics 2024年第10期37卷 275-293页

作者： Qi yu Wanchun CHEN Wenbin yu School of Astronautics Beihang UniversityBeijing 102206China

In the scenario that a solid-fuel launch vehicle maneuvers in outer space at high angles of attack and sideslip for energy management,Approximate Analytical Solutions(AAS)for the threedimensional(3D)ascent flight states are derived,which are the only solutions capable of considering time-varying Mass Flow Rate(MFR)at *** uneven MFR makes the thrust vary nonlinearly and thus increases the difficulty of the problem *** AAS are derived based on a 3D Generalized Ascent Dynamics Model(GADM)with a normalized mass as the independent *** simplify some highly nonlinear terms in the GADM,several approximate functions are introduced carefully,while the errors of the approximations relative to the original terms are regarded as minor ***,a finite series with positive and negative exponents,called Exponent-Symmetry Series(ESS),is proposed for function approximation to decrease the highest exponent in the AAS so as to reduce computer round-off *** calculate the ESS coefficients,a method of seeking the Optimal Interpolation points(OIp)is proposed using the leastsquares-approximation *** to the artful design of the approximations,the GADM can be decomposed into two analytically solvable subsystems by a perturbation method,and thus the AAS are obtained ***,to help implement the AAS,two indirect methods for measuring the remaining mass and predicting the burnout time in flight are put forward using information from *** results verify the superiority of the AAS under the condition of time-varying MFR.

关键词： Approximate analytical solutions 3D ascent trajectory Solid-fuel launch vehicle Uneven thrust Energy management

Low-melting mixture solvents: extension of deep eutectic solvents and ionic liquids for broadening green solvents and green chemistry

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Green Chemical Engineering 2024年第4期5卷 409-417页

作者： yu Chen Zhiwu yu MOE Key Laboratory of Bioorganic phosphorous Chemistry and Chemical Biology Department of ChemistryTsinghua University

Green solvents such as water and ionic liquids(ILs) are pillars of the great mansion of green chemistry and green processing. Initially proposed as a new family of ILs,deep eutectic solvents(DESs) have received fast development in the past two decades. In this contribution,DESs are reviewed critically and the concept is extended to lowmelting mixture solvents(Lo MMSs),which cover all kinds of materials including ionic compounds,molecular compounds,and metals. Six classes of Lo MMSs are proposed as the new classification system and examples are given. Finally,several thermodynamic issues concerning Lo MMSs are discussed. Two new concepts,robustness of Lo MMSs and high-entropy Lo MMSs,are proposed.

关键词： Green solvents Deep eutectic solvents Low transition temperature mixture solvents phase diagram EGaIn

Topological Stability and Entropy for Certain Set-valued Maps

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Acta Mathematica Sinica,English Series 2024年第4期40卷 962-984页

作者： yu ZHANG yu Jun ZHU School of Mathematical Sciences Xiamen UniversityXiamen 361005P.R.China

In this paper,the dynamics(including shadowing property,expansiveness,topological stability and entropy)of several types of upper semi-continuous set-valued maps are mainly considered from differentiable dynamical systems points of *** is shown that(1)if f is a hyperbolic endomorphism then for eachε>0 there exists a C^(1)-neighborhood U of f such that the induced set-valued map F_(f,U)has theε-shadowing property,and moreover,if f is an expanding endomorphism then there exists a C^(1)-neighborhood U of f such that the induced set-valued map F_(f,U)has the Lipschitz shadowing property;(2)when a set-valued map F is generated by finite expanding endomorphisms,it has the shadowing property,and moreover,if the collection of the generators has no coincidence point then F is expansive and hence is topologically stable;(3)if f is an expanding endomorphism then for eachε>0 there exists a C^(1)-neighborhood U of f such that h(F_(f,U,ε))=h(f);(4)when F is generated by finite expanding endomorphisms with no coincidence point,the entropy formula of F is ***,the dynamics of the set-valued maps based on discontinuous maps on the interval are also considered.

关键词： Set-valued map orbit space hyperbolic endomorphism perturbation shadowing expansiveness topological stability entropy

A new liquid membrane diffusion model for characterizing the adsorption kinetics of europium by using a continuous measurement of adsorption platform

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Nuclear Science and Techniques 2024年第1期35卷 59-72页

作者： Hao-Qi yu Tao yu Jian-Hua Ye State Key Laboratory of Nuclear Resources and Environment East China University of TechnologyNanchang 330013China CGN Cangnan Nuclear power Co. Ltd.Cangnan 325800China Jiangxi province Key Laboratory of polymer Micro/Nano Manufacturing and Devices East China University of TechnologyNanchang 330013China School of Nuclear Science and Engineering East China University of TechnologyNanchang 330013China

To explore the kinetic adsorption under continuous and nonequilibrium states, an integration of continuous measurement and adsorption platform kinetics method was proposed, which was initially called the ICM-Ap kinetics method, and a corresponding kinetic adsorption experimental method was developed. Adsorption experiments of europium(Eu) on Ca-bentonite,Na-bentonite, and the D231 cation exchange resin were performed using the ICM-Ap kinetics method and continuous measurements. Because the kinetic experimental results observed in this study were different from those of traditional batch adsorption data, pseudo-first-order or pseudo-second-order kinetic models were unsuitable for fitting the experimental ***, a liquid membrane diffusion(LMD) model was developed based on the assumption of simultaneous adsorption/desorption to discuss the mechanism of kinetic adsorption. The kinetic adsorption mechanism was also studied by using *** results indicated that the proposed adsorption model can fit the experimental data more suitably, and the adsorption/desorption behaviors of Eu on bentonite and the D231 resin were simultaneously observed, suggesting that the adsorption kinetics of Eu(Ⅲ) was mainly dominated by hydrated Eu(Ⅲ) ions on the liquid membrane.

关键词： ICM-Ap method LMD model Adsorption mechanism Eu(Ⅲ)