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Room-temperature extraction of individual elements from charged spent LiFePO_(4)batteries

Rare Metals 2022年第5期41卷 1595-1604页

作者： Mei-Cen Fan yun Zhao yu-qiong kang John Wozny Zheng Liang Jun-Xiong Wang Guang-Min Zhou Bao-Hua Li Naser Tavajohi Fei-yu kang Shenzhen Key Laboratory on Power Battery Safety and Shenzhen Geim Graphene Center Tsinghua Shenzhen International Graduate School(SIGS)Shenzhen 518055China Department of Chemistry and Biochemistry Northern Illinois UniversityDekalb 60115USA School of Chemistry and Chemical Engineering Frontiers Science Center for Transformative MoleculesShanghai Jiao Tong UniversityShanghai 200240China Shenzhen Geim Graphene Center Tsinghua-Berkeley Shenzhen Institute and Tsinghua Shenzhen International Graduate SchoolTsinghua UniversityShenzhen 518055China Department of Chemistry Umea UniversityUmeii 90187Sweden

Recycling millions of metric tons of spent LiFePO_(4) batteries would benefit human health while reducing resource depletion and environmental ***,recovering individual elements from the spent batteries without generating waste is ***,we present a distinctive approach for recycling spent LiFePO_(4) batteries at room temperature,where water is the only leaching agent ***_(4) and lithium intercalated graphite act as a precursor material for selectively extracting lithium,iron,and phosphorus through charging the LiFePO_(4) batteries to the delithiated *** solution extracted Fe from FePO_(4) within 30 min and regenerated without consumption,similar to a *** the optimal leaching conditions(1 mol·L^(-1) NaOH,0.5 h,NaOH/Fe molar ratio of 4.5),Fe and P leaching efficiencies achieved 89.1%and 99.2%,*** methodology reflected in this research reduced the material cost per kg cathode material to a fraction of previously published reports,only occupies 6.13%of previous *** addition,the method improved the battery recycling revenue calculated by the EverBatt model by 2.31 times and 1.94 times over pyrometallurgical and hydrometallurgical *** proposed method allows for the convenient recovery of the elemental components of spent LiFePO_(4) batteries.

关键词： Battery recycling Spent LiFePO_(4)batteries Charged batteries FePO_(4) Lithiated anode

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Lithium metal recycling from spent lithium-ion batteries by cathode overcharging process

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Rare Metals 2022年第6期41卷 1843-1850页

作者： Mei-Cen Fan John Wozny Jue Gong yu-qiong kang Xian-Shu Wang Zhe-Xu Zhang Guang-Min Zhou yun Zhao Bao-Hua Li Fei-yu kang Shenzhen Key Laboratoryon Power Battery Safety and Shenzhen Geim Graphene Center Tsinghua Shenzhen International Graduate School(SIGS)Shenzhen518055.China Department of Chemistryand Biochemistry Northern Iinois UniversityDekalb 60115.USA School of Materials and Energy and Center for Applied Chemistry University of Electronic Science and Technology of ChinaChengdu 611731China Shenzhen Geim Graphene Center Tsinghua-Berkeley Shenzhen Institute and Tsinghua Shenzhen International Graduate SchoolTsinghua UniversityShenzhen 518055China

The burgeoning growth of lithium-ion batteries(LIBs)has caused great concern for the uninterrupted supply of *** spent LIBs are a richer source of lithium than the natural resources from ore,salt lake brine,or seawater,traditional methodology for recycling of lithium in spent LIBs suffers from costly energy consumption and the generation of unfriendly environmental pollutants.

关键词： lithium charging process

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A novel three-step approach to separate cathode components for lithium-ion battery recycling

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Rare Metals 2021年第6期40卷 1431-1436页

作者： yun Zhao Ling-Zhe Fang yu-qiong kang Li Wang yu-Nan Zhou Xin-Yi Liu Tao Li Yan-Xi Li Zheng Liang Zhe-Xu Zhang Bao-Hua Li Engineering Laboratory for Next Generation Power and Energy Storage Batteries Graduate School at ShenzhenTsinghua UniversityShenzhen 518055China Department of Chemistry and Biochemistry Northern Illinois UniversityDekalb 60115USA Institute of Nuclear and New Energy Technology Tsinghua UniversityBeijing 100084China Department of Materials Science and Engineering Stanford UniversityStanford 94305USA

Lithium-ion batteries(LIBs)represent efficient energy storage technology that can help to alleviate fossil fuel-based CO_(2) ***,LIBs are being applied extensively in consumer electronics and electric vehicles,but because of limited resources,there is an urgent need for spent LIB recycling *** complexity of LIBs,especially the electrode part,makes it difficult to achieve precision separations for each single component from the used electrode with low ***,we propose a three-step treatment for the separation of cathode *** detail,detaching of the current collector from the cathode is accomplished by the solvent method,which was found to be an ideal strategy compared with previous ***,a thermal treatment is used to remove the polymer binder in the second step because we demonstrated that it is challenging to separate polyvinylidene fluoride(PVDF)from other cathode components by dissolution with *** separation efficiency between the active material and conductive carbon by the polymer solution in the third step showed reasonably good *** anticipate this work will serve as an important reference for the separation of each single electrode component in both laboratory-and industrialscale *** of binder and development of novel binders,which can be easily recycled for sustainable LIBs,are fruitful areas for further research.

关键词： Lithium-ion batteries Recycling Electrode separation PVDF Thermal treatment Polymer solution

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Synergistic anionic/zwitterionic mixed surfactant system with high emulsification efficiency for enhanced oil recovery in low permeability reservoirs

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Petroleum Science 2024年第2期21卷 936-950页

作者： Hai-Rong Wu Rong Tan Shi-Ping Hong qiong Zhou Bang-yu Liu Jia-Wei Chang Tian-Fang Luan Ning kang Ji-Rui Hou National Key Laboratory of Petroleum Resources and Engineering China University of Petroleum-BeijingBeijing102249China Unconventional Petroleum Research Institute China University of Petroleum-BeijingBeijing102249China Gas Production Plant 5 of PetroChina Changqing Oilfield Company PetroChinaXi'an710000ShaanxiChina College of Petroleum Engineering China University of Petroleum-BeijingBeijing102249China College of Science China University of Petroleum-BeijingBeijing102249China Kazakh-British Technical University Almaty050000Kazakhstan

Emulsification is one of the important mechanisms of surfactant flooding. To improve oil recovery for low permeability reservoirs, a highly efficient emulsification oil flooding system consisting of anionic surfactant sodium alkyl glucosyl hydroxypropyl sulfonate(APGSHS) and zwitterionic surfactant octadecyl betaine(BS-18) is proposed. The performance of APGSHS/BS-18 mixed surfactant system was evaluated in terms of interfacial tension, emulsification capability, emulsion size and distribution, wettability alteration, temperature-resistance and salt-resistance. The emulsification speed was used to evaluate the emulsification ability of surfactant systems, and the results show that mixed surfactant systems can completely emulsify the crude oil into emulsions droplets even under low energy conditions. Meanwhile,the system exhibits good temperature and salt resistance. Finally, the best oil recovery of 25.45% is achieved for low permeability core by the mixed surfactant system with a total concentration of 0.3 wt%while the molar ratio of APGSHS:BS-18 is 4:6. The current study indicates that the anionic/zwitterionic mixed surfactant system can improve the oil flooding efficiency and is potential candidate for application in low permeability reservoirs.

关键词： Anionic/zwitterionic mixed surfactant system Emulsification Synergistic effect Low permeability reservoir Enhanced oil recovery

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Paleogene transgression process and environmental evolution in the deepwater area of the Baiyun Depression in the northern South China Sea

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Acta Oceanologica Sinica 2024年第4期43卷 15-24页

作者： Peijun Qiao yuchi Cui qiong Ma Qiang yu Lei Shao State Key Laboratory of Marine Geology Tongji UniversityShanghai 200092China CNOOC Energy Technology&Services-Drilling&Production Co. CNOOC Central Laboratory Shenzhen BranchGuangdong 516000China

Multiple borehole samples are collected from the Baiyun Depression in deep-water area of the northern South China Sea(SCS)in an effort to reconstruct transgression processes during the Paleogene based on palynalgal *** study indicates that the Baiyun Depression generated a large group of palynopore assemblages and fluvial/lacustrine-related algae during the early and middle Eocene when the Wenchang Formation was *** entire depression was dominated by fluvial and lacustrine facies before *** eastern and southeastern sags transitioned to shallow marine environment by generating a large abundance of marine dinoflagellates during the Enping deposition of the late ***,the southern uplift zone simply yielded fluvial/lacustrine-related palynopores and algae,and was dominated by the fluvial and lacustrine environment during the early stage of the Enping Formation,prior to shifting into transitional setting in the later *** sags remained extensive fluvial and delta facies without existence of marine *** was until the depositional stage of the Zhuhai Formation(Oligocene)that the overall depression was strongly impacted from transgression *** eastern and southeastern sags were mainly under deep marine setting on a continental slope while northwestern and southern areas developed transitional *** distribution and accumulation patterns varied greatly among sub-sags,the overall Baiyun Depression was characterized by widespread development of marine *** should be noted that the northwestern sag also partly generated large-scale river delta *** to the eustatic rise and change of SCS spreading axis,the overall Baiyun Depression was mostly influenced by the deep marine environment on a continental slope during the early *** northwestern sag and southern uplift zone were found plentiful marine *** summary,transgression initiated from the ea

关键词： South China Sea Paleogene transgression sedimentary environment plant ecology

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Steel-refractory reactions in lanthanum-,cerium-,and ytrium-added steels

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Journal of Iron and Steel Research International 2024年第6期31卷 1473-1485页

作者： Jian kang Hong-po Wang yu Wang College of Materials Science and Engineering Chongqing UniversityChongqing 400044China The State Key Laboratory of Mechanical Transmissions Chongqing UniversityChongqing 400044China

A systematic experimental study was conducted on the similarities and differences in the reactions between commonly used rare earth elements(REEs)and frequently used refractories in the steelmaking *** results indicate that the reaction behaviors of La,Ce,and Y with MgO,Al_(2)O_(3),and MgO·Al_(2)O_(3) crucibles differed *** consumption rates of La,Ce,and Y in the molten steel were in descending order of La>Ce>Y for smelting with all three kinds of *** the REEs reacted with the crucible,the contents of Mg and Al showed a trend of first increasing and then *** laboratory-scale smelting conditions,the reactions related to REEs were dominated by steel-crucible reactions,and the contact area between the unit mass of molten steel and refractory materials mainly determined the consumption rates of ***-and Ce-crucible reactions generated loose and porous reaction interfaces;however,Y-crucible reactions generated a dense Y_(2)O_(3) layer,dramatically suppressing the consumption rate of *** calculation indicated that the reactions between rare earth and different refractory materials were first-order *** crucible materials significantly affected the product type and morphology of the steel-crucible reaction interfaces,thereby influencing the consumption rate of *** reactions between REEs and refractories must be seriously considered,especially for small-scale smelting.

关键词： Rare earth Inclusion Refractory Thermodynamics Dynamics

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Experimental observations on the nonproportional multiaxial ratchetting of cast AZ91 magnesium alloy at room temperature

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International Journal of Minerals,Metallurgy and Materials 2024年第5期31卷 1115-1125页

作者： Binghui Hu yu Lei Hang Li Ziyi Wang Chao yu Guozheng kang Applied Mechanics and Structure Safety Key Laboratory of Sichuan Province School of Mechanics and Aerospace EngineeringSouthwest Jiaotong UniversityChengdu 610031China

The nonproportional multiaxial ratchetting of cast AZ91 magnesium (Mg) alloy was examined by performing a sequence of axial-torsional cyclic tests controlled by stress with various loading paths at room temperature (RT).The evolutionary characteristics and path dependence of multiaxial ratchetting were *** illustrate that the cast AZ91 Mg alloy exhibits considerable nonproportional additional softening during cyclic loading with multiple nonproportional multiaxial loading paths;multiaxial ratchetting presents strong path dependence,and axial ratchetting strains are larger under nonproportional loading paths than under uniaxial and proportional45°linear loading paths;multiaxial ratchetting becomes increasingly pronounced as the applied stress amplitude and axial mean stress ***,stress-strain curves show a convex and symmetrical shape in axial/torsional *** ratchetting exhibits quasi-shakedown after certain loading *** abundant experimental data obtained in this work can be used to develop a cyclic plasticity model of cast Mg alloys.

关键词： cast magnesium alloy ratchetting multiaxial loading loading path stress level

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Integration of urchin-like MnCo_(2)O_(4)@C core–shell nanowire arrays within porous copper current collector for superior performance Li-ion battery anodes

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Rare Metals 2024年第2期43卷 599-611页

作者： Xue-Ru Zhang qiong Wu Yong Zhang Xi-Fei Li Ting Xie yu-Cheng Wu Instrumental Analysis Center Hefei University of TechnologyHefei230009China Key Laboratory of Advanced Functional Materials and Devices of Anhui Province Hefei230009China School of Materials Science and Engineering Hefei University of TechnologyHefei230009China Institute of Advanced Electrochemical Energy Xi’an University of TechnologyXi’an710048China

Spinel MnCo_(2)O_(4) is a promising energy storage candidate as anode materials in lithium-ion batteries owing to synergistic effects of two intrinsic solid-state redox ***,low conductivity,poor rate capacity and rapid capacity fading have seriously impaired its practical *** overcome the inferiorities,urchin-like MnCo_(2)O_(4)@C core–shell nanowire arrays have been fabricated directly within a porous copper current collector via a facile hydrothermal method followed by a chemical vapor deposition carbonization *** a typical nanowire,the core is composed of interconnected MnCo_(2)O_(4)nanoparticles and the shell shows as a thin amorphous carbon *** integrated MnCo_(2)O_(4)@C/Cu structure could act as working anodes without using additives or polymer *** MnCo_(2)O_(4)@C/Cu possesses slightly longer Li-ion insertion/desertion pathway than that of MnCo_(2)O_(4)/Cu,the carbon shell could effectively prevent the pulverization of MnCo_(2)O_(4) and lower down charge transfer resistance and actively participate in Li-ion *** rearrangement of carbon atoms during lithiation/delithiation cycling could inhibit the formation of passive solid electrolyte interphase *** a result,the MnCo_(2)O_(4)@C/Cu electrode presents superior rate capacity(600 mAh·g^(−1) at 1 A·g^(−1)) and better stability(797 mAh·g^(−1) after 200 cycles at 100 mA·g^(−1)).The excellent reversible Li ion storage capacity,cycling stability and rate capacity endow MnCo_(2)O_(4)@C/Cu great potential as stable and high output integrated anode materials in Li-ion batteries.

关键词： MnCo_(2)O_(4)@C Urchin-like nanowire arrays Core-shell Integrated anode materials Lithium-ion batteries

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De-biased knowledge distillation framework based on knowledge infusion and label de-biasing techniques

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Journal of Electronic Science and Technology 2024年第3期22卷 57-68页

作者： Yan Li Tai-kang Tian Meng-yu Zhuang yu-Ting Sun School of Economics and Management University of Electronic Science and Technology of ChinaChengdu611731China School of Economics and Management Beijing University of Posts and TelecommunicationBeijing100876China School of Electrical Engineering and Computer Science The University of QueenslandBrisbane4072Australia

Knowledge distillation,as a pivotal technique in the field of model compression,has been widely applied across various ***,the problem of student model performance being limited due to inherent biases in the teacher model during the distillation process still *** address the inherent biases in knowledge distillation,we propose a de-biased knowledge distillation framework tailored for binary classification *** the pre-trained teacher model,biases in the soft labels are mitigated through knowledge infusion and label de-biasing *** on this,a de-biased distillation loss is introduced,allowing the de-biased labels to replace the soft labels as the fitting target for the student *** approach enables the student model to learn from the corrected model information,achieving high-performance deployment on lightweight student *** conducted on multiple real-world datasets demonstrate that deep learning models compressed under the de-biased knowledge distillation framework significantly outperform traditional response-based and feature-based knowledge distillation models across various evaluation metrics,highlighting the effectiveness and superiority of the de-biased knowledge distillation framework in model compression.

关键词： De-biasing Deep learning Knowledge distillation Model compression

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Online estimation and characteristic analysis of double nugget diameters during aluminum/steel resistance spot welding process

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Journal of Iron and Steel Research International 2024年第8期31卷 2053-2067页

作者： kang Zhou Wen-xiao yu Bao-kai Ren Gang Wang School of Mechatronical Engineering Beijing Institute of TechnologyBeijing 100081China

Online estimation of the double nugget diameters was performed by means of a back propagation neural *** double nugget diameters were obtained using actual welding experiment and numerical simulation,according to different characteristics of aluminum nugget and steel *** input of the neural network was some key characteristic parameters extracted from dynamic power signal,which were peak point,knee point and their variation rate over time,as well as heat energy delivered into the welding *** architecture of the neural network was confirmed by confirming the number of neurons in hidden layer through a series of *** key parameters of the neural network were obtained by means of training 81 arrays of data ***,the neural network was used to test the remaining 20 arrays of verifying data set,and the results showed that both of the mean errors for the two nugget diameters were below 3%.In addition,corresponding analyses showed that the accuracy of two nugget diameters was higher than that of tensile-shear strength.

关键词： Resistance spot welding Aluminum Steel Double nugget Dynamic power signal.Neural network

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