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Studies on the Crystal Structure and Photoluminescence of a Mercury(Ⅱ)Complex Based on a Novel Pyridine Ligand

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Chinese Journal of Structural Chemistry 2010年第7期29卷 1029-1032页

作者： WU jie-ying zhou Wen LI Wei-jie zhou Hong-Ping TIAN Yu-Peng Department of Chemistry Key Laboratory of Functional Inorganic Materials Chemistry of Anhui Province Anhui University Hefei 230039 China

A novel mercury（H） complex HgL2Br2 was prepared from HgBr2 and the organic ligand 2-（N-methyl-N-（4-（（E）-2-（pyridine-4-yl）vinyl）phenyl）amino）ethanol （L）. The ligand was synthesized and then characterized by FT-IR spectroscopy, tH NMR, mass spectrum and elemental analysis, while the single-crystal diffraction data of the complex were collected on a Siemens Smart CCD diffractometer. The complex crystallizes in triclinic space group PI with a = 5.367（5）, b = 12.466（5）, c = 23.945（5） A, α = 90.812（5）, β = 96.318（4）, γ = 96.093（5）°, Z = 2, Dc = 1.817 ***3,μ = 7.395 mm^-1, S = 0.825, and the final R= 0.0396. The Hg（Ⅱ） ion in the distorted tetrahedral mercury（Ⅱ） complex C32H36HgBr2N4O2 is coordinated by two N atoms from the two ligands together with two bromide ions. Solid-state emission of the ligand and its complex has been investigated at room temperature.

关键词： mercury(Ⅱ) complex single-photon fluorescence crystal structure

Endogenous automatic nerve discharge promotes nerve repair: an optimized animal model

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Neural Regeneration Research 2019年第2期14卷 306-312页

作者： Jing Rui ying-jie zhou Xin Zhao Ji-Feng Li Yu-Dong Gu jie Lao Department of Hand Surgery Huashan Hospital Fudan University Key Laboratory of Hand Reconstruction Ministry of Health Shanghai Key Laboratory of Peripheral Nerve and Microsurgery

Exogenous electrical nerve stimulation has been reported to promote nerve regeneration. Our previous study has suggested that endogenous automatic nerve discharge of the phrenic nerve and intercostal nerve has a positive effect on nerve regeneration at 1 month postoperatively, but a negative effect at 2 months postoperatively, which may be caused by scar compression. In this study, we designed four different rat models to avoid the negative effect from scar compression. The control group received musculocutaneous nerve cut and repair. The other three groups were subjected to side-to-side transfer of either the phrenic(phrenic nerve group), intercostal(intercostal nerve group) or thoracodorsal nerves(thoracic dorsal nerve group), with sural nerve autograft distal to the anastomosis site. Musculocutaneous nerve regeneration was assessed by electrophysiology of the musculocutaneous nerve, muscle tension, muscle wet weight, maximum cross-sectional area of biceps, and myelinated fiber numbers of the proximal and distal ends of the anastomosis site of the musculocutaneous nerve and the middle of the nerve graft. At 1 month postoperatively, compound muscle action potential amplitude of the biceps in the phrenic nerve group and the intercostal nerve group was statistically higher than that in the control group. The myelinated nerve fiber numbers in the distal end of the musculocutaneous nerve and nerve graft anastomosis in the phrenic nerve and the intercostal nerve groups were statistically higher than those in the control and thoracic dorsal nerve groups. The neural degeneration rate in the middle of the nerve graft in the thoracic dorsal nerve group was statistically higher than that in the phrenic nerve and the intercostal nerve groups. At 2 and 3 months postoperatively, no significant difference was detected between the groups in all the assessments. These findings confirm that the phrenic nerve and intercostal nerve have a positive effect on nerve regeneration at the

关键词： nerve regeneration peripheral nerve regeneration endogenous automatic discharge side-to-side nerve anastomosis phrenic nerve intercostal nerve animal model electrical treatment rats nerve compression neural regeneration

Identify Congested Links Based on Enlarged State Space

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Journal of Computer Science & Technology 2016年第2期31卷 350-358页

作者： Sheng-Li Pan Zhi-Yong Zhang ying-jie zhou Feng Qian Guang-Min Hu School of Communication and Information Engineering University of Electronic Science and Technology of China Chengdu 611731 China School of Computer and Communication Sciences Swiss Federal Institute of Technology Lausanne Lausanne 1015 Switzerland College of Computer Science Sichuan University Chengdu 610065 China

When paths share a common congested link, they will all suffer from a performance degradation. Boolean tomography exploits these performance-level correlations between different paths to identify the congested links. It is clear that the congestion of a path will be distinctly intensive when it traverses multiple congested links. We adopt an enlarged state space model to mirror different congestion levels and employ a system of integer equations, instead of Boolean equations, to describe relationships between the path states and the link states. We recast the problem of identifying congested links into a constraint optimization problem, including Boolean tomography as a special case. For a logical tree, we propose an up-to-bottom algorithm and prove that it always achieves a solution to the problem. Compared with existing algorithms, the simulation results show that our proposed algorithm achieves a higher detection rate while keeping a low false positive rate.

关键词： network monitoring network tomography end-to-end measurement congested link identification optimization

Contribution of Root Respiration to Total Soil Respiration in a Betula ermanii-Dark Coniferous Forest Ecotone of the Changbai Mountains, China

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Pedosphere 2005年第4期15卷 448-455页

作者： LIU ying HAN Shi-jie zhou Yu-Mei ZHANG Jun-Hui Institute of Applied Ecology Chinese Academy of Sciences Shenyang 110016 （China）.

Total and root-severed soil respiration rates for five plots set up 50 m apart in a Betula ermanii Cham.-dark coniferous forest ecotone on a north-facing slope of the Changbai Mountains, China, were measured to evaluate the seasonal variations of soil respiration, to assess the effect of soil temperature and water content on soil respiration, and to estimate the relative contributions of root respiration to the total soil respiration. PVC cylinders in each of 5 forest types of a B. ermanii-dark coniferous forest ecotone were used to measure soil respirations both inside and outside of the cylinders. The contribution of roots to the total soil respiration rates ranged from 12.5% to 54.6%. The mean contribution of roots for the different plots varied with the season, increasing from 32.5% on June 26 to 36.6% on August 3 and to 41.8% on October 14. In addition, there existed a significant (P < 0.01) logarithmic relationship between total soil respiration rate and soil temperature at 5 cm soil depth. Also, a similar trend was observed for the soil respiration and soil water content at the surface (0-5 cm) during the same period of time.

关键词： Betula ermanii Cham. dark coniferous forest ecotone root respiration soil respiration

Sox9 is indispensable for testis differentiation in the red-eared slider turtle,a reptile with temperaturedependent sex determination

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Zoological Research 2021年第6期42卷 721-725页

作者： Hang-Bo Hui Ling Xiao Wei Sun ying-jie zhou Hai-Yan Zhang Chu-Tian Ge Institute of Animal Sex and Development Zhejiang Wanli UniversityNingboZhejiang 315100China

SOX9(SRY-related HMG box gene 9)is an essential regulator of male sex determination and testis differentiation in many vertebrate ***,the functional role of Sox9 in testis differentiation has not yet been identified in any reptilian ***,Sox9 knockdown in the red-eared slider turtle(Trachemys scripta)embryos at a male-producing temperature led to complete male-to-female sex reversal,characterized by the formation of an ovary-like structure,disappearance of male marker AMH,and ectopic expression of ovarian regulator FOXL2,as well as a female distribution pattern of germ ***,in-ovo overexpression of Sox9 at a female-producing temperature resulted in partial masculinization of putative female embryos,with the coexistence of AMH and *** study provides the first direct evidence that Sox9 is indispensable for testicular differentiation in a reptilian species,further confirming the conserved role of Sox9 in vertebrate sexual development.

关键词： Sox9 determination indispensable

Effects of Mo promoters on the Cu-Fe bimetal catalysts for the DMC formation from CO_2 and methanol

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Chinese Chemical Letters 2013年第4期24卷 307-310页

作者： ying-jie zhou Min Xiao Shuan-Jin Wang Dong-Mei Han Yi-Xin Lu Yue-Zhong Meng The Key Laboratory of Low-carbon Chemistry & Energy Conservation of Guangdong Province/State Key Laboratory of Optoelectronic Materials and Technologies Sun Yat-sen University Department of Chemistry & Medicinal Chemistry Program Office of Life SciencesNational University of Singapore

The Mo-promoted Cu-Fe bimetal catalysts were prepared and used for the formation of dimethyl carbonate （DMC） from CO2 and methanol. The catalysts were characterized by X-ray diffraction （XRD）, temperature programmed reduction （TPR）, laser Raman spectra （LRS）, energy dispersive spectroscopy （EDS） and temperature programmed desorption （TPD） techniques. The experimental results demonstrated that the Mo promoters can decrease the reducibility and increase the dispersion of Cu-Fe clusters, The concentration balance of base-acid sites can be readily adjusted by changing the Mo content. The moderate concentration balance of acid and base sites was in favor of the DMC formation, Under optimal experimental conditions, the highest methanol conversion of 6,99% with a DMC selectivity of 87.7% can be obtained when 2.5 wt% of Mo was loaded.

关键词： Dimethyl carbonateCarbon dioxideCatalysisBimetal catalyst

Structural engineering of high-entropy alloys for advanced electrocatalytic reactions

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Tungsten 2025年第1期7卷 1-31页

作者： Qiao Xie ying-jie Yu Hai-Jun Zhang Ya-Ping Deng Wen Lei The State Key Laboratory of Refractories and Metallurgy Wuhan University of Science and Technology Department of Chemical Engineering Waterloo Institute for Sustainable Energy Waterloo Institute for Nanotechnology University of Waterloo

High-entropy alloys(HEAs) have emerged as promising candidates to replace traditional precious metal catalysts,owing to their unique chemical and physical *** review commences by revisiting the fundamental concepts of HEAs,including their synthesis methods and structural control strategies in *** underscores the critical role of meticulously manipulating both macroscopic and microscopic structures of the HEAs to optimize their catalytic performance.A deep understanding of the structure-activity relationship in HEAs across various configurations is pivotal in developing more effective *** review methodically encapsulates the research progress of structural control strategies for HEAs in achieving efficient energy conversion,with the aim of gaining a better understanding of the relationship between structure and *** review concludes by summarizing the current achievements and challenges,and suggestions for potential future directions of HEAs in the fields of energy conversion and environmental purification.

关键词： Electrocatalytic Energy conversion High-entropy alloys Structural modulation

DUCA双环多天线MIMO系统性能分析与研究

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通信学报 2016年第12期37卷 11-20页

作者：邵根富姚颖莉周杰菊池久和杭州电子科技大学自动化学院浙江杭州310018 南京信息工程大学电子与信息工程学院江苏南京210044 国立新泻大学工学部日本新泻950-2181

针对非频率选择性瑞利衰落信道,在三维(3D,three-dimensional)空间域信道模型中分析和研究紧凑型双环阵列(DUCA,double uniform circular array)多天线MIMO系统。采用互耦效应的等效电路模型,首次导出DUCA天线阵元间的信号衰落相关性的... 详细信息

针对非频率选择性瑞利衰落信道,在三维(3D,three-dimensional)空间域信道模型中分析和研究紧凑型双环阵列(DUCA,double uniform circular array)多天线MIMO系统。采用互耦效应的等效电路模型,首次导出DUCA天线阵元间的信号衰落相关性的通用表达式,阐明互耦效应的影响机理。分析结果与传统MIMO线性阵列(ULA,uniform linear array)和单环阵列(UCA,uniform circular array)相比较,阵元空间配置及其互耦效应将对信号衰落相关性起到决定性作用。研究结果对未来massive MIMO多天线的设计和性能优化具有很好的指导意义。

关键词： MIMO多天线双环阵列互耦效应信号衰落相关性

Storage time affects the level and diagnostic efficacy of plasma biomarkers for neurodegenerative diseases

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Neural Regeneration Research 2025年第8期20卷 2373-2381页

作者： Lifang Zhao Mingkai Zhang Qimeng Li Xuemin Wang jie Lu ying Han Yanning Cai Department of Clinical Biobank Xuanwu HospitalCapital Medical UniversityBeijingChina Beijing Geriatric Medical Research Center BeijingChina Department of Neurology Xuanwu HospitalCapital Medical UniversityBeijingChina Department of Radiology and Nuclear Medicine Xuanwu HospitalCapital Medical UniversityBeijingChina Beijing Key Laboratory of Magnetic Resonance Imaging and Brain Informatics BeijingChina Key Laboratory of Neurodegenerative diseases Ministry of EducationBeijingChina School of Biomedical Engineering Hainan UniversityHaikouHainan ProvinceChina Center of Alzheimer’s Disease Beijing Institute for Brain DisordersBeijingChina National Clinical Research Center for Geriatric Diseases BeijingChina Institute of Biomedical Engineering Shenzhen Bay LaboratoryGaoke Innovation CenterShenzhenGuangdong ProvinceChina Department of Neurobiology Xuanwu HospitalCapital Medical UniversityBeijingChina

Several promising plasma biomarker proteins,such as amyloid-β(Aβ),tau,neurofilament light chain,and glial fibrillary acidic protein,are widely used for the diagnosis of neurodegenerative ***,little is known about the long-term stability of these biomarker proteins in plasma samples stored at-80°*** aimed to explore how storage time would affect the diagnostic accuracy of these biomarkers using a large *** samples from 229 cognitively unimpaired individuals,encompassing healthy controls and those experiencing subjective cognitive decline,as well as 99 patients with cognitive impairment,comprising those with mild cognitive impairment and dementia,were acquired from the Sino Longitudinal Study on Cognitive Decline *** samples were stored at-80°C for up to 6 years before being used in this *** results showed that plasma levels of Aβ42,Aβ40,neurofilament light chain,and glial fibrillary acidic protein were not significantly correlated with sample storage ***,the level of total tau showed a negative correlation with sample storage ***,in individuals without cognitive impairment,plasma levels of total protein and tau phosphorylated protein threonine 181(p-tau181)also showed a negative correlation with sample storage *** was not observed in individuals with cognitive ***,we speculate that the diagnostic accuracy of plasma p-tau181 and the p-tau181 to total tau ratio may be influenced by sample storage ***,caution is advised when using these plasma biomarkers for the identification of neurodegenerative diseases,such as Alzheimer's ***,in cohort studies,it is important to consider the impact of storage time on the overall results.

关键词： Alzheimer’s disease amyloid-β diagnostic ability glial fibrillary acidic protein neurodegeneration neurofilament light chain plasma biomarkers single molecule array storage time tau