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国际医学放射学杂志 2024年第4期 495-495页

作者： S.yun j.E.Park N.y.Kim S.y.Park H.S.Kim 王笑男

摘要目的开发一种结合梯度回波和快速自旋回波的对比增强MRI深度学习（DL）模型（双增强DL）用于检测脑转移瘤（BM），并与神经影像医师以及仅使用梯度回波影像

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Hetero-deformation promoted strengthening and toughening in BCC rich eutectic and near eutectic high entropy alloys

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journal of Materials Science & Technology 2023年第15期146卷 1-9页

作者： D.H.Chung j.Lee Q.F.He y.K.Kim K.R.Lim H.S.Kim y.yang y.S.Na Department of Special Alloys Extreme Materials Research InstituteKorea Institute of Materials ScienceChangwonThe Republic of Korea Department of Mechanical Engineering City University of Hong KongKowloon TongKowloonHong KongChina Graduate Institute of Ferrous Technology Pohang University of Science and TechnologyPohangThe Republic of Korea Center for Heterogenic Metal Additive Manufacturing Pohang University of Science and TechnologyPohangThe Republic of Korea Department of Materials Science and Engineering City University of Hong KongKowloon TongKowloonHong KongChina

Heterostructured eutectic high-entropy alloys(EHEAs)have attracted significant attention owing to their novel properties,such as balanced combinations of strength and fracture ***,the toughening/strengthening mechanisms of these EHEAs have not been thoroughly *** this study,we developed a series of dual-phase Al_((18–2x))Co_(30)Cr_((11+x))Fe_((11+x))Ni_(3)0(x=-1,0,1)eutectic and neareutectic HEAs containing face-centered cubic(FCC)and body-centered cubic(BCC)*** the high amount of BCC,which is referred to as the brittle phase,newly developed EHEAs exhibited superior fracture ***,we discovered that a fully eutectic HEA exhibited further improvements in both yield stress and fracture toughness,outperforming our off-eutectic and other previously reported *** combining experiments and theoretical models,we demonstrated that the synergistic increase in both strength and toughness in our fully eutectic HEA was derived from the high hetero-deformationinduced(HDI)strengthening/toughening associated with a high misorientation angle at the grain/phase boundaries.

关键词： Eutectic high entropy alloy Fracture toughness Heterogeneous structure Hetero deformation induced strengthening Misorientation angle

Hybrid TiO_(2)/Ag NPs/g-C_(3)N_(4) nanocomposite coatings on TC4 titanium alloy for enhanced synergistic antibacterial effect under full spectrum light

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journal of Materials Science & Technology 2022年第23期118卷 35-43页

作者： Xi.Rao L.Du j.j.Zhao X.D.Tan y.X.Fang L.Q.Xu y.P.Zhang School of Materials and Energy Southwest UniversityChongqing 400715China Chongqing Key Laboratory of Soft-Matter Material Chemistry and Function Manufacturing Southwest UniversityChongqing 400715China

The hybrid TiO_(2)/AgNPs/g-C_(3) N_(4) nanocomposite coatings were constructed on TC4 alloy by a hydrothermal and calcining ***_(2)/AgNPs/g-C_(3) N_(4) nanocomposite coatings demonstrated excellent biocompatibility and osteogenesis compared to those of titanium *** existence of trace AgNPs on the surface and interface of the heterojunction could further enhance the transfer and separation of photogenerated electron/hole pairs,which greatly improved the antibacterial performance under full spectrum *** at the valence band of TiO_(2) and g-C_(3) N_(4) reacted with adsorbed H_(2) O to generate·OH,killing bacteria through photocatalytic redox reaction under light irradiation,while released AgNPs exhibited bacteriostatic efficacy with or without *** study provides a pathway of coating modification for further improving the antibacterial properties of heterojunction coatings and maintaining the biocompatibility of matrix materials.

关键词： TiO_(2)/AgNPs/g-C_(3)N_(4)nanocomposite g-C_(3)N_(4) Photocatalysis Photocatalytic inactivation of bacteria Disinfection mechanism

Plant triterpenoid saponins function as susceptibility factors to promote the pathogenicity of Botrytis cinerea

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Molecular Plant 2024年第7期17卷 1073-1089页

作者： Francisco j.Escaray Amelia Felipo-Benavent Cristian j.Antonelli Begona Balaguer Maria Pilar Lopez-Gresa Pablo Vera Instituto de Biologia Molecular y Celular de Plantas Universidad Politecnica de Valencia-C.S.l.CCiudad Politecnica de la InnovacionEdificio 8Eacceso GIngeniero Fausto Elios/n46022ValenciaSpain

The gray mold fungus Botrytis cinerea is a necrotrophic pathogen that causes diseases in hundreds of plant species,including high-value *** polyxenous nature and pathogenic success are due to its ability to perceive host signals in its *** this study,we found that laticifer cells of Euphorbia lathyris are a source of susceptibility factors required by *** to cause ***,poor-in-latex(pil)mutants,which lack laticifer cells,show full resistance to this pathogen,whereas lot-of-latex mutants,which produce more laticifer cells,are *** S factors are triterpenoid saponins,which are widely distributed natural products of vast structural *** downregulation of laticifer-specific oxydosqualene cyclase genes,which encode the first committed step enzymes for triterpene and,therefore,saponin biosynthesis,conferred disease resistance to ***,the Medicago truncatula Iha-1 mutant,compromised in triterpenoid saponin biosynthesis,showed enhanced ***,the application of different purified triterpenoid saponins pharmacologically complemented the diseaseresistant phenotype ofpil and hla-1 mutants and enhanced disease susceptibility in different plant *** found that triterpenoid saponins function as plant cues that signal transcriptional reprogramming in ***,leading to a change in its growth habit and infection strategy,culminating in the abundant formation of infection cushions,the multicellular appressoria apparatus dedicated to plant penetration and biomass destruction in *** together,these results provide an explanation for how plant triterpenoid saponins function as disease susceptibility factors to promote *** pathogenicity.

关键词： Euphorbia lathyris laticifer cell latex appressorium infection cushion necrotrophic fungi

Thermal stability and deformation mechanisms in Ni-Co-Fe-Cr-Al-Ti-Nb-type nanoparticle-strengthened high-entropy alloys

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journal of Materials Science & Technology 2023年第36期167卷 171-183页

作者： j.X.Hou j.y.Zhang j.X.Zhang j.H.Luan y.X.Wang B.X.Cao y.L.Zhao Z.B.jiao X.j.Liu W.W.Song P.K.Liaw T.yang Department of Materials Science and Engineering Hong Kong Institute for Advanced StudyCity University of Hong KongHong KongChina School of Materials Science and Engineering Harbin Institute of Technology(Shenzhen)Shenzhen 518055China Department of Mechanical Engineering The Hong Kong Polytechnic UniversityHong KongChina Steel Institute RWTH Aachen UniversityAachen 52072Germany Institute of Materials Engineering University of KasselKassel 334125Germany Department of Materials Science and Engineering The University of TennesseeKnoxvilleTN 37996-2200USA City University of Hong Kong China

The precipitate morphologies,coarsening kinetics,elemental partitioning behaviors,grain structures,and tensile properties were explored in detail for L1_(2)-strengthened Ni_(39.9)Co_(20)Fe_(15)Cr_(15)Al_(6)Ti_(4-x)Nb_(x)B_(0.1)(x=0 at.%,2 at.%,and 4 at.%)high-entropy alloys(HEAs).By substituting Ti with Nb,the spheroidal-to-cuboidal precipitate morphological transition,increase in the coarsening kinetics,and phase decomposition upon aging at 800°C *** excessive addition of Nb brings about the grain boundary precipitation of an Nb-rich phase along with the phase decomposition from the L1_(2)to lamellar-structured D019 phase upon the long-term aging *** partially substituting Ti with Nb,the chemically complex and thermally stable L12 phase with a composition of(Ni_(58.8)Co_(9.8)Fe_(2.7))(Al_(12.7)Ti_(5.8)Nb_(7.5)Cr_(2.3))ensures the stable phase structure and clean grain boundaries,which guarantees the superb high-temperature mechanical properties(791±7 MPa for yielding and 1013±11 MPa for failure)at 700℃.Stacking faults(SFs)were observed to prevail during the plastic deformation,offering a high work-hardening capability at 700°*** anomalous rise in the yield strength at 800℃was found,which could be ascribed to the multi-layered super-partial dislocations with a cross-slip configuration within the L1_(2)particles.

关键词： High-entropy alloys Coarsening kinetics Coherent precipitation strengthening Mechanical properties

GO/MgO/Mg interface mediated strengthening and electromagnetic interference shielding in AZ31 composite

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journal of Magnesium and Alloys 2023年第10期11卷 3800-3814页

作者： Z.y.Xu C.F.Fang C.j.Li R.Wang X.P.Zhang j.Tan y.M.Wang Key Laboratory of Solidification Control and Digital Preparation Technology(Liaoning Province) School of Materials Science and EngineeringDalian University of TechnologyDalian 116024China Faculty of Materials Science and Engineering Kunming University of Science and TechnologyKunming 650093China College of Materials Science and Engineering Chongqing UniversityChongqing 400045China Key Laboratory of Materials Modification by Laser Ion and Electron Beams(Ministry of Education)School of Materials Science and EngineeringDalian University of TechnologyDalian 116023China

More requirements of electromagnetic interference(EMI) shielding performance are put forward for lightweight structural materials due to the development of aerospace and 5G communications. Herein, graphene oxide(GO) decorated with SnO_(2) coating is introduced as reinforcement into AZ31 Mg alloy. During the smelting process, the MgO layer is in situ gernerated at interface between GO and the molten Mg alloy matrix by consuming SnO_(2). In the solid state, such kind of interface structure can improve the GO-Mg interface bonding intensity,also significantly generate stacking faults. The AZ31 composite reinfoced by trace modified GO(0.1 wt%) exhibits high ultimate strength and almost the same elongation with AZ31 alloy. Compared with AZ31 alloy, the yield strength and ultimate tensile strength of composite are increased by 33.5% and 23.7%, respectively. Meanwhile, the multi-level electromagnetic reflection from the multi-layer structure of GO and the interface polarization caused by the MgO mid-layer can significantly improve EMI shielding performance. The appropriate interface design strategy achieves the effect of “two birds with one stone”.

关键词： Metal-matrix composites Mechanical properties EMI shielding Microstructures

Simultaneous enhancement of mechanical and shape memory properties by heat-treatment homogenization of Ti_(2)Ni precipitates in TiNi shape memory alloy fabricated by selective laser melting

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journal of Materials Science & Technology 2022年第6期101卷 205-216页

作者： H.Z.Lu L.H.Liu C.yang X.Luo C.H.Song Z.Wang j.Wang y.D.Su y.F.Ding L.C.Zhang y.y.Li National Engineering Research Center of Near-net-shape Forming for Metallic Materials South China University of TechnologyGuangzhou 510640China Musculoskeletal Oncology Department Sun Yat-Sen University Cancer CenterGuangzhouGuangdong ProvinceChina Shenyang Aircraft Design and Research Institute Shenyang 110035China Guangdong Huayi Plumbing Fittings Industry Co. Ltd.Kaiping 529321China School of Engineering Edith Cowan University270 Joondalup DriveJoondalupPerthWA 6027Australia

The excellent shape memory and mechanical properties of Ti Ni shape memory alloys(SMAs) fabricated using selective laser melting(SLM) are highly desirable for a wide range of critical applications. In this study, we examined the simultaneous enhancement of mechanical and shape memory properties using heat-treatment homogenization of Ti_(2)Ni precipitates in a Ti_(50.6)Ni_(49.4)SMA fabricated using SLM. Specifically, because of the complete solution treatment, nanoscale spherical Ti_(2)Ni precipitates were homogeneously dispersed throughout the grain interior. Interestingly, the resultant SMA exhibited an ultrahigh tensile strength of 880 ± 13 MPa, a large elongation of 22.4 ± 0.4%, and an excellent shape memory effect, with a recovery rate of > 98% and ultrahigh recoverable strain of 5.32% after ten loading–unloading cycles. These simultaneously enhanced properties are considerably superior than those of most previously reported Ti Ni SMAs fabricated using additive manufacturing. Fundamentally, the enhancement in tensile strength is ascribed to precipitation strengthening and work hardening, and the large plasticity is mainly attributed to the homogeneous nanoscale globular Ti_(2)Ni precipitates, which effectively impeded the rapid propagation of microcracks. Furthermore, the enhanced shape memory properties are derived from the suppression of dislocation movement and formation of retained stabilized martensite by the presence of high-density dislocations, nanoscale Ti_(2)Ni precipitates, and abundant interfaces. The obtained results provide insight into the enhancement of the two types of properties in Ti Ni SMAs and will accelerate the wider application of SMAs.

关键词： Shape memory alloy Selective laser melting Heat treatment Mechanical properties Shape memory properties

Formation,characteristics and control of sludge in Al-containing magnesium alloys:An overview

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journal of Magnesium and Alloys 2022年第3期10卷 643-658页

作者： y.Fu G.G.Wang A.Hu y.Li K.B.Thacker j.P.Weiler H.Hu Department of Mechanical Automotive and Materials EngineeringUniversity of Windsor401 Sunset AveWindsorON N9B 3P4Canada Global Technology Centre Meridian Lightweight Technologies25 MacNab AveStrathroyON N7G 4H6Canada

Sludge consisting of heavy element phases and oxides is often generated during the casting operation of aluminum(Al)and magnesium(Mg)*** the help of the well-established Sludge Factor(SF)formula,it is relatively easy to control the sludge generation in aluminum *** formation mechanisms and characteristics of sludge in die casting magnesium alloys are still *** ensure the production of high quality die cast components at a low cost,a full understanding of sludge in die casting Mg alloys and its proper control measures need to be developed,since excessive sludge formation affects deleteriously material and operation cost,and casting *** the present report,the formation,characteristics and control of Mg die-casting sludge,based on the established knowledge of sludge formation and sludge factor in Al die casting alloys,are *** work on characterization and assessment of sludge in die cast Mg alloys are *** principles for control of sludge in ingot production in association with die casting of Mg alloys are *** assessment of Mg oxide and intermetallics relevant to sludge formation in Mg alloys are highlighted.

关键词： Sludge Magnesium alloys Die casting Al-Mn(-Fe)intermetallics Magnesium oxide Microstructure characterization

Electron tomography for sintered ceramic materials by a neural network algebraic reconstruction technique

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journal of Materials Science & Technology 2022年第5期100卷 75-81页

作者： R.H.Shen y.T.He W.Q.Ming y.Zhang X.D.Xu j.H.Chen Centre for High Resolution Electron Microscopy College of Materials Science and EngineeringHunan UniversityChangsha 410082China

The missing wedge effect in electron tomography introduces various types of artifacts in the tomograms and lowers the reconstruction resolution and *** artifacts produced in tomographic reconstruction of bulk materials can be very severe,particularly for sintered bulk ceramic materials in which there are often nano-pores or pore-like microstructure ***,we report a neural network algebraic reconstruction algorithm with no prior knowledge to perform electron tomography for a sintered SiC material with nano carbon *** results show that the proposed algorithm has a great suppressive effect on the missing wedge artifacts and a high tolerance for *** information in the missing wedge can be partly recovered by this ***,both the shape of the bulk SiC specimen and its irregular inner pore-like features are correctly retrieved in the obtained 3D *** study shows the effectiveness of the neural network algorithm for improving the reconstruction accuracy of electron tomography,in order to reveal sophisticated 3D microstructures generally existing in sintered ceramic materials.

关键词： Neural network Missing wedge Electron tomography Sintered ceramics

Comparison of microstructure and mechanical behavior of Ti-35Nb manufactured by laser powder bed fusion from elemental powder mixture and prealloyed powder

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journal of Materials Science & Technology 2022年第10期105卷 1-16页

作者： j.C.Wang y.j.Liu S.X.Liang y.S.Zhang L.Q.Wang T.B.Sercombe L.C.Zhang School of Engineering Edith Cowan University270 Joondalup DriveJoondalupPerthWA 6027Australia School of Engineering M050The University of Western Australia35 Stirling HighwayCrawleyPerthWA 6009Australia Northwest Institute for Nonferrous Metal Research Xi’an 710016China State Key Laboratory of Metal Matrix Composites School of Material Science and EngineeringShanghai Jiao Tong UniversityShanghai 200240China

Although different types of powder feedstock are used for additive manufacturing via laser powder bed fusion(L-PBF),limited work has attempted to directly compare the microstructure and mechanical behavior of components manufactured from those powder *** work investigated the microstructure,phase composition,melt pool morphology,and mechanical properties of a prealloyed Ti-35Nb alloy manufactured using L-PBF and compared these to their counterparts produced from elemental powder *** samples manufactured from the powder mixture are composed of randomly distributed undissolved Nb in theα/βmatrix,resulting from the unstable melt pool during the melting of the powder *** contrast,parts produced from prealloyed powder display a homogeneous microstructure withβandαphases,owing to the full melting of prealloyed powder,therefore,a more stable melt pool to achieve a homogeneous *** Ti-35Nb manufactured from prealloyed powder exhibits large tensile ductility(about 10 times that of the counterparts using mixed powder),attributed to the high homogeneity in microstructure and chemical composition,strong interface bonding,relatively low oxygen content,and the existence of a large amount ofβ*** work sheds insights into understanding the effect of powder feedstock on the melt pool stability therefore the microstructure and mechanical behavior of the resultant parts.

关键词： Titanium-niobium Powder bed fusion Additive manufacturing Melt pool stability Microstructure Mechanical properties