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Effect of nanoparticles on the nucleation and agglomeration rates of hydrate growth using THF-water clathrates

Petroleum Science 2020年第2期17卷 467-476页

作者： Syed y.Nahri James L.Nielsen yuanhang chen Craft and Hawkins Department of Petroleum Engineering Louisiana State UniversityBaton RougeLA 70803USA

Four types of nanoparticles,amorphous carbon,ironⅢoxide,SiO2,and amino-coated SiO2,were tested to determine changes in tetrahydrofuran-water(THF-water)clathrate hydrate nucleation and *** were experimentally found to determine their viability for preventing natural gas hydrates from developing during offshore drilling ***-water clathrates were chosen as a model to represent gas hydrate growth at atmospheric *** of each nanoparticle between 0.15%and 1.0%by weight were tested as a kinetic inhibitor to hydrate *** were repeated at various temperatures below the formation temperature of 4.4℃for THF-water clathrate *** were made to identify how the concentration of THF affects the clathrate hydrates forming under static conditions between20%and 30%by mole of *** primary tests in this study were performed using a 20:80 THF/water *** increases during hydrate nucleation for THF-water were measured between-5 and 3℃.The range of ideal nanoparticle concentrations was found to be between 0.15%and 0.45%by weight for optimal static,kinetic inhibition of hydrate *** approximately 0.3%by weight,the most significant inhibition was observed under static conditions for all four types of nanoparticles *** found that functionalized amino-coated SiO2 nanoparticles,across all tests,significantly increased the time required for the formation of THF-water clathrate hydrates compared to the other three non-functionalized *** amorphous carbon and ironⅢoxide nanoparticles performed similarly across each test and were both the least effective in their inhibition of the clathrate hydrates of the four nanoparticles studied compared to a control.

关键词： Nanoparticles Gas hydrates Clathrates Hydrate inhibition Functionalized nanoparticles

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Multi-population particle swarm optimization algorithm for automatic design of steel frames

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Frontiers of Structural and Civil Engineering 2024年第1期18卷 89-103页

作者： Wenchen SHAN Jiepeng LIU yao DING y.Frank chen Junwen ZHOU Institute of Smart City and Intelligent Transportation Southwest Jiaotong UniversityChengdu 610000China School of Civil Engineering Chongqing UniversityChongqing 400045China Department of Civil Engineering the Pennsylvania State UniversityMiddletownPA 17057USA

Steel structures are widely used;however,their traditional design method is a trial-and-error procedure which is neither efficient nor cost ***,a multi-population particle swarm optimization(MPPSO)algorithm is developed to optimize the weight of steel frames according to standard design *** are made to improve the algorithm performances including the constraint-based strategy,piecewise mean learning strategy and multi-population cooperative *** proposed method is tested against the representative frame taken from American standards and against other steel frames matching Chinese design *** related parameter influences on optimization results are *** the representative frame,MPPSO can achieve greater efficiency through reduction of the number of analyses by more than 65% and can obtain frame with the weight for at least 2.4%lighter.A similar trend can also be observed in cases subjected to Chinese design *** addition,a migration interval of 1 and the number of populations as 5 are recommended to obtain better MPPSO *** purpose of the study is to propose a method with high efficiency and robustness that is not confined to structural scales and design *** aims to provide a reference for automatic structural optimization design problems even with dimensional *** proposed method can be easily generalized to the optimization problem of other structural systems.

关键词： steel frame multi-population particle swarm optimization automatic structural optimization design

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Plasma enhanced diamond deposition on steel and Si substrates

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Acta Metallurgica Sinica(English Letters) 2009年第5期22卷 321-329页

作者： y.S. Li y. Tang Wo chen Q. yang C.Xiao A. Hirose Plasma Physics Laboratory University of Saskatchewan Saskatoon SK S7N 5E2 Canada Department of Mechanical Engineering University of Saskatchewan Saskatoon S7N 5A9 Canada

Diamond growth on Fe-Cr-Al-Si steel and Si substrates was comparatively investigated in microwave plasma enhanced chemical vapor deposition （MPCVD） reactor with different deposition parameters. Adherent nanocrystalline diamond films were directly deposited on this steel substrate under a typical deposition condition, whereas microcrystalline diamond films were produced on Si wafer. With increasing CH4 concentration, reaction pressure, or the total gas flow rate, the quality of nanocrystalline diamond films formed on Fe-Cr-Al-Si substrates is gradually deteriorated in terms of density and adhesion. This impaired diamond quality on steels is primarily associated with a combined effect by the substrate composition and the specific process conditions that favor excessive nucleation of diamond.

关键词： Plasma CVD Diamond film Steel Si

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Tensile and cyclic deformation response of friction-stir-welded dissimilar aluminum alloy joints:Strain localization effect

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Journal of Materials Science & Technology 2021年第14期73卷 91-100页

作者： P.L.Niu W.y.Li D.L.chen State Key Laboratory of Solidification Processing Shaanxi Key Laboratory of Friction Welding TechnologiesNorthwestern Polytechnical UniversityXi'an710072.China Department of Mechanical and Industrial Engineering Ryerson University350 Victoria StreetTorontoOntarioM5B2K3Canada

Cyclic deformation behavior of friction-stir-welded dissimilar AA2024-T351 to AA7075-T65 aluminum alloy joints was evaluated via stepwise tests at different strain rates,along with transmission electron microscopy examinations to characterize the precipitates required to assess internal *** backscatter diffraction was employed to observe the inhomogeneous microstructures of the FSWed *** localization appeared in the heat affected zone(HAZ)of AA2024 *** cyclic deformation of 500 cycles at a total strain amplitude of 0.5%,the strength of the dissimilar joints resumed basically to that of AA2024 base *** the AA2024 HAZ was obviously hardened,which should be attributed to the introduced dislocations during cyclic deformation *** hardening capacity of the joints increased with decreasing strain rate.

关键词： Friction stir welding Dissimilar aluminum alloys Strain localization Cyclic hardening Slip irreversibility

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Recent progress in the structure optimization and development of proton-conducting electrolyte materials for low-temperature solid oxide cells

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International Journal of Minerals,Metallurgy and Materials 2022年第4期29卷 848-869页

作者： Jia Song yuvraj y.Birdja Deepak Pant Zhiyuan chen Jan Vaes Separation and Conversion Technology Flemish Institute for Technological Research(VITO)Mol 2400Belgium

This work reviews technologies that can be used to develop low-temperature solid oxide cells(LT-SOCs)and can be applied in fuel cells and electrolyzers operating at temperatures below 500℃,thus providing a more cost-effective alternative than conventional high-temperature *** routes showing potential to reduce the operating temperature of SOCs to below 500℃ are *** first route is the principal way to enhance cell performance,namely,structure *** technique includes the reduction of electrolyte thickness to the nanometer scale and the exploration of electrode structure with low polarization *** other route is the development of novel protonconducting electrolyte materials,which is in the frontier of SOCs *** fundamentals of proton conduction and the design principles of commonly used electrolyte materials are briefly *** most widely studied electrolyte materials for LT-SOCs,namely,perovskitetype BaCeO_(3) -and BaZrO_(3) -based oxides,and the effect of doping on the physical-chemical properties of these oxide materials are summarized.

关键词： low-temperature solid oxide cells perovskite doping thin-film

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Enhancing strength and ductility of AlSi10Mg fabricated by selective laser melting by TiB_(2)nanoparticles

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Journal of Materials Science & Technology 2022年第14期109卷 254-266页

作者： y.K.Xiao H.chen Z.y.Bian T.T.Sun H.Ding Q.yang y.Wu Q.Lian Z.chen H.W.Wang State Key Laboratory of Metal Matrix Composites Shanghai Jiao Tong UniversityShanghai 200240China School of Materials Science&Engineering Shanghai Jiao Tong UniversityShanghai 200240China

In the metallic components fabricated by the emerging selective laser melting(SLM)technology,most strategies used for strengthening the materials sacrifice the ductility,leading to the so-called strengthductility *** the present study,we report that the strength and ductility of materials can be enhanced simultaneously by introducing nanoparticles,which can break the trade-off of the metallic *** the case of in-situ nano-TiB_(2)decorated AlSi10Mg composites,the introduced nanoparticles lead to columnar-to-equiaxed transition,grain refinement and texture *** increasing content of nanoparticles,the strength increases ***,the ductility first increases and then *** results show that the ductility is controlled by the competition between the crack-induced catastrophic fracture and ductile fracture associated with dislocation *** first increase of ductility is mainly attributed to the suppression of crack-induced catastrophic fracture when TiB_(2)nanoparticles *** the further increase of TiB_(2)nanoparticles,the subsequent decrease of ductility is mainly controlled by dislocation ***,the materials will exhibit the optimum strength and ductility combination in a certain range of TiB_(2)*** study clarifies the physical mechanism controlling ductility for nano-TiB_(2)decorated Al Si10Mg composites,which provides the insights for the design of structural materials.

关键词： Selective laser melting Aluminium matrix composites Ductility Mechanical behavior Dislocations Cracks

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Harmonic balance-based approach for optimal time delay to control unstable periodic orbits of chaotic systems

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Acta Mechanica Sinica 2020年第4期36卷 918-925页

作者： y.M.chen Q.X.Liu J.K.Liu Department of Mechanics Sun Yat-sen UniversityGuangzhou 510275China

As a classical technique for chaos suppression,the time-delayed feedback controlling strategy has been widely developed by stabilizing unstable periodic orbits(UPOs)embedded in chaotic systems.A critical issue for achieving high controlling precision is to search for an appropriate time *** paper proposes a simple yet effective approach,based on incremental harmonic balance method,to determine the optimal time delay in the delayed feedback *** time delay is adjusted within the iterative scheme provided by the proposed method,and finally converges to the period of the target *** long as the optimal time delay is fixed,moreover,the attained solution makes it quite convenient to analyze its stability according to the Floquet theory,which further provides the effective interval of the feedback gain.

关键词： Chaos control Unstable periodic orbit Delayed feedback Optimal time delay Incremental harmonic balance method

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Enhanced pitting corrosion resistance of a Zr-based metallic glass by ultraviolet light irradiation

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Journal of Iron and Steel Research International 2023年第8期30卷 1642-1649页

作者： Z.chen D.P.Wang S.Wang y.X.Geng y.X.Guo y.C.Wu Z.G.Liu y.y.Zhang y.X.Wang School of Materials Science and Engineering Jiangsu University of Science and Technology.Zhenjiang 212003JiangsuChina School of Mechanical Engineering Jiangsu University of Science and TechnologyZhenjiang 212003JiangsuChina

The influence of ultraviolet light irradiation on the pitting corrosion performance of a Zr_(2)Ni metallic glass was examined using electrochemical methods and immersion test in 0.05 mol/L NaCl *** the results of potentiostatic polarization,the pitting potential of the ultraviolet light-irradiated sample shifted positively with a value of~300 mV,revealing the enhanced pitting corrosion resistance of the *** corrosion morphology after the immersion test also demonstrated lower degree of corrosion damage and improved pitting resistance of the sample with ultraviolet light irradiation.X-ray photoelectron spectroscopy analysis revealed more zirconium enrichment in the passive film and no chloride ions adsorption for the samples with ultraviolet irradiation,accounting for the suppression of the pit generation and *** findings indicate that ultraviolet light irradiation improves the pitting corrosion resistance of the Zr-based metallic glasses,which are promising structural materials to be used in corrosion environments with high ultraviolet irradiation.

关键词： Metallic glass Pitting-Corrosion Ultraviolet light irradiation Passive film

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MICROSTRUCTURE AND INCLUSION CHARACTERIZATION IN THE SIMULATED COARSE-GRAIN HEAT AFFECTED ZONE WITH LARGE HEAT INPUT OF A Ti-Zr-MICROALLOyED HSLA STEEL

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Acta Metallurgica Sinica(English Letters) 2005年第2期18卷 96-106页

作者： y.T.chen X.chen Q.F.Ding J.Zeng TechnologyCenter WuhanIronandSteel（group）CooperationWuhan430080China

The microstructure and the characteristics of the inclusions embedded in ferrite matrix in simulated coarse-grain heat affected zone (CGHAZ) of a Ti-Zr-treated high strength low alloy (HSLA) steel have been investigated. The microstructure of the simulated CGHAZ dominantly consisted of intragranular acicular ferrite (IAF) combining with a small amount of polygonal ferrite (PF), widmanst tten ferrite (WF), bainite ferrite (BF), pearlite and martensite-austenite (M-A) islands. The PF, WF and BF were generally observed at the prior austenite grain boundaries and the interlocking acicular ferrite was usually found intragranularly. It was found that the inclusions were composed of Ti2O3, ZrO2, Al2O3 locating at the center of the particles and MnS lying on the surface layer of the inclusions. The intragranular complex inclusions promoted the acicular ferrite formation and the refinement of microstructure whilst those at prior austenite grain boundaries caused PF formation on the inclusions. The simulated CGHAZ consisting of such complicated microstructure exhibited desired mechanical properties.

关键词： microalloyed HSLA steel heat affected zone microstructure mechanical property inclusion acicular ferrite titanium zirconium

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PREPARATION OF MULTI-WALLED CARBON NANOTUBES USING NiO CATALyST SyNTHESIZED By HyDROTHERMAL METHOD

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Acta Metallurgica Sinica(English Letters) 2003年第5期16卷 416-420页

作者： y.J.Zhu y.L.chen X.M.Xue y.M.chen C.y.Wu T.C.Kuang S.H.Li H.y.Zhang DepartmentofAppliedPhysics GuangdongUniversityofTechnologyGuangzhou510090China CenterofAnalysisTesting GuangdongUniversityofTechnologyGuangzhou510O9OChina FacultyofMaterialandEnergy GuangdongUniversityofTechnologyGuangzhou510090.China

The Ni(OH)2/SiO2 binary colloid was prepared using Ni(NO3)2.6H2O and (C2H5O)4SiO4 as starting materials and was used to form NiO/SiO2. composite powder by hydrothermal method and desiccant method in open air respectively. Multi-walled carbon nanotubes (MWCNTs) were synthesized respectively by chemical vapor deposition using the NiO/SiO2 catalyst prepared by different methods. The phase and morphology of the catalysts and the morphology, output yield and purity of MWCNTs were compared by XRD, TEM and SEM. The results show that the catalyst powder prepared by hydrothermal method, compared with that by desiccant method, is smaller, better dispersion and has stronger catalytic activity. Pure MWCNTs with smaller tube diameter and narrow range could be obtained at a high yield using that NiO/SiO2 powder prepared by hydrothermal method as catalyst.

关键词： hydrothermal method dry method at atmosphere carbon nan- otube catalytic pyrolysis

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