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Preface

Journal of Iron and Steel Research(International) 2024年第6期31卷 1289-1290页

作者： Ao Huang Bei-yue Ma xin-mei hou Sheng-li Jin Xu-dong Luo State Key Laboratory of Refractories and Metallurgy and Faculty of Materials Wuhan University of Science and TechnologyWuhan 430081HubeiChina School of Metallurgy Northeastern UniversityShenyang 110819LiaoningChina Institute for Carbon Neutrality University of Science and Technology BeijingBeijing 100083China Chair of Ceramics Montanuniversitaet LeobenLeoben 8700StyriaAustria School of Metallurgy and Materials Engineering Liaoning Institute of Science and TechnologyBenxi 117004LiaoningChina

This special issue is dedicated to the 3Oth anniversary of Journal of Iron and Steel Research *** the past 30 years,Journal of Iron and Steel Research International has been focusing on the academic research and advan... 详细信息

关键词： materials. metallic Preface

Effect and mechanism of nano-Ca_(10)(PO_(4))_(6)(OH)_(2)additive on compressive strength of calcium aluminate cement at high temperature

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Journal of Iron and Steel Research(International) 2022年第7期29卷 1063-1072页

作者： Qian Sun En-hui Wang xin-mei hou Zhi-jun He Tong-xiang Liang Collaborative Innovation Center of Steel Technology University of Science and Technology BeijingBeijing 100083China School of Material and Metallurgy University of Science and Technology LiaoningAnshan 114501LiaoningChina School of Materials Science and Engineering Jiangxi University of Science and TechnologyGanzhou 341000JiangxiChina

Calcium aluminate cement(CAC)is widely used as a binder for refractory materials,and thus the improvement in compressive strength is of vital importance for CAC applied at high *** this purpose,nano-Ca_(10)(PO_(4))_(6)(OH)_(2)additive with a ratio of 0.5–1.5 mass%was added with the water-cement ratio to be 0.4.X-ray diffraction and isothermal calorimetry analysis demonstrate that nano-Ca_(10)(PO_(4))_(6)(OH)_(2)additive can shorten the hydration process and promote the formation of main hydrates of CaAl2O4·10H2O(CAH10)and Ca2Al2O5·8H2O(C2AH8).In addition,scanning electron microscopy results suggest that nano-Ca_(10)(PO_(4))_(6)(OH)_(2)can protect CAH10 and C2AH8 from being destroyed during the calcination,guaranteeing that these thin lamellar crystals are intertwined to form the denser *** from above effects,nano-Ca_(10)(PO_(4))_(6)(OH)_(2)can obviously improve the compressive strength of the CAC mortar samples cured for 7 d after calcination at 1100°C,while the improving effect is dependent upon its ***,compared with the one without the additive,the compressive strength of the sample with 1.0%nano-Ca_(10)(PO_(4))_(6)(OH)_(2)is increased by 14%.

关键词： Nano-Ca_(10)(PO_(4))_(6)(OH)_(2) Cement Calcination Microstructure Compressive strength

Preparation and photo-catalytic activity of TiO_2-coated medical stone-based porous ceramics

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International Journal of Minerals,Metallurgy and Materials 2013年第6期20卷 593-597页

作者： Ru-qin Gao xin-mei hou School of Environmental and Municipal Engineering North China University of Water Resources and Electric Power School of Metallurgical and Ecological Engineering University of Science and Technology Beijing

Medical stone-based porous ceramics as a carrier were prepared by ultra-fine grinding and low-temperature sintering method. Nano-TiO~ thin films were loaded on the carrier by chemical liquid deposition method using titanium tetrachloride as a precursor. The micro-morphology and microstructure of the synthesized samples were characterized using X-ray diffraction, scanning electron microscopy with energy dispersive spectrometry, and mercury injection method. The photo-catalytic activity of the TiO2 thin films was investigated by degrading formaldehyde. The main crystalline phase in the TiO2 thin films calcined at 550~C is anatase with the average particle size about 10 nm. The specific surface area of the carrier-coated nano-TiO2 increases from 3.68 to 5.32 m2/g. The formaldehyde removal rate of the TiO2/medical stone-based porous ceramics irradiated under an ultraviolet lamp for 120 min reaches 85.6%.

关键词： porous materials ceramics medical stone titanium dioxide thin films formaldehyde photocatalysis

Thermal oxidation of SiAlON powders synthesized from coal gangue

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International Journal of Minerals,Metallurgy and Materials 2011年第1期18卷 77-82页

作者： xin-mei hou Chang-sheng Yue mei Zhang Kuo-chih Chou School of Metallurgical and Ecological Engineering University of Science and Technology Beijing Beijing 100083 China The Key Laboratory of Ecological ＆ Recycle Metallurgy Ministry of Education of China Beijing 100083 China

The oxidation behavior of different SiAlON phases（β-SiAlON,X-phase SiAlON and 12H powders） synthesized from coal gangue in air atmosphere was investigated using isothermal thermogravimetry（TG） and field-emission scanning electron microscopy（FE-SEM）.The effect of ferric oxide impurities in coal gangue was *** results show that ferric oxide contributes to the growth of SiAlON crystalline during the synthesis *** the oxidation experiment,the existence of ferric oxide decreases the oxidation resistance of *** reason is that the impurity causes the formation of a liquid phase at a higher *** 1423-1623 K,the oxidation of SiAlON powders is diffusion controlled and it can be described by Chou＇s model.A fair agreement is found between theoretical calculations and the experimental data.

关键词： oxidation kinetics silicon compounds powders coal

Reaction mechanisms for 0.5Li_2MnO_3 ·0.5LiMn_(0.5)Ni_(0.5)O_2 precursor prepared by low-heating solid state reaction

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International Journal of Minerals,Metallurgy and Materials 2012年第9期19卷 856-862页

作者： Dong Li Fang Lian xin-mei hou Kuo-chih Chou School of Materials Science and Engineering University of Science and Technology Beijing Beijing 100083 China Department of Physical Chemisitry University of Science and Technology Beijing Beijing 100083 China

Lithium-excess manganese layered oxides, which are commonly described in chemical formula 0.5Li2MnO3·0.5LiMn0.5Ni0.5O2, were prepared by low-heating solid state reaction. The reaction mechanisms of synthesizing precursors, the decomposition mechanism, and intermediate materials in calcination were investigated by means of Fourier transform infrared spectroscopy （FT-IR）, X-ray diffraction （XRD）, field emission scanning electron microscopy （FESEM）, thermogravimetric analysis （TGA）, and differential scanning calorimetry （DSC）. The major diffraction patterns of 0.5Li2MnO3·0.5LiMn0.5Ni0.5O2 powder calcinated at 720℃ for 15 h are indexed to the hexagonal structure with a space group of R3m, and the clear splits of doublets at （006）/（102） and （108）/（110） indicate that the sample adopts a well-layered structure. FESEM images show that the size of the agglomerated particles of the sample ranges from 100 to 300 nm.

关键词： lithium batteries electrode manganese oxide solid state reactions calcination

Tunable fabrication of single-crystalline CsPbI_(3) nanobelts and their application as photodetectors

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International Journal of Minerals,Metallurgy and Materials 2021年第6期28卷 1030-1037页

作者： Tao Yang Ya-peng Zheng Kuo-Chih Chou xin-mei hou Collaborative Innovation Center of Steel Technology University of Science and Technology BeijingBeijing 100083China

Lead halide perovskites have received increasing attention recently as a candidate material in various optoelectronic areas because of their high performance as light ***,we report the growth of CsPbI_(3) nanobelts via a solution process.A single-crystalline CsPbI_(3) nanobelt with uniform morphology can be achieved by controlling the amount of PbI_(2).A single-crystalline CsPbI_(3) nanobelt possesses a mean width,length,and thickness of 100 nm,5μm,and 20 nm,*** this work,photodetectors(PDs)based on individual CsPbI_(3) nanobelts are constructed and found to perform well with an external quantum efficiency and responsivity of 2.39×10^(5)% and 770 A/W,*** PDs also show a high detectivity of up to 3.12×10^(12) Jones,which is at par with that of Si *** PDs developed in this work exhibit great promise in various optoelectronic nanodevices.

关键词： photodetector cesium lead triiodide perovskite nanobelt detectivity

High-performance chromite by structure stabilization treatment

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Journal of Iron and Steel Research(International) 2020年第2期27卷 169-179页

作者： En-hui Wang Chang Luo Jun-hong Chen xin-mei hou Collaborative Innovation Center of Steel Technology University of Science and Technology BeijingBeijing 100083China School of Materials Science and Engineering University of Science and Technology BeijingBeijing 100083China

Chromite is an important raw material applied in *** have been made to obtain high-performance chromite by adding MgO and Al203 from the viewpoint of structure *** order to explore the effect of Al203 and MgO on the structure,two formulas,i.e.,Mg-rich and Al-rich ones,were *** phase and microstructure development of samples heated in the temperature range of 1200-1600℃ were studied by X-ray diffraction and scanning electron microscopy with energy-dispersive *** and Al203 added have diffused into chromite successfully by heat *** diffuses into chromite,occupying the tetrahedral vacancies caused by the diffusion and oxidation of Fe2+ions to stabilize the ***203 diffuses into the surface layer of chromite,forming spinel-sesquioxide ***-rich sample which has spinel-sesquioxide structure shows better corrosion resistance toward fayalite slag than Mg-rich sample which has single spinel structure by blocking the interdiffusion between Fe^2+ions in fayalite slag and Mg^2+ions in chromite.

关键词： Chromite Structure optimization Corrosion resistance Refractory

Metal-organic-framework-derived copper-based catalyst for multicomponent C-S coupling reaction

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Chinese Journal of Chemical Engineering 2024年第6期70卷 1-8页

作者： Lixin Chen Hui Zhang Linxi hou xin Ge Key Laboratory of Synthetic and Biological Colloids Ministry of EducationSchool of Chemical and Material EngineeringJiangnan UniversityWuxi 214122China Department of Materials-Oriented Chemical Engineering School of Chemical EngineeringFuzhou UniversityFuzhou 350116China Qingyuan Innovation Laboratory Quanzhou 362801China

Copper-based metal-organic frameworks(Cu-MOFs)are a promising multiphase catalyst for catalyzing C-S coupling reactions by virtue of their diverse structures and ***,the unpleasant odor and instability of the organosulfur,as well as the mass-transfer resistance that exists in multiphase catalysis,have often limited the catalytic application of Cu-MOFs in C-S coupling *** this paper,a Cu-MOFs catalyst modified by cetyltrimethylammonium bromide(CTAB)was designed to enhance mass transfer by increasing the adsorption of organic substrates using the long alkanes of ***,elemental sulfur was used to replace organosulfur to achieve a highly efficient and atom-economical multicomponent C-S coupling reaction.

关键词： Design Copper-based metal-organic frameworks (Cu-MOFs) Adsorption C-S coupling reaction Multiphase reaction

Dissolution and diffusion of TiO_2 in the CaO-Al_2O_3-SiO_2 slag

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International Journal of Minerals,Metallurgy and Materials 2014年第4期21卷 345-352页

作者： Zhong-shan Ren Xiao-jun Hu xin-mei hou Xiang-xin Xue Kuo-chih Chou State Key Laboratory of Advanced Metallurgy University of Science and Technology Beijing School of Metallurgical and Ecological Engineering University of Science and Technology Beijing School of Materials and Metallurgy Northeastern University

The dissolution of TiO2 in the CaO-Al2O3-SiO2 slag under static conditions was studied in the temperature range from 1643 K to 1703 K. After TiO2 dissolved, the microstructure of the interface between TiO2 and the slag was observed by scanning electron microscopy, and the concentration profiles of Ti4＋and other ions across the TiO2/slag interfaces were analyzed by energy-dispersive X-ray spectroscopy. On the basis of these results, the dissolution behavior of TiO2 was evaluated, and the diffusivity of Ti4＋in the bulk slag was estimated. Ac-cording to the Stokes-Einstein relation, the viscosity calculated by a previously reported model gave a diffusivity of Ti4＋ions greater than that estimated by the concentration profiles of Ti4＋ions. The mechanism of TiO2 dissolution in the CaO-Al2O3-SiO2 slag is discussed in de-tail.

关键词： slags titanium dioxide dissolution diffusion interface