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A micro-crosslinked amphoteric hydrophobic association copolymer as high temperature-and salt-resistance fluid loss reducer for water-based drilling fluids

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Petroleum Science 2024年第3期21卷 1980-1991页

作者： Jian Li Yu-Xi Ji Xiao-Xiao Ni Kai-He Lv xian-bin huang Jin-Sheng Sun School of Petroleum Engineering China University of Petroleum(East China)Qingdao266580ShandongChina Key Laboratory of Unconventional Oil&Gas Development China University of Petroleum(East China)Qingdao26650ShandongChina Inspection and Testing Center of Huabei Oil Field Company PetroChinaRenqiu062552HebeiChina Drilling Fluid Research Institute CNPC Engineering Technology R&D Company LimitedBeijing102206China

During ultradeep oil and gas drilling,fluid loss reducers are highly important for water-based drilling fluids,while preparing high temperature-and salt-resistance fluid loss reducers with excellent rheology and filtration performance remains a ***,a micro-crosslinked amphoteric hydrophobic association copolymer(i.e.,DADC)was synthesized using N,N-dimethyl acrylamide,diallyl dimethyl ammonium chloride,2-acrylamido-2-methylpropane sulfonic acid,hydrophobic monomer,and pentaerythritol triallyl ether *** to the synergistic effects of hydrogen bonds,electrostatic interaction,hydrophobic association,and micro-crosslinking,the DADC copolymer exhibited outstanding temperature-and *** rheological experiments have shown that the DADC copolymer had excellent shear dilution performance and a certain degree of salt-responsive viscosity-increasing *** DADC copolymer could effectively adsorb on the surface of bentonite particles through electrostatic interaction and hydrogen bonds,which bring more negative charge to the bentonite,thus improving the hydration and dispersion of bentonite particles as well as the colloidal stability of the drilling ***,the drilling fluids constructed based on the DADC copolymer exhibited satisfactory rheological and filtration properties(FLHTHP=12 m L)after aging at high temperatures(up to200℃)and high salinity(saturated salt)***,this work provided new insights into designing and fabricating high-performance drilling fluid treatment agents,demonstrating good potential applications in deep and ultradeep drilling engineering.

关键词： Fluid loss reducer Temperature-and salt-resistance Hydrophobic association Amphoteric Micro-crosslinking

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Improving the anti-collapse performance of water-based drilling fluids of Xinjiang Oilfield using hydrophobically modified silica nanoparticles with cationic surfactants

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Petroleum Science 2023年第3期20卷 1768-1778页

作者： He Li xian-bin huang Jin-Sheng Sun Kai-He Lv Xu Meng Zhen Zhang Key Laboratory of Unconventional Oil&Gas Development(China University of Petroleum(East China) Ministry of Education)Qingdao266580ShandongPR China School of Petroleum Engineering China University of Petroleum(East China)Qingdao266580ShandongPR China PetroChina Tarim Oilfield Company Korla841000XinjiangPR China

Wellbore instability,especially drilling with water-based drilling fluids(WBDFs)in complex shale for-mations,is a critical challenge for oil and gas *** purpose of this paper is to study the feasibility of using hydrophobically modified silica nanoparticle(HMN)to enhance the comprehensive performance of WBDFs in the Xinjiang Oilfield,especially the anti-collapse *** effect of HMN on the overall performance of WBDFs in the Xinjiang Oilfield,including inhibition,plugging,lu-bricity,rheology,and filtration loss,was studied with a series of *** mechanism of HMN action was studied by analyzing the changes of shale surface structure and chemical groups,wettability,and capillary *** experimental results showed that HMN could improve the performance of WBDFs in the Xinjiang Oilfeld to inhibit the hydration swelling and dispersion of *** plugging and lubrication performance of the WBDFs in the Xinjiang Oilfield were also enhanced with HMN based on the experimental *** had less impact on the rheological and filtration performance of the WBDFs in the Xinjiang *** addition,HMN significantly prevented the decrease of shale *** potential mechanism of HMN was as *** chemical composition and structure of the shale surface were altered due to the adsorption of HMN driven by electrostatic *** of the shale surface resulted in significant wettability *** capillary force of the shale was converted from a driving force of water into the interior to a *** summary,hydrophobic nanoparticles presented afavorable application potential for WBDFs.

关键词： Hydrophobic nanoparticle Wetting alteration Wellbore stability Water-based drilling fluids Shale

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Laponite:a promising nanomaterial to formulate high-performance water-based drilling fluids

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Petroleum Science 2021年第2期18卷 579-590页

作者： xian-bin huang Jin-Sheng Sun Yi huang Bang-Chuan Yan Xiao-Dong Dong Fan Liu Ren Wang Key Laboratory of Unconventional Oil and Gas Development China University of Petroleum(East ChinaMinistry of Education)Qingdao266580ShandongPeople’s Republic of China School of Petroleum Engineering China University of Petroleum(East China)Qingdao266580ShandongPeople’s Republic of China Zhanjiang Branch of China National Offshore Oil Corporation Limited Zhanjiang524057GuangdongChina CNPC Engineering Technology R&D Company Limited Beijing102206People’s Republic of China

High-performance water-based drilling fluids(HPWBFs)are essential to wellbore stability in shale gas exploration and *** is a synthetic hectorite clay composed of disk-shaped *** paper analyzed the application potential of laponite in HPWBFs by evaluating its shale inhibition,plugging and lubrication *** inhibition performance was studied by linear swelling test and shale recovery *** performance was analyzed by nitrogen adsorption experiment and scanning electron microscope(SEM)*** pressure lubricity test was used to evaluate the lubrication *** results show that laponite has good shale inhibition property,which is better than commonly used shale inhibitors,such as polyamine and *** can effectively plug shale *** considerably decreases the surface area and pore volume of shale,and SEM results show that it can reduce the porosity of shale and form a seamless *** is beneficial to increase lubricating property of drilling fluid by enhancing the drill pipes/wellbore interface smoothness and isolating the direct contact between wellbore and drill ***,laponite can reduce the fluid loss *** to mechanism analysis,the good performance of laponite nanoparticles is mainly attributed to the disk-like nanostructure and the charged surfaces.

关键词： Laponite Nanoparticles High performance Drilling fluid Shale gas

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Carbon nanotube enhanced water-based drilling fluid for high temperature and high salinity deep resource development

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Petroleum Science 2022年第2期19卷 916-926页

作者： Jing-Ping Liu xian-Fa Zhang Wen-Chao Zhang Kai-He Lv Yin-Rui Bai Jin-Tang Wang xian-bin huang Jia-Feng Jin Jin-Sheng Sun College of Petroleum Engineering China University of Petroleum(East China)Qingdao 266580China CNPC Engineering Technology R&D Company Limited Beijing 102206China

Drilling fluids face failure during drilling deep reservoir with high temperature and high *** experimental results show that high temperature and salinity reduce the negative charge on the surface of bentonite in the drilling fluid and cause the coalescence of bentonite *** a result,the particles coalesce,the grid structure is destroyed,and the rheological properties,rock-carrying capacity and filtration properties are *** resolve the foregoing,in this study,0.05-wt%carbon nanotubes are introduced into a 4%bentonite drilling fluid under conditions where the temperature and concentration of added Na Cl reach 180°C and 10 wt%,*** carbon nanotubes adsorb on the bentonite surface and increase the space among bentonite *** steric hindrance prevents the coalescence of bentonite in high temperature and high salt *** bentonite maintains the small size distribution of bentonite and supports the bentonite grid structure in the drilling *** a result,the rock-carrying capacity of the drilling fluid increases by 85.1%.Moreover,the mud cake formed by the accumulation of small-sized bentonite particles is dense;consequently,the filtration of bentonite drilling fluid reduced by 30.2%.

关键词： High temperature Water-based drilling fluid High salinity Carbon nanotube Deep resources

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Combustion mechanism of benzene in iron ore sintering process:experimental and simulation

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Journal of Iron and Steel Research International 2024年第1期31卷 195-203页

作者： Zhi-gang Que Jin-ming Shi xian-bin Ai Institute of Energy Research Jiangxi Academy of ScienceNanchang330096JiangxiChina Jiangxi Carbon Neutralization Research Center Nanchang330096JiangxiChina

Benzene is a typical component of volatile organic compounds(VOCs)in the iron ore sintering flue *** combustion behavior of benzene directly affects the emission of VOCs in iron ore sintering *** effects of temperature,benzene,and oxygen concentrations on the conversion ratio of benzene were investigated by experiments and numerical *** experiments were carried out in a tube reactor at temperatures of 773-1098 K,benzene concentrations of 0.01-0.03 vol.%,and oxygen concentrations of 10-21 vol.%.The numerical simulation was performed with the plug flow model in the CHEMKIN program based on a kinetic model that consists of 132 chemical species and 772 elementary step-like *** experimental results reveal that increasing the temperature and benzene concentration could signifi-cantly promote benzene *** is attributed to the increase in the reaction rates of all steps in the pathway for forming CO_(2)and H_(2)*** addition,due to the large equivalent ratio of oxygen to benzene,the conversion ratio of benzene remained constant at different oxygen *** simulation results were in good agreement with the experimental results and indicated that six elementary reactions dominated the formations of CO_(2)and H_(2)*** oxidations of C_(6)H_(5)O,CO,and C_(5)H_(4)O intermediates to CO_(2)were the limiting steps in the reaction pathways.

关键词： Benzene Volatile organic compound Iron ore sinter Combustion Simulation Temperature Oxygen

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Sub-Nyquist sampling-based wideband spectrum sensing:a compressed power spectrum estimation approach

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Frontiers of Computer Science 2024年第2期18卷 139-145页

作者： Jilin WANG Yinsen huang bin WANG National Key Laboratory of Science and Technology on Communications University of Electronic Science and Technology of ChinaChengdu 611731China

In this paper,we introduce a sub-Nyquist sampling-based receiver architecture and method for wideband spectrum *** of recovering the original wideband analog signal,the proposed method aims to directly reconstruct the power spectrum of the wideband analog signal from sub-Nyquist *** that power spectrum alone is sufficient for wideband spectrum *** only the covariance matrix of the wideband signal is needed,the proposed method,unlike compressed sensing-based methods,does not need to impose any sparsity requirement on the frequency *** proposed method is based on a multi-coset sampling *** exploiting the inherent sampling structure,a fast compressed power spectrum estimation method whose primary computational task consists of fast Fourier transform(FFT)is *** results are presented to show the effectiveness of the proposed method.

关键词： wideband spectrum sensing sub-Nyquist multicoset sampling FCPSE

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Study on the four Qi of Pfaffia glomerata based on the metabolomics technology and comparison of Dangshen(Radix Codonopsis) in the equivalent substitution prescription

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Journal of Traditional Chinese Medicine 2024年第4期44卷 713-721页

作者： SONG Zhenguang YANG bin WANG Fei YAN Dongmei ZHOU Xiaoqing huang Liping GAO Xuemei LI bin huang Luqi Academician Workstation Jiangxi University of Chinese MedicineNanchang 330004China State Key Laboratory of Characteristic Chinese Medicine Resources in Southwest China School of PharmacyChengdu University of Traditional Chinese MedicineChengdu 610075China National Resource Center for Chinese Materia Medica Chinese Academy of Chinese Medical Sciences(CACMS)Beijing 100700China

OBJECTIVE:To explore the four Qi of Pfaffia glomerata(PG)and endow this foreign folk herb with the properties of Chinese medicine,make it Chinese medicinal and localized,and could be used as a Chinese ***:The normal group,six cold herb groups,six hot herb groups,six cool herb groups,PG prescription group(PGPG),and Dangshen(Radix Codonopsis)prescription group(CPPG)were prepared with corresponding concentrations of water extracts,these herb extracts were administered by gavage to SpragueDawley rats,and the 12 h urine at night on the 29th day of the SD rats in each group were collected,Liquid Chromatograph Mass Spectrometer system was used to analyze them,the best discriminant models for the medicinal properties of cold-hot and cold-cool were set up,so as to the medicinal properties of PGPG,CPPG and PG were *** on the Progenesis QI,Human Metabolome Database,Kyoto Encyclopedia of Genes and Genomes,MetaboAnalyst 5.0 database,we enriched metabolic pathway and classification mechanism of medicinal properties of cold-cool Chinese herbs and the molecular mechanism of PG ***:We established a best model of cold-hot herbal discrimination in the positive ion mode,then the probability that PGPG was predicted cold property was 88.9%.Furthermore,a model of cold-cool herbal discrimination was established,then the probability of PGPG containing the cool property was 77.8%.In addition,typical cold and cool herbs mainly affected nine biomarkers such as tyrosine-proline,(R)-3',7-Dihydroxy-2',4'-dimethoxyisoflavane in *** regulation trend of PGPG on markers was basically as same as the cool herbs and mainly involved in regulating the two pathways of cytochrome P450 and purine ***:The results showed PGPG had a cool medicinal property as same as CPPG,and the regulation trend of PGPG on markers was consistent with cool ***,the medicine properties PG and CP should be consistent,and the Traditional Chinese Medicine p

关键词： Pfaffia glomerata medicinal properties of Chinese medicine metabolomics molecular mechanism equivalent substitution

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Shape embedding and retrieval in multi-ﬂow deformation

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Computational Visual Media 2024年第3期10卷 439-451页

作者： Baiqiang Leng Jingwei huang Guanlin Shen bin Wang School of Software Tsinghua UniversityBeijingChina Huawei Technologies ShenzhenChina

We propose a unified 3D ﬂow frameworkfor joint learning of shape embedding and deformationfor different categories. Our goal is to recovershapes from imperfect point clouds by fitting thebest shape template in a shape repository afterdeformation. Accordingly, we learn a shape embeddingfor template retrieval and a ﬂow-based network forrobust deformation. We note that the deformationﬂow can be quite different for different shapecategories. Therefore, we introduce a novel multi-hubmodule to learn multiple modes of deformation toincorporate such variation, providing a network whichcan handle a wide range of objects from differentcategories. The shape embedding is designed to retrievethe best-fit template as the nearest neighbor in a latentspace. We replace the standard fully connected layerwith a tiny structure in the embedding that significantlyreduces network complexity and further improvesdeformation quality. Experiments show the superiorityof our method to existing state-of-the-art methods viaqualitative and quantitative comparisons. Finally, ourmethod provides efficient and flexible deformation thatcan further be used for novel shape design.

关键词： deformation shape retrieval embedding reconstruction

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High-efficiency Multiplexed Buck-type PFC Converter

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CSEE Journal of Power and Energy Systems 2024年第3期10卷 1053-1063页

作者： Lunquan Li Qianhong Chen Jichao huang bin Liu School of Automation Nanjing University of Aeronautics and AstronauticsNanjing 211106China Gaoyi Zhineng Electric Ltd. Shenzhen 518101China School of Information Engineering Nanchang Hang Kong UniversityNanchang 330063China IEEE CSEE

This paper proposes a high-efficiency PFC rectifier based on multiplexing the *** with a traditional six-switch PFC rectifier,the proposed rectifier extends the switches’active angle by making use of three bridge *** a result,lower conduction resistance can be realized for ***,system efficiency can be *** with a traditional six-switch PFC rectifier with doubled switches,the proposed rectifier can achieve almost the same efficiency improvement while no additional switches are *** continuous inductor current is chopped and resulting current pulses cannot be injected into the grid directly,input filter design and resonance damping are discussed for the proposed *** controller design of the rectifier is *** inductor current reference is shaped considering the input voltage envelope and forward ***,the effectiveness of the proposed rectifier is verified through simulations and experiments.

关键词： Buck-type rectifier commutation state controller design efficiency multiplex

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Highly Improved Creep Resistance in Polypropylene Through Thermally Reduced Graphene Oxide and Its Creep Lifetime Prediction

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Chinese Journal of Polymer Science 2024年第2期42卷 256-266,I0010页

作者： Can-Can Zhang Jun-Long Yang Ya-Jiang huang Guang-xian Li College of Polymer Science and Engineering State Key Laboratory of Polymer Materials Engineering of ChinaSichuan UniversityChengdu610065China

Polypropylene(PP) exhibits suboptimal creep resistance due to the presence of methyl groups on its main chain, leading to irregular chain segment distribution, diminished inter-chain interaction, and crystallinity. This structural feature causes chain slippage in PP under stress,significantly constraining its service lifetime. In this study, thermally reduced graphene oxide(TrGO) nanosheets were incorporated into the PP matrix, yielding a nanocomposite with exceptional creep resistance performance. Results demonstrated that at a stress of 25 MPa, a 2.0 wt% TrGO content could enhance the creep failure lifetime of PP by 21.5 times compared to neat PP. Rheology, transmission electron microscopy(TEM),and scanning electron microscopy(SEM) characterization techniques were employed to analyze the mechanism of TrGO's influence on PP's creep behavior. It was observed that when TrGO content exceeded 1.0 wt%, an effective particle network structure formed within the PP matrix. This homogeneously dispersed TrGO-formed particle network structure restricted the migration and rearrangement of PP molecular chains, enabling prolonged stress resistance without structural failure. By combining the time-strain superposition method with the critical failure strain as a criterion, generalized creep compliance curves for PP and its composites were established, facilitating the prediction of material creep failure lifetimes, with a strong agreement between experimental and predicted lifetime values. This research proposes a novel strategy aimed at developing polypropylene materials and products with enhanced long-term stability and durability, thus extending service life, reducing failure risk, and broadening their potential across various application domains.

关键词： Thermally reduced graphene oxide Polypropylene Creep failure and lifetime prediction

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