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Efficient concentration of trace analyte with ordered hotspot construction for a robust and sensitive SERS platform

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International Journal of Extreme Manufacturing 2024年第3期6卷 532-542页

作者： Youdi hu Yanlei hu Zhenyu wang Jiale Yong wei Xiong Dong wu Shixiang Xu Shenzhen Key Laboratory of Micro-Nano Photonic Information Technology College of Physics and Optoelectronic EngineeringShenzhen UniversityShenzhenGuangdong 518060People’s Republic of China CAS Key Laboratory of Mechanical Behavior and Design of Materials Key Laboratory of Precision Scientific Instrumentation of Anhui Higher Education InstitutesDepartment of Precision Machinery and Precision InstrumentationUniversity of Science and Technology of ChinaHefeiAnhui 230027People’s Republic of China wuhan National Laboratory for Optoelectronics Huazhong University of Science and TechnologyWuhanHubeiPeople’s Republic of China

Surface-enhanced Raman scattering(SERS)platform,which enables trace analyte detection,has important application *** structuring/modifying the surface of the SERSsubstrate,analyte in highly diluted solutions can be concentrated into localized active areas for highly sensitive ***,subject to the difficulty of the fabrication process,itremains challenging to balance hot-spot construction and the concentration capacity of analyte ***,preparing SERS substrates with densely ordered hot spots andefficient concentration capacity is of great significance for highly sensitive ***,we propose an Ag and fluoroalkyl-modified hierarchical armour substrate(Ag/F-HA),which has a double-layer stacking design to combine analyte concentration with hotspot *** microarmour structure is fabricated by femtosecond-laser processing to serve as asuperhydrophobic and low-adhesive surface to concentrate analyte,while the anodic aluminium oxide(AAO)template creates a nanopillar array serving as dense and ordered hot *** the synergistic action of hot spots and analyte concentration,Ag/F-HA achieves a detectionlimit down to 10^(-7)M doxorubicin(DOX)molecules with a RSD of 7.69%.Additionally,Ag/F-HA exhibits excellent robustness to resist external disturbances such as liquid splash or *** on our strategy,SERS substrates with directional analyte concentrations are further explored by patterning microcone arrays with *** work opens a way to the realistic implementation of SERS in diverse scenarios.

关键词： surface-enhanced Raman scattering anodic aluminium oxide femtosecond laser processing concentration of trace analytes mechanical robustness

Dynamic Response of Foundations during Startup of High-Frequency Tunnel Equipment

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Computer Modeling in Engineering & Sciences 2024年第7期140卷 821-844页

作者： Dawei Ruan Mingwei hu College of Civil and Transportation Engineering Shenzhen UniversityShenzhen518060China State Key Laboratory of Intelligent Geotechnics and Tunnelling Shenzhen UniversityShenzhen518060China Key Laboratory of Coastal Urban Resilient Infrastructures of Ministry of Education Shenzhen UniversityShenzhen518060China Underground Polis Academy Shenzhen UniversityShenzhen518060China Shenzhen Key Laboratory of Green Efficient and Intelligent Construction of Underground Metro StationShenzhen UniversityShenzhen518060China

The specialized equipment utilized in long-line tunnel engineering is evolving towards large-scale,multifunctional,and complex *** vibration caused by the high-frequency units during regular operation is supported by the foundation of the units,and the magnitude of vibration and the operating frequency fluctuate in different engineering contexts,leading to variations in the dynamic response of the *** high-frequency units yield significantly diverse outcomes under different startup conditions and times,resulting in failure to meet operational requirements,influencing the normal function of the tunnel,and causing harm to the foundation structure,personnel,and property in severe *** article formulates a finite element numerical computation model for solid elements using three-dimensional elastic body theory and integrates field measurements to substantiate and ascertain the crucial parameter configurations of the finite element *** proposing a comprehensive startup timing function for high-frequency dynamic machines under different startup conditions,simulating the frequency andmagnitude variations during the startup process,and suggesting functions for changes in frequency and magnitude,a simulated startup schedule function for high-frequency machines is created through *** into account the selection of the transient dynamic analysis step length,the dynamic response results for the lower dynamic foundation during its fundamental frequency crossing process are *** validation checks if the structural magnitude surpasses the safety threshold during the critical phase of unit startup traversing the structural resonance *** design recommendations for high-frequency units’dynamic foundations are provided,taking into account the startup process of the machine and ensuring the safe operation of the tunnel.

关键词： Tunnel equipment high-frequency units startup conditions transient dynamics dynamic response foundation design

On n-universal quadratic forms over dyadic local fields

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Science China Mathematics 2024年第7期67卷 1481-1506页

作者： Zilong He Yong hu School of Computer Science and Technology Dongguan University of TechnologyDongguan523808China Department of Mathematics Southern University of Science and TechnologyShenzhen518055China

Let n≥2 be an integer. we give necessary and sufficient conditions for an integral quadratic form over dyadic local fields to be n-universal by using invariants from Beli's theory of bases of norm ***, we provide a minimal set for testing n-universal quadratic forms over dyadic local fields, as an analogue of Bhargava and Hanke's 290-theorem(or Conway and Schneeberger's 15-theorem) on universal quadratic forms with integer coefficients.

关键词： integral quadratic forms n-universal quadratic forms dyadic fields 290-theorem

Electricity Theft Detection Method Based on Ensemble Learning and Prototype Learning

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Journal of Modern Power Systems and Clean Energy 2024年第1期12卷 213-224页

作者： Xinwu Sun Jiaxiang hu Zhenyuan Zhang Di Cao Qi huang Zhe Chen weihao hu the School of Mechanical and Electrical Engineering University of Electronic Science and Technology of ChinaChengduChina Southwest University of Science and TechnologyChengduChina

with the development of advanced metering infrastructure(AMI),large amounts of electricity consumption data can be collected for electricity theft ***,the imbalance of electricity consumption data is violent,which makes the training of detection model *** this case,this paper proposes an electricity theft detection method based on ensemble learning and prototype learning,which has great performance on imbalanced dataset and abnormal data with different abnormal *** this paper,convolutional neural network(CNN)and long short-term memory(LSTM)are employed to obtain abstract feature from electricity consumption *** calculating the means of the abstract feature,the prototype per class is obtained,which is used to predict the labels of unknown *** the meanwhile,through training the network by different balanced subsets of training set,the prototype is *** with some mainstream methods including CNN,random forest(RF)and so on,the proposed method has been proved to effectively deal with the electricity theft detection when abnormal data only account for 2.5%and 1.25%of normal *** results show that the proposed method outperforms other state-of-the-art methods.

关键词： Electricity theft detection ensemble learning prototype learning imbalanced dataset deep learning abnormal level

Vortex excites unidirectional water waves near ancient Luoyang Bridge

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Frontiers of physics 2024年第3期19卷 163-165页

作者： Yichen Li Xinhua hu Department of Materials Science and Key Laboratory of Micro-and Nano-Photonic Structures(Ministry of Education) Fudan UniversityShanghai 200433China

Since the discovery of generalized Snell’s law in 2011[1],metasurfaces have opened up the mainstream of arbitrary wavefront manipulation in *** a gradient-index metasurface,the parallel wavenumber kx of reflected wave can be not equal to the incident one(kx=ξ+k0sinθi,where k0 andθi are the incident wavenumber and angle,andξis the phase gradient of metasurface in its supercell)[1].whenξ>k0,the reflected wave becomes a surface wave bounded on the metasurface(where|kx|>k0,kz is imaginary,and z is normal to the metasurface)[2].However,as research of metasurfaces continually evolves,some articles have pointed out that such graded metasurfaces suffer from a series of problems[3-6].In particular,multiple metallic resonators are adopted in a subwavelength supercell,resulting in impedance mismatch,moderate conversion efficiency,wave absorption,and fabrication ***,although the approach of graded metasurfaces has been demonstrated in the microwave regime,it is hard to extend to infrared and optical ranges with shorter *** solve this problem,Ra’di et al.[7]devised metagratings with periodic arrays of bianisotropic scatterers and showed that they enable wave front engineering with unitary efficiency and significantly lower fabrication demands.

关键词： graded reflected imaginary

Stable, efficient inverted perovskite solar cells enabled by the multifunctional ytterbium oxide buffer

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Science China Chemistry 2024年第8期67卷 2423-2424页

作者： Manman hu Sang Il Seok Department of Energy and Chemical Engineering Ulsan National Institute of Science and TechnologyUlsan 44919Republic of Korea

Significant advancements in single-junction inverted perovskite solar cells (PSCs) have led to power conversion efficiencies (PCEs) exceeding 25% [1]. However, their operational stability under strict conditions falls short compared with commercial solar panels, primarily due to the ion migration. This migration alters the chemical composition within the perovskite layer, increasing the heterogeneity and forming degradation sites [2]. Additionally, ion accumulation at metal interfaces corrodes electrodes, while metal diffusion into perovskite layers further compromises the stability, highlighting critical areas for the improvement in long-term device performance [3,4].

关键词： perovskite exceeding stability

Removal of pathogenic indicator microorganisms during partial nitrification:the role of free nitrous acid

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Frontiers of Environmental Science & Engineering 2024年第3期18卷 93-102页

作者： Jiaojiao Xu Xiaotian Chen Rui Tang Jingwei Feng Shoujun Yuan wei wang Zhen-hu hu Anhui Engineering Laboratory of Rural water Environment and Resource School of Civil EngineeringHefei University of TechnologyHefei 230009China Hefei 168 High School Hefei 230025China Shanghai Key Laboratory of Materials Protection and Advanced Materials in Electric Power Shanghai University of Electric PowerShanghai 200090China

Digested wastewater contains pathogenic microorganisms and high ammonia concentrations,which can pose a potential risk to public *** removal of pathogens and nitrogen is crucial for the post-treatment of digested *** nitrification-anammox is an energy-saving nitrogen removal *** nitrous acid(FNA),an intermediate product of partial nitrification,has the potential to inactivate ***,the efficiency and mechanisms of FNA-related inactivation in pathogens during partial nitrification remains *** this study,Enterococcus and Escherichia coli(***)were selected to investigate the efficiency and mechanisms of FNA-related inactivation in partial nitrification *** results revealed that 83%±13%and 59%±27%of *** and Enterococcus were removed,respectively,in partial nitrification process at FNA concentrations of 0.023−0.028 mg/*** the concentration of FNA increased from 0 to 0.5 mg/L,the inactivation efficiencies of *** and Enterococcus increased from 0 to 99.9%and 89.9%,*** exhibited a higher resistance to FNA attack compared to ***.3D-laser scanning microscopy(3D-LSM)and scanning electron microscopy(SEM)revealed that FNA exposure caused the surface collapse of *** and Enterococcus,as well as visible pore formation on the surface of *** cells.4',6-Diamidino-2-phenylindole dihydrochloride n-hydrate(DAPI)/propidium iodide(PI)and biomolecule leakage confirmed that inactivation of *** and Enterococcus occurred due to breakdown of cell walls and cell *** findings indicate that partial nitrification process can be used for the removal of residual pathogenic microorganisms.

关键词： Partial nitrification Free nitrous acid Pathogenic indicator microorganism Inactivation Cell structure

Carbonation of Dicalcium Silicate Enhanced by Ammonia Bicarbonate and Its Mechanism

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Journal of wuhan University of Technology(Materials Science) 2024年第1期39卷 69-74页

作者：周浩刘鹏 wANG Fazhou hu Chuanlin School of Chemistry Chemical Engineering and Life ScienceWuhan University of TechnologyWuhan 430070China State Key Laboratory of Silicate Materials for Architectures Wuhan University of TechnologyWuhan 430070China

The strength development law of γ-type dicalcium silicate (γ-C_(2)S) under different carbonation processes was investigated,and the carbonation mechanism of γ-C_(2)S under the action of NH_(4)HCO_(3) was clarified by using a wide range of test methods,including XRD and SEM.A method of saturated NH_(4)HCO_(3) solution as a curing agent was identified to improve the carbonation efficiency and enhance the carbonation degree of γ-C_(2)S,and then a high-strength carbonated specimen was *** analysis and SEM morphology analysis were conducted on the carbonised specimens obtained under atmospheric pressure carbonisation conditions using the curing *** was found that γ-C_(2)S could perform carbonisation well under atmospheric pressure,which promoted the carbonisation efficiency and decreased the carbonisation cost ***,a new carbonisation process solution was proposed for the rapid carbonisation of γ-C_(2)S.

关键词： type dicalcium silicate carbonization process curing agent atmospheric carbonization

Changes in extreme high temperature warning indicators over China under different global warming levels

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Science China Earth Sciences 2024年第6期67卷 1895-1909页

作者： Yuxia ZHANG Ying SUN Ting hu Chinese Academy of Meteorological Sciences Beijing 100081China National Climate Center Laboratory for Climate StudiesChina Meteorological AdministrationBeijing 100081China

High temperature warning indicators play a pivotal role in meteorological departments,serving as crucial criteria for issuing warnings that guide both social production and daily *** their importance,limited studies have explored the relationship between different global warming levels and changes in high temperature warning *** this study,we analyze data from 2,419 meteorological stations over China and utilize the Coupled Model Intercomparison Project Phase 6(CMIP6)models to examine historical changes in high temperature warning indicators used by the China Meteorological *** evaluate model performance and estimate future changes in these indicators using an annual cycle bias correction *** results indicate that since 1961,the number of high temperature days(TX35d and TX40d)and length of season(TX40d and TX40l)with daily maximum temperature reaching or exceeding 35℃ and 40℃ have increased over *** intensity of high temperatures(TXx)has strengthened and the geographical extent affected by high temperatures has *** 2022,the occurrence of 40℃ high temperatures surges,with Eastern China experiencing a two-day increase in TX40d and an extended seasonal length in TX40l by over five *** CMIP6 models have underestimated the high temperature indictors associated with 35℃ during historical periods,notable difference is not observed between the models and observations for TX40d and TX40l,given their rare ***,future projections,after bias correction,indicate that the increasing trends for 35℃ and 40℃ high temperature days and length of season become more pronounced than the raw projection,suggesting a more severe increase than that anticipated *** global warming intensifies,the high temperature days and length of season are projected to increase non-linearly,while the intensity of high temperatures is expected to increase *** every 1℃ increase in global temperature,the intensity is

关键词： Extreme high temperatures Meteorological warning CMIP6 Global warming levels Future projection