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Thermoluminescence characterization of natural and synthetic irradiated Ce-monazites

Journal of Rare Earths 2024年第4期42卷 643-650页

作者： v.correcher C.Boronat J.Garcia-Guinea J.F.Benavente T.Rivera-Montalvo CIEMAT Av.Complutense 4028040MadridSpain MNCN-CSIC J.Gutierrez Abascal 228006MadridSpain Instituto Politécnico Nacional CICATA-IPNAv.Legaria 694Mexico City11500Mexico

The thermoluminescence(TL)emission of synthetic and natural Ce-monazites was characterized here to determine the potential application in the identification of microscopic defects from a qualitative point of view trying to link each TL peak to a chemical-physical process.The kinetic parameters that lead the luminescence processes were calculated by means of variable heating rate and computing glow curve deconvolution methods and allow identifying three groups of components at~90,130 and 290℃(for the mineral sample)and~90,170,220,270 and 320℃(for the synthetic CePO_(4):Nd_(0.20),La_(0.25)).The main differences appreciated in these complex TL curves are mainly due to(i)the content of impurities(natural sample contains lanthanides as well as U 0.60%and Th 5.22%)and(ii)the degree of crystallinity of the samples which is directly related to the type of impurities(synthetic monazite relies only on Nd and La).The behavior of the dose response in the range of 1-8 Gy is similar for both samples;the TL intensity increases linearly as the dose increases without changes in the position of the maxima,denoting first-order kinetic luminescence mechanism.Each peak could be mostly associated with structural defects(i.e.,phase transitions),chemical reactions(i.e.,Ce3+?Ce4+redox reaction,dehydration or dehydroxylation processes)or intrinsic defects(i.e.,Frenkel defects,ODCs or NBOHCs).

关键词： Thermoluminescence Kineticparameters Phosphate Ce-monazite Defects Rare earths

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KCl:Eu^(2+) as a solar Uv-C radiation dosimeter. Optically stimulated luminescence and thermoluminescence analyses

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Journal of Rare Earths 2009年第4期27卷 579-583页

作者： I.Aguirre de Cárcer H.L.D'Antoni M.Barboza-Flores v.correcher F.Jaque Departamento Física de Materiales Universidad Autónoma Madrid Spain NASA Ames Research Center Moffett Field California USA Centro de Investig ción en Física Universidad de Sonora México Centro Investigaciones Energía y Medioambientales (CIEMAT) Madrid Spain

The KCI：Eu2＋ system response to Uv-C was investigated by analyzing the optically stimulated luminescence （OSL） and ther- mo-luminescence （TL） signal produced by ultraviolet light exposure at room temperature. It was found that after Uv-C irra.diation, OSL was produced on a wide band of visible wavelengths with decay time that varied by several orders of magnitude depending on the Eu2＋ aggregation state. In spite of the low intensity of solar Uv-C reaching the Earth＇s surface in Madrid （40° N, 700 m a.s.1.）, it was possible to measure the Uv-C radiation dose at 6：48 solar time by using the TL response of the KCI：Eu2＋ system and differentiate it from the ambient beta radiation dose.

关键词： thermo-luminescence rare-earth-doped alkali halides solar ultraviolet dosimeter environmental radiation

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