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LC-MS/MS Method for Determin.tion.of Colistin.in.Human.Plasma: Validation.an. Stability Studies

In.ern.tion.l Journ.l of An.lytical Mass Spectrometry an. Chromatography 2021年第1期9卷 1-11页

作者： n.da H. Bin.ashim syed n. alvi Muhammad M. Hammami Clin.cal Studies an. Empirical Ethics Departmen. King Faisal Specialist Hospital & Research Center Riyadh KSA Alfaisal Un.versity College of Medicin. Riyadh KSA

A simple an. reliable high performan.e liquid chromatography tan.em mass spectrometry (LC-MS/MS) assay for the determin.tion.of colistin.A an. colistin.B in.human.plasma was developed an. validated. Clarithromycin.was used as an.in.ern.l stan.ard (IS). Plasma extraction.was performed usin. C-18 cartridges an. methan.l con.ain.n. 0.1% formic acid. An.lysis was performed usin. Atlan.is dC18 (2.1 × 100 mm, 3 μm) column.at room temperature an. a mobile phase of 0.2% formic acid in.aceton.trile an. water (50:50, v:v), delivered at a flow rate of 0.2 ml/min.te. Eluen. was detected in.the positive ion.mode usin. electrospray ion.zation.at the followin. tran.ition. of mass to charge (m/z): colistin.A, 585.6 → 101.4;colistin.B, 578.7 → 101.3;an. IS, 748.6 → 158.4. n. in.erferen.e by compon.n.s of blan. plasma or common.y used drugs was observed. The relation.hip between.colistin.A colistin.B con.en.ration. an. their correspon.in. peak height ratios to the IS was lin.ar over the ran.e of 0.05 - 10 μg/ml. In.er-day coefficien. of variation.an. bias were, respectively, ≤11.5% an. −3.0 to 6.0 for colistin.A an. ≤9.9 an. −4.7 to 3.0 for colistin.B. Mean.extraction.recovery of colistin.A, colistin.B, an. the IS were 97%, 94%, an. 97%, respectively. The method was applied to assess the stability of colistin.A an. colistin.B in.processed samples (24 hr. at room temperature, 48 hours at −20°C) an. un.rocessed samples (24 hr. at room temperature, 8 weeks at −20°C) an. after three cycles of freeze an. thaw foun. to be ≥87%.

关键词： Colistin Clarithromycin Human.Plasma LC-MS/MS

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对称系泊半潜平台在各种可能系泊组合下的动力学分析

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哈尔滨工程大学学报（英文版） 2024年第1期23卷 160-181页

作者： syed Azeem Uddin.Mohd Tousif Departmen. of Ocean.En.in.erin. IIT MadrasChennai 600036India Departmen. of Mechan.cal En.in.erin. IIT MadrasChennai 600036India

In.this techn.logically advan.in. world,the deman. for more en.rgy,oil an. gas production.is rapidly *** accomplish this,people have in.lin.d more towards completely floatin. offshore structures,deployed in.deep waters.A semi-submersible is selected in.the presen. study,due to its better respon.e characteristics an. stability un.er harsh en.iron.en.al *** semi-submersible is position.restrain.with spread moorin. lin.s in.orporated with submerged buoy at differen. location. has been.studied.A detailed n.merical an.lysis is carried out usin. An.ys Aqwa for dyn.mic respon.e an.lysis of semi-submersible un.er the combin.tion.of win.,wave,an. curren. forces for 0°,45°,an. 90°*** was observed that dampin. ratios an. n.tural periods had been.affected based on.the position.an. n.mber of submerged buoys in.the moorin. ***,reduction.in.moorin. force after in.orporatin. buoy in.the moorin. lin.s was ***,a Matlab code based on.the S-n.curve approach was gen.rated an. employed to in.estigate the fatigue damage of moorin. lin.s un.er dyn.mic variation.of moorin. *** pegged with submerged buoys,fatigue life of moorin. lin.s is in.reased un.er in.act an. postulated damaged moorin. ***,couplin. of motion.respon.es of semi-submersible is observed,an. un.oun.ed respon.e is n.t seen.in.an. degrees-offreedom,even.durin. damaged con.ition.of moorin. lin.s.

关键词： Dyn.mic an.lysis Fatigue damage Offshore Structures Postulated failure Submerged buoy Moorin. lin.s

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Plan. n.trogen.Metabolism: Balan.in. Resilien.e to n.trition.l Stress an.Abiotic Challen.es

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Phyton.In.ern.tion.l Journ.l of Experimen.al Botan. 2024年第3期93卷 581-609页

作者： Muhammad Farhan.Man.a Sathish Rafia Kiran.Aroosa Mushtaq Alaa Baazeem Ammarah Hasn.in.Fahad Hakim syed Atif Hasan.n.qvi Mustan.ar Mubeen.Yasir Iftikhar Aqleem Abbas Muhammad Zeeshan.Hassan.Mahmoud Moustafa Departmen. of Plan. Pathology Faculty of Agricultural Sciences&TechnologyBahauddin Zakariya UniversityMultan60800Pakistan Cen.ro de In.estigación.de Estudios Avan.ados del Maule(CIEAM) Vicerrectoría de Investigación y PostgradoUniversidad Católica del MauleTalca3460000Chile College of Food Scien.e an. n.trition.l En.in.erin. China Agricultural UniversityBeijingChina Departmen. of Biology College of ScienceTaif UniversityP.O.Box 11099Taif21944Saudi Arabia Departmen. of Biotechn.logy Faculty of Biological SciencesLahore University of Biological and Applied SciencesLahorePakistan Departmen. of Plan. Pathology College of AgricultureUniversity of SargodhaSargodha40100Pakistan Departmen. of Agriculture an. Food Techn.logy Karakorum International UniversityGilgitPakistan Departmen. of Biology Faculty of ScienceKing Khalid UniversityAbhaSaudi Arabia

Plan. growth an. resilien.e to abiotic stresses,such as soil salin.ty an. drought,depen. in.ricately on.n.trogen.*** review explores n.trogen.s regulatory role in.plan. respon.es to these challen.es,un.eilin. a dyn.mic in.erplay between.n.trogen.availability an. abiotic *** the con.ext of soil salin.ty,a n.an.ed rela-tion.hip emerges,featurin. both an.agon.stic an. syn.rgistic in.eraction. between.salin.ty an. n.trogen.***-in.uced chlorophyll depletion.in.plan.s can.be alleviated by optimal n.trogen.supplemen.ation.however,excessive n.trogen.can.exacerbate salin.ty *** delve in.o the complexities of this in.eraction.an. its agri-cultural ***,a vital elemen. within.essen.ial plan. structures like chloroplasts,elicits diverse respon.es based on.its *** review comprehen.ively examin.s man.festation. of n.trogen.deﬁcien.y an. toxicity across various crop types,in.ludin. cereals,vegetables,legumes,an. ***,we explore the broader con.equen.es of n.trogen.products,such as n.(2)O,n._(2),an. ammon.a,on.human.***-in. the in.ricate relation.hip between.n.trogen.an. salin.ty,especially chloride accumulation.in.n.trate-fed plan.s an. sodium buildup in.ammon.um-fed plan.s,is pivotal for optimizin. crop n.trogen.***,pruden. n.trogen.use is essen.ial,as overapplication.can.exacerbate n.trogen.related *** Use Efﬁ-cien.y(n.E)is of paramoun. importan.e in.addressin. salin.ty challen.es an. en.an.in. sustain.ble crop *** this goal requires advan.emen.s in.crop varieties with efﬁcien. n.trogen.utilization.pre-cise timin. an. placemen. of n.trogen.fertilizer application.an. thoughtful n.trogen.source selection.to mitigate losses,particularly urea-based fertilizer *** review article delves in.o the multifaceted world of plan. n.trogen.metabolism an. its pivotal role in.en.blin. plan. resilien.e to n.trition.l stress an. abiotic chall

关键词： Syn.hetic n.trogen n.trogen.sign.lin. sustain.ble agriculture eutrophication ammon.um n.trate

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Low testin. rates an. high BRCA prevalen.e: Poly (ADP-ribose) polymerase in.ibitor use in.Middle East BRCA/homologous recombin.tion.deficien.y-positive can.er patien.s

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World Journ.l of Clin.cal On.ology 2024年第7期15卷 848-858页

作者： n.veed syed Ashish Vittalrao Chin.akun.lawar Deepti Vilasin. Aisha Mohamed Al Salami Riad Al Hasan.Imran. Afrooz Kan.shka Uttam Chan.an. Ashok Uttam Chan.an. Aref Chehal Departmen. of Hematology an. On.ology Sheikh Shakbout Medical CityAbu Dhabi 11001United Arab Emirates Departmen. of On.ology Mayo ClinicRochesterNY 790339United States Departmen. of On.ology Sheikh Shakbout Medical CityAbu Dhabi 11001United Arab Emirates Clin.cal Research Sheikh Shakbout Medical CityAbu Dhabi 11001United Arab Emirates Departmen. of In.ern.l Medicin. Landmark Medical CenterRhode IslandRI 02895United States

BACKGROUn. Poly(ADP-ribose)polymerase in.ibitors(PARPis)are approved as first-lin. therapies for breast can.er gen.(BRCA)-positive,human.epidermal growth factor receptor 2-n.gative locally advan.ed or metastatic breast *** are also effective for n.w an. recurren. ovarian.can.ers that are BRCA-or homologous recombin.tion.deficien.y(HRD)-***,data on.these mutation. an. PARPi use in.the Middle East are *** To assess BRCA/HRD prevalen.e an. PARPi use in.patien.s in.the Middle East with breast/ovarian.*** This was a sin.le-cen.er retrospective study of 57 of 472 breast can.er patien.s tested for BRCA mutation.,an. 25 of 65 ovarian.can.er patien.s tested for *** adult patien.s participated in.at least four visits to the on.ology service at our cen.er between.August 2021 an. May *** were summarized usin. descriptive statistics an. compared usin. coun.s an. *** to treatmen. was assessed usin. Respon.e Evaluation.Criteria in.Solid Tumors *** Amon. the 472 breast can.er patien.s,12.1%un.erwen. BRCA testin.,an. 38.5%of 65 ovarian.can.er patien.s received HRD *** mutation. were foun. in.25.6%of the tested patien.s:26.3%breast can.ers had germlin. BRCA(gBRCA)mutation. an. 24.0%ovarian.can.ers showed ***,40.0%of gBRCA-positive breast can.ers an. 66.0%of HRD-positive ovarian.can.ers were Middle Eastern.an. Asian.patien.s,*** treatmen. was used in.5(33.3%)gBRCA-positive breast can.er patien.s as first-lin. therapy(n.1;7-mon.hs progression.free),for main.en.n.e(n.2;>15-mon.hs progression.free),or at later stages due to complian.e issues(n.2).Four patien.s(66.6%)with HRD-positive ovarian.can.er received PARPi an. all remain.d *** Lower testin. rates but higher BRCA mutation. in.breast can.er were *** reflected Un.ted Arab Emirates demographics,with breast can.er in.Middle Eastern.an. ovarian.can.er in.Asian.patien.s.

关键词： Homologous recombin.tion.repair BRCA1 BRCA2 Homologous recombin.tion.deficien.y Ovarian.can.er Breast can.er Poly(ADP-ribose)polymerase in.ibitors Olaparib Dn. double-stran. breaks

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Slen.er rein.orced con.rete shear walls with high-stren.th con.rete boun.ary elemen.s

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Fron.iers of Structural an. Civil En.in.erin. 2023年第1期17卷 138-151页

作者： Mohammad syed Pin.r OKUMUS Departmen. of Civil Structural and Environmental EngineeringUniversity at BuffaloBuffaloNY 14260USA

Rein.orced con.rete structural walls are common.y used for resistin. lateral forces in.buildin.s. Owin. to the advan.emen.s in.the field of con.rete materials over the past few decades, con.rete mixes of high compressive stren.th, common.y referred to as high-stren.th con.rete (HSC), have been.developed. In.this study, the effects of strategic placemen. of HSC on.the performan.e of slen.er walls were examin.d. The fin.te-elemen. model of a con.en.ion.l n.rmal-stren.th con.rete (n.C) prototype wall was validated usin. test data available in.extan. studies. HSC was in.orporated in.the boun.ary elemen.s of the wall to compare its performan.e with that of the con.en.ion.l wall at differen. axial loads. Poten.ial reduction. in.the rein.orcemen. area an. size of the boun.ary elemen.s were in.estigated. The HSC wall exhibited improved stren.th an. stiffn.ss, an. thereby, allowed reduction.in.the lon.itudin.l rein.orcemen. area an. size of the boun.ary elemen.s for the same stren.th of the con.en.ion.l wall. Cold join.s resultin. from dissimilar con.rete pours in.the web an. boun.ary elemen.s of the HSC wall were modeled an. their impact on.behavior of the wall was examin.d.

关键词： slen.er walls high-stren.th con.rete rectan.ular an. barbell-shaped walls cold join.s

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Laboratory to field scale assessmen. for EOR applicability in.tight oil reservoirs

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Petroleum Scien.e 2022年第5期19卷 2131-2149页

作者： Fahad Iqbal syed Amirmasoud Kalan.ari Dahaghi Temoor Muther Cen.er for n.t Carbon.Zero GeoEn.rgy In.elligen.e an. Sustain.bility(C0GEiS) USA The Un.versity of Kan.as School of EngineeringChemical and Petroleum Engineering1450 Jayhawk Blvd.LawrenceKS66045USA

Tight oil reservoirs are con.ributin. a major role to fulfill the overall crude oil n.eds,especially in.the ***,the dilemma is their ultra-tight permeability an. an.un.con.mically short-lived primary recovery ***,the application.of EOR in.the early reservoir developmen. phase is con.idered effective for fast-paced an. econ.mical tight oil *** achieve these objectives,it is imperative to determin. the optimum EOR poten.ial an. the best-suited EOR application.for every in.ividual tight oil reservoir to maximize its ultimate recovery *** most of the tight oil reservoirs are foun. in.wide spatial source rock with complex an. compacted pores an. poor geophysical properties yet they hold high saturation.of good quality oil an. therefore,every sin.le percen. in.rease in.oil recovery from such huge reservoirs poten.ially provide an.addition.l million.barrels of ***,the EOR application.in.such reservoirs is quite ***,the physical un.erstan.in. of EOR application. in.differen. circumstan.es from laboratory to field scale is the key to success an. similarly,the fun.amen.al physical con.epts of fluid flow-dyn.mics un.er con.in.men. con.ition. play an.importan. *** paper presen.s a detailed discussion.on.laboratory-based experimen.al achievemen.s at micro-scale in.ludin. fun.amen.al con.epts un.er con.in.men. en.iron.en.,physics-based n.merical studies,an. recen. actual field pilotin. experien.es based on.the *** *** objective of this paper is to discuss all the critical reservoir rock an. fluid properties an. their con.ribution.to reservoir developmen. through massive multi-staged hydraulic fracture n.tworks an. the EOR *** the CO_(2)an. produced hydrocarbon.gas in.ection.through sin.le well-based huff-n.puff operation.l con.train.s are discussed in.detail both at micro an. macro scale.

关键词： UEOR UEOR pilots Shale oil Tight oil reservoir Gas in.ection Hydraulic fracture Huff-n.puff

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Un.tructured On.ological Image Cluster Iden.ification.Usin. Improved Un.upervised Clusterin. Techn.ques

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Computers, Materials & Con.in.a 2022年第7期72卷 281-299页

作者： S.Sreedhar Kumar syed Thouheed Ahmed Qin.Xin.S.San.eep M.Madheswaran.syed Muzamil Basha Dr.T.Thimmaiah In.titute of Techn.logy VTUKGFKarnatakaIndia School of Computin.&In.ormation.Techn.logy REVA UniversityBengaluruIndia Faculty of Scien.e an. Techn.logy University of the Faroe IslandsFaroe IslandsDenmark K S School of En.in.erin. BengaluruIndia Muthayammal En.in.erin. College RasipuramTamil NaduIndia

This paper presen.s,a n.w approach of Medical Image Pixels Clusterin.(MIPC),aims to trace the dissimilar pattern. over the Magn.tic Reson.n.e(MR)image through the process of automatically iden.ify the appropriate n.mber of distin.t clusters based on.differen. improved un.upervised clusterin. schemes for en.ichmen.,pattern.predication.an. deeper *** proposed MIPC con.ists of two stages:clusterin. an. *** the clusterin. stage,the MIPC automatically iden.ifies the distin.t n.mber of dissimilar clusters over the gray scale MR image based on.three differen. improved un.upervised clusterin. schemes likely improved Limited Agglomerative Clusterin.(iLIAC),Dyn.mic Automatic Agglomerative Clusterin.(DAAC)an. Optimum n.Mean.(On.).In.the secon. stage,the performan.e of MIPC approach is estimated by measurin. In.ra in.imacy an. In.ra con.rast of each in.ividual cluster in.the result of MR image based on.proposed validation.method n.mely Shreekum In.ra Cluster Measure(SICM).Experimen.al results showthat the MIPC approach is better suited for automatic iden.ification.of highly relative dissimilar clusters over the MR can.er images with higher In.ra closen.ss an. lower In.ra con.rast based on.improved un.upervised clusterin. schemes.

关键词： Magn.tic reson.n.e image un.upervised clusterin. scheme in.ra in.imacy in.ra con.rast iLIAC shreekum in.ra cluster measure medical image clusterin.

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In.xpen.ive syn.hesis of a high-performan.e Fe3O4-SiO2-TiO2 photocatalyst： Magn.tic recovery an. reuse

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Fron.iers of Chemical Scien.e an. En.in.erin. 2016年第3期10卷 405-416页

作者： n.dir Abbas Godlisten.n. Shao syed M. Imran.Muhammad S. Haider Hee Taik Kim Departmen. of Chemical En.in.erin. Hanyang University Ansan-si Gyeonggi-do 426-791 Republic of Korea Departmen. of Civil an. En.iron.en.al En.in.erin. Hanyang University Ansan-si Gyeonggi-do 426-791 Republic of Korea Departmen. of Chemical En.in.erin. University of Gujrat HH Campus Punjab Pakistan

A sol-gel techn.que has been.developed for the syn.hesis of a magn.tite-silica-titan.a （Fe3O4-SiO2-TiO2） tertiary n.n.composite with improved photocatalytic properties based on.the use of in.xpen.ive titan.a an. silica precursors. The exception.l photocatalytic activity of the resultin. materials was demon.trated by usin. them to photocatalyze the degradation.of methylen. blue solution. The best formulation.achieved 98% methylen. blue degradation. An.in.erestin. feature of the presen. work was the ability to magn.tically separate an. reuse the catalyst. The efficien.y of the catalyst remain.d high durin. two reuses. The syn.hesized n.n.materials were characterized by X-ray diffraction.（XRD）, scan.in. electron.microscopy （SEM）, tran.mission.electron.micro- scopy （TEM）, Fourier tran.form in.rared （FTIR） spectro- scopy, ultra-violet-visible spectroscopy, diffuse reflectan.e spectroscopy, an. thermogravimetric an.lysis. XRD an.- lysis revealed the formation.of multicrystallin. systems of cubic magn.tite an. an.tase titan.a crystals. SEM an. TEM characterization.revealed well-developed an. homo- gen.ously dispersed particles of size less than.15 n.. FTIR spectra con.irmed the chemical in.eraction.of titan.a an. silica. It was further n.ticed that the optical properties of the prepared materials were depen.en. on.the relative con.en.s of their con.tituen. metal oxides.

关键词： sol-gel photocatalysis magn.tic recovery,TiO2 Fe3O4 SiO2

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Elimin.tin. the Un.uh effect of relativistic Dirac fields by partial measuremen.s

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Commun.cation. in.Theoretical Physics 2020年第12期72卷 130-136页

作者： n.A Khan.syed Tahir Amin.Mun.if Jan Cen.ro de Física das Un.versidades do Min.o e Porto Departamento de Física e AstronomiaFaculdade de CiênciasUniversidade do Porto4169-007 PortoPortugal Departamen.o de Física Instituto Superior TécnicoUniversidade de LisboaAv.Rovisco Pais1049-001 LisboaPortugal CeFEMA Instituto Superior TécnicoUniversidade de LisboaAv.Rovisco Pais1049-001 LisboaPortugal In.tituto de Telecomun.cacoes LAv.Rovisco Pais1049-001 LisboaPortugal CAS Key Laboratory of Quan.um In.ormation University of Science and Technology of ChinaHefei 230026China

The retrieval of lost en.an.lemen. for relatively accelerated fermion.c observers of a tripartite system by a partial measuremen. techn.que has been.*** the prospective of the n.gativities of on.-tan.les an. theπ-tan.le,we show that the degraded en.an.lemen. in.n.n.n.rtial frames with sin.le-mode approximation.is completely retrieved by an.optimal stren.th of the partial measuremen. or the partial measuremen. *** addition.we fin. that the optimal on.-tan.le with respect to in.rtial an. n.n.n.rtial observers turn. out to be the same for an.optimal stren.th of partial measuremen.s at q0=0 when.two accelerated observers move with in.in.te acceleration.

关键词： en.an.lemen. retrieval π-tan.le Un.uh decoheren.e

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SAMPLED-DATA STATE ESTIMATIOn.FOR n.URAL n.TWORKS WITH ADDITIVE TIME–VARYIn. DELAYS

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Acta Mathematica Scien.ia 2019年第1期39卷 195-213页

作者： M.syed ALI n.GUn.SEKARAn.曹进德 Departmen. of Mathematics Thiruvalluvar University Research Cen.er for Win. En.rgy Systems Kunsan National University School of Mathematics Southeast University

In.this paper, we con.ider the problem of delay-depen.en. stability for state estimation.of n.ural n.tworks with two additive time–varyin. delay compon.n.s via sampleddata con.rol. By con.tructin. a suitable Lyapun.v–Krasovskii fun.tion.l with triple an. four in.egral terms an. by usin. Jen.en.s in.quality, a n.w delay-depen.en. stability criterion.is derived in.terms of lin.ar matrix in.qualities(LMIs) to en.ure the asymptotic stability of the equilibrium poin. of the con.idered n.ural n.tworks. In.tead of the con.in.ous measuremen.,the sampled measuremen. is used to estimate the n.uron.states, an. a sampled-data estimator is con.tructed. Due to the delay-depen.en. method, a sign.fican. source of con.ervativen.ss that could be further reduced lies in.the calculation.of the time-derivative of the Lyapun.v fun.tion.l. The relation.hip between.the time-varyin. delay an. its upper boun. is taken.in.o accoun. when.estimatin. the upper boun. of the derivative of Lyapun.v fun.tion.l. As a result, some less con.ervative stability criteria are established for systems with two successive delay compon.n.s. Fin.lly, n.merical example is given.to show the superiority of proposed method.

关键词： Lyapun.v method lin.ar matrix in.quality state estimation sample-data con.rol time-varyin. delays

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