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Influence of CaO on damping capacity and mechanical properties of Mg alloy

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中国有色金属学会会刊：英文版 2009年第B9期19卷 76-79页

作者： Dong-In JANG Jin-kyu LEE Dae-Up kim shae-k kim Advanced Material Division Korea Institute of Industrial Technology Hyudai Mobis

For developing cost effective damping Mg alloys with high damping capacity and better mechanical properties, the microstructures, the mechanical properties at room temperature and the damping capacity of Mg alloy adding CaO were investigated and compared with those of k1A alloy. CaO adding into pure Mg maintains the damping capacity and increases the ultimate tensile strength compared with those of pure Mg. Mg-CaO alloy can be regarded as cost-effective damping alloy with high damping and mechanical properties as well as with the advantages of improving oxidation and burning resistances.

关键词：阻尼能力力学性能镁合金氧化钙成本效益微观结构阻尼性能电阻合金

Effect of Ca addition on the microstructure and mechanical properties of heat-treated Mg-6.0Zn-1.2Y-0.7Zr alloy

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Journal of Magnesium and Alloys 2021年第5期9卷 1636-1648页

作者： Young Gil Jung Wonseok Yang Yong Joo kim shae.k.kim Young Ok Yoon Hyunkyu Lim Do Hyang kim Advanced Materials and Process R&D Department Korea Institute of Industrial Technology156Gaetbeol-roIncheon 21999Republic of Korea Department of Metallurgical Engineering Yonsei University50Yonsei-roSeoulSeodaemun-gu 03722Republic of Korea

In this study,the effects of Ca addition on the microstructure,thermal properties,and mechanical properties of a Mg-6.0Zn-1.2Y-0.7Zr(ZWk611)alloy at room temperature and 150℃ were *** an increase in the Ca content,the ignition resistance of the ZWk611 alloy improved and the grains became *** as-cast ZWk611 alloy consisted mainly of the dendriticα-Mg matrix and I-phase(Mg_(3)Zn_(6)Y)at the grain *** the other hand,theτ-(Ca_(2)Mg_(6)Zn_(3))and I-phases were formed in the Ca-added ZWk611 *** fraction of theτ-phase increased with an increase in the Ca *** the solid-solution treatment,these phases remained partially at the grain boundaries of the Ca-added ZWk611 alloys and an additional W-phase(Mg_(3)Zn_(3)Y)was *** phases remaining at the grain boundaries restricted the grain growth through the grain boundary pinning *** aging treatment resulted in the formation of MgZn'precipitates in theα-Mg matrix of the *** precipitates were more uniformly distributed in the Ca-added alloys than in the alloys without ***,the heat treatment-induced precipitation improved the tensile and creep properties of the T6-treated *** T6-treated ZWk611+0.7Ca alloy exhibited the best mechanical properties at room temperature and 150℃ among all the tested alloys.

关键词： Mg-Zn-Y alloys Heat-treatment Precipitate Mechanical properties Thermal analysis

Effects of Mg Enhancement and Heat Treatment on Microstructures and Tensile Properties of Al2Ca-Added ADC12 Die Casting Alloys

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Journal of Materials Science & Technology 2016年第10期32卷 1043-1048页

作者： Gil-Yong Yeom Hyun kyu Lim shae k.kim Soong-keun Hyun Young-Ok Yoon korea Institute of Industrial Technology lncheon 406-840 South Korea Department of Materials Science and Engineering Inha University lncheon 402-751 South Korea

The effects of Mg enhancement and heat treatment on the microstructures and tensile properties of Al_2Ca-added ADC12 die casting alloys were investigated. 0.3% and 0.5% Mg in the form of a master alloy including a trace amount of Al_2Ca were added to conventional ADC12（383 and AlSi10Cu2Fe） alloy with an initial Mg-content of 0.3% to increase the Mg content to 0.6% and 0.8%, respectively. To avoid heat treatmentinduced surface blisters, shortened solution treatment for 15 min at 490 ℃ and artificial aging for 6 h at 150 ℃ was undertaken. The results show that a 10% improvement in the shape factor of eutectic Si particles was achieved for Al_2Ca-added ADC12 with 0.8% Mg compared to the conventional ADC12 in the as-aged condition. Al_2Ca-added ADC12 with 0.8% Mg exhibited a yield strength of 289 MPa, a tensile strength of 407 MPa, and an elongation of 4.22%.

关键词： Al2Ca ADC12 alloy Heat treatment Die casting Inclusion

Ca对AlMg5合金均匀化过程中热压缩行为和微观结构稳定性的影响（英文）

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Transactions of Nonferrous Metals Society of China 2020年第3期30卷 571-581页

作者： Bong Huang kim Majid SEYED SALEHI Ashkan NOURI Mohammad Sadegh MOHEBI Seong Ho HA Young Ok YOON Hyun kyu LIM shae kkim BGhasem EISAABADI korea Institute of Industrial Technology 156 Gaetbeol-roYeonsu-guIncheon 21999Korea Department of Materials Science&Engineering Yonsei University262 Seongsan-roSeodaemun-guSeoul 120-749Korea Faculty of Materials Science and Engineering K.N.Toosi University of TechnologyTehranIran Department of Materials Science and Engineering Faculty of EngineeringArak UniversityArak 38138-5-3945Iran Department of Mechanical Engineering Qom University of TechnologyQomIran

研究微量Ca添加对AlMg5热变形过程中微观结构稳定性和动态回复行为的影响。研究手段包括扫描电子显微术(SEM)、差示扫描量热法(DSC)、电子背散射衍射(EBSD)分析和透射电子显微术(TEM)。利用JMatPro程序包对合金的凝固路径进行模拟。结... 详细信息

研究微量Ca添加对AlMg5热变形过程中微观结构稳定性和动态回复行为的影响。研究手段包括扫描电子显微术(SEM)、差示扫描量热法(DSC)、电子背散射衍射(EBSD)分析和透射电子显微术(TEM)。利用JMatPro程序包对合金的凝固路径进行模拟。结果表明,Ca的加入对铸态试样的显微组织和热压缩行为没有影响,但能阻止均匀化过程中晶粒的急剧长大。在热压缩过程中,无Ca合金中的粗晶粒促进合金的动态回复,减缓动态再结晶,其再结晶晶粒的主要形核机制是粒子激发形核。另一方面,热压缩含Ca合金的显微组织受到Al4Ca金属间化合物的显著影响。通过JMatPro预测,并通过DSC、SEM和TEM揭示Al4Ca相的形成。最后,在含Ca合金的晶界处发现Al4Ca析出相通过Zener钉扎效应阻碍α(Al)相的增长,提高均匀化过程中微观结构的稳定性。

关键词： AlMg5合金热压缩均匀化显微组织粒子激发形核 Zener钉扎效应

Effect of CaO addition on ignition behavior in molten AZ31 and AZ91D Magnesium alloys

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Rare Metals 2006年第Z2期25卷 155-159页

作者： LEE Jin-kyu JO Hyung-Ho kim shae k. Department of Advanced Material Engineering Sungkyunkwan University 300 Chunchun-dong Jangan-gu Suwon Gyunggi-do 440-746 KoreaAdvanced Material Center Korea Institute of Industrial Technology 7-47 Songdo-dong Yeonsu-gu Incheon 406-840 Korea dvanced Material Center Korea Institute of Industrial Technology 7-47 Songdo-dong Yeonsu-gu Incheon 406-840 Korea

Mg alloys have been widely used in automobile and electronic industries because of high specific strength, good castability, etc. However, molten Mg alloys will burn rapidly in air if not protected. To solve this problem, the molten metal should be protected from oxidation by blanketing the surface with flux or protective gases. SF6 gas is widely used for Mg alloys as a cover gas and has proved to be a successful inhibitor. However, the use of SF6 gas is limited because of its high cost and its significant impact on non-global warming potential. Therefore, SF6 gas is being replaced by alternative protection gases. Recent studies show that there has been another attempt by adding CaO into Mg alloys. The aim of this study is to evaluate the effect of CaO on the minimum amount of protective gas, which is necessary not to make ignition in the molten AZ31 and AZ91 Mg alloys.

关键词： AZ91 AZ31 CaO clean production ignition resistance

Effect of thixoextrusion parameters on mechanical properties of 7003 Aluminum wrought alloy

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Rare Metals 2006年第Z2期25卷 124-128页

作者： YOON Young-Ok JANG Dong-In JO Hyung-Ho kim Young-Jig kim shae k Department of Advanced Material Engineering Sungkyunkwan University 300 Chunchun-dong Jangan-gu Suwon Gyunggi-do 440-746 KoreaAdvanced Material Center Korea Institute of Industrial Technology 7-47 Songdo-dong Yeonsu-gu Incheon 406-840 Korea Advanced Material Center Korea Institute of Industrial Technology 7-47 Songdo-dong Yeonsu-gu Incheon 406-840 Korea Department of Advanced Material Engineering Sungkyunkwan University 300 Chunchun-dong Jangan-gu Suwon Gyunggi-do 440-746 Korea

The processing of high strength Al wrought alloys does lead either to restrictions for geometrical complexity or to high production costs due to low productivity and multiple-step processes. Thixoextrusion process to overcome these difficulties has been under investigation. In the present study, the effect of thixoextrusion parameters was investigated on mechanical properties of 7003 Al wrought alloy. The maximum extrusion pressure of the thixoextrusion process is three times lower than that of the hot extrusion process. The elongated grains which have the axisymmetry with extrusion direction are generally observed during hot extrusion process, while the microstructures of the thixoextruded are isotropic. The tensile and yield strengthes of the thixoextruded bar are lower than those of the hot extruded bar, while the elongation value of the thixoextruded bar is higher than that of the hot extruded bar.

关键词： thixoextrusion isotropy 7003 Al wrought alloy

Cr对ECO-7175铝合金热压过程中流变行为和加工图的影响

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Transactions of Nonferrous Metals Society of China 2022年第5期32卷 1442-1459页

作者： Majid SEYED-SALEHI Bong Hwan kim Seung Yoon YANG shae kwang kim Ghasem EISAABADI BOZCHALOEI Faculty of Materials Science and Engineering K.N.Toosi University of Technology***TehranIran korea Institute of Industrial Technology 7-47 Songdo-dongIncheon 406-840Korea Department of Advanced Materials Science and Engineering Sungkyunkwan UniversitySuwon 16419Korea Department of Materials Science and Engineering Faculty of EngineeringArak University***ArakIran

研究Cr元素对新开发的ECO-7175合金热变形行为的影响。采用Gleeble热模拟机对含Cr和不含Cr的ECO-7175样品进行热压(温度为350~500℃、应变速率为0.001~1 s^(−1)),研究合金的本构方程、加工图和显微组织演变。对变形激活能的分析表明,含C... 详细信息

研究Cr元素对新开发的ECO-7175合金热变形行为的影响。采用Gleeble热模拟机对含Cr和不含Cr的ECO-7175样品进行热压(温度为350~500℃、应变速率为0.001~1 s^(−1)),研究合金的本构方程、加工图和显微组织演变。对变形激活能的分析表明,含Cr合金中速率控制变形机制由Al的自扩散(或Al中Mg的扩散)逐渐转变为Al中Cr的扩散,且Zener−Hollomon参数减小。对含Cr合金的加工图的分析表明,动态再结晶(DRX)区局限于高温和低应变速率下的变形,且随着应变的增加而扩大。另一方面,发现Al的自扩散(或Al中Mg的扩散)是无铬合金在所有加工条件下热变形过程中唯一的速率控制机制,其DRX区与塑性应变无关。

关键词：热变形本构方程加工图 ECO-7175铝合金

Behavior of CaO and Calcium in pure Magnesium

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Rare Metals 2006年第Z2期25卷 150-154页

作者： HA Seong-Ho LEE Jin-kyu JO Hyung-Ho JUNG Seung-Boo kim shae k. Department of Advanced Material Engineering Sungkyunkwan University 300 Chunchun-dong Jangan-gu Suwon Gyunggi-do 440-746 KoreaAdvanced Material Division Korea Institute of Industrial Technology 7-47 Songdo-dong Yeonsu-gu Incheon 406-840 Korea Advanced Material Division Korea Institute of Industrial Technology 7-47 Songdo-dong Yeonsu-gu Incheon 406-840 Korea Department of Advanced Material Engineering Sungkyunkwan University 300 Chunchun-dong Jangan-gu Suwon Gyunggi-do 440-746 Korea

Mg alloys exhibit a number of good properties such as low density, good castability and high specific strength. However, molten Mg and Mg alloys are ignited without the melt protective gases during melting and casting process due to their high reactivity. The purpose of this study is to investigate effects of Ca and CaO on pure Mg through microstructure observation, ignition test and phase analysis. With increasing Ca and CaO contents, the ignition resistance of Ca or CaO added pure Mg is increased and the grains are refined. As results of XRD and EDS, CaO is reduced to Ca in CaO added pure Mg. Mg2Ca phase is formed even in 0.1 wt.%CaO added pure Mg by reduction mechanism, while Mg2Ca phase is formed over 1.35 wt.% Ca added pure Mg.

关键词： Mg CaO ignition resistance Mg2Ca phase