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Amination of biochar surface from watermelon peel for toxic chromium removal enhancement

Chinese Journal of Chemical Engineering 2021年第8期34卷 199-222页

作者： mohamed a.el-Nemr Ibrahim m.A.Ismail Nabil m.Abdelmonem Ahmed el Nemr safaa Ragab Department of Chemical Engineering Faculty of EngineeringCairo UniversityGizaEgypt Renewable Energy Program Zewail City of Science and TechnologyEgypt Environmental Division National Institute of Oceanography and FisheriesKayet BeyEl-AnfoushyAlexandriaEgypt

Watermelon peel residues were used to produce a new biochar by dehydration *** new biochar has undergone two methods of chemical modification and the effect of this chemical modification on its ability to adsorb Cr(VI)ions from aqueous solution has been *** biochars,melon-B,melon-BO-NH_(2) and melon-BO-TETA,were made from watermelon peel via dehydration with 50%sulfuric acid to give melon-B followed by oxidation with ozone and amination using ammonium hydroxide to give melon-BO-NH_(2) or Triethylenetetramine(TETA)to give *** prepared biochars were characterized by BET,BJH,SEm,FT-IR,TGA,DSC and EDAX *** highest removal percentage of Cr(VI)ions was 69%for melon-B,98%for melon-BO-NH_(2) and 99%for melon-BO-TETA biochars of 100 mg·L^(−1) Cr(VI)ions initial concentration and 1.0 g·L^(−1) adsorbents *** unmodified biochar(melon-B)and modified biochars(melon-BO-NH_(2) and melon-BO-TETA)had maximum adsorption capacities(Q_(m))of 72.46,123.46,and 333.33 mg·g^(−1),*** amination of biochar reduced the pore size of modified biochar,whereas the surface area was *** obtained data of isotherm models were tested using different error function *** Freundlich,Tempkin and Langmuir isotherm models were best fitted to the experimental data of melon-B,melon-BO-NH_(2) and melon-BO-TETA,*** adsorption rate was primarily controlled by pseudo-second–order rate ***,the functional groups interactions are important for adsorption mechanisms and expected to control the adsorption *** adsorption for the melon-B,melon-BO-NH_(2) and melon-BO-TETA could be explained for acid–base interaction and hydrogen bonding interaction.

关键词： Waste treatment Powder technology Citrullus lanatus Hexavalent chromium Biochar amination Adsorption

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Bedouin farms in the Saint Katherine mountainous area(South Sinai,Egypt)

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Journal of mountain Science 2019年第10期16卷 2232-2242页

作者： Kamal H.SHALTOUT Khaled H.el-HAmDI safaa a.el-m.sry Ebrahem m.EID Botany Department Faculty of ScienceTanta UniversityTanta31527Egypt Soil Department Faculty of AgricultureMansoura UniversityMansoura35516Egypt Biology Department College of ScienceKing Khalid UniversityAbha61321P.O.Box9004Saudi Arabia Botany Department Faculty of ScienceKafr El-Sheikh UniversityKafr El-Sheikh33516Egypt

This study aims to assess the natural and cultivated plant species in 26 Bedouin farms in Saint Katherine Protectorate(SKP),identify their soil and water characteristics,and assess the suitability of these farms for the cultivation of some wild medicinal *** farms were selected to represent wide wadis with deep sand and clay deposits,gorge-like wadis covered with rock fragments of different sizes,spot-like oases,and the Al Q’aa *** TWINSPAN(two-way indicator species analysis)and DCA(detrended correspondence analysis)techniques,the 26 farms were classified into 5 groups(Ⅰ-Ⅴ)based on their floristic composition of wild *** groups reflect an elevation gradient among the farms above sea level from a mean of 119 m to a mean of1,865m.A total of 73 wild species were recorded,with47 in groupⅡ(500-1,000 m)and 25 in group V(>1,700 m).The common target species were Artemisia judaica,Acacia tortilis ***,Origanum syriacum *** and Varthemia montana(34.6%-26.9%).The cultivated speciesnumbered 25,with 17 in groupⅡ(500-1,000 m) andⅡin groupⅣ(1,500-1,700 m).The common fruit trees were olive,grape,fig,apple,palm,almond,apricot and pomegranate(73.0%-42.3%).Based on the soil characteristics,13 farms belong to soil class 2that describes good soils with moderate limitations,and 12 belong to soil class 3 that describes modera.ely good soils,which can be used regularly for crops after proper treatment.

关键词： Agroforestry Saint Katherine Protectorate Wild medicinal plants elevation gradient multivariate analysis Wadi Feiran

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Spirulina platensis extract improves the production and defenses of the common bean grown in a heavy metals-contaminated saline soil

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Journal of Environmental Sciences 2023年第7期129卷 240-257页

作者： mostafa m.Rady Ahmed S.elrys Eman Selem Ahmed A.A.mohsen safaa m.A.I.Arnaout Ahmed H.el-Sappah Khaled a.el-Tarabily el-Sayed m.Desoky Botany Department Faculty of AgricultureFayoum UniversityFayoum 63514Egypt College of Tropical Crops Hainan UniversityHaikou 570228China Soil Science Department Faculty of AgricultureZagazig UniversityZagazig 44511Egypt Botany and microbiology Department Faculty of ScienceZagazig UniversityZagazig 44511Egypt Horticulture Department Faculty of AgricultureZagazig UniversityZagazig 44511Egypt Botany Department Faculty of AgricultureZagazig UniversityZagazig 44511Egypt Genetics Department Faculty of AgricultureZagazig UniversityZagazig 44511Egypt Department of Biology College of ScienceUnited Arab Emirates UniversityAl-Ain 15551United Arab Emirates Khalifa Center for Genetic Engineering and Biotechnology United Arab Emirates UniversityAl-Ain 15551United Arab Emirates Harry Butler Institute Murdoch UniversityMurdoch 6150Australia

Plants have to cope with several abiotic stresses,including salinity and heavymetals(Hms).Under these stresses,several extracts have been used as effective natural biostimulants,however,the use of Spirulina platensis(SP)extract(SPE)remains *** effects of SPE were evaluated as soil addition(SA)and/or foliar spraying(FS)on antioxidant defenses and Hms content of common bean grown in saline soil contaminated with ***(40 or 80 mg SPE/hill added as SA or 20 or 40 mg SPE/plant added as FS)or integrative(SA+FS)applications of SPE showed significant improvements in the following order:SA-80+FS-40>SA-80+FS-20>SA-40+FS-40>SA-40+FS-20>SA-80>SA-40>FS-40>FS-20>***,the integrative SA+FS with 40 mg SP/plant was the most effective treatment in increasing plant growth and production,overcoming stress effects and minimizing contamination of the edible *** significantly increased plant growth(74%–185%)and yield(107%–227%)by enhancing net photosynthetic rate(78.5%),stomatal conductance(104%),transpiration rate(124%),and contents of carotenoids(60.0%),chlorophylls(49%–51%),and NPK(271%–366%).These results were concurrent with the marked reductions in malondialdehyde(61.6%),hydrogen peroxide(42.2%),nickel(91%–94%),lead(80%–9%),and cadmium(74%–91%)contents due to the improved contents of glutathione(87.1%),ascorbate(37.0%),andα-tocopherol(77.2%),and the activities of catalase(18.1%),ascorbate peroxidase(18.3%),superoxide dismutase(192%),and glutathione reductase(52.2%)as reinforcing ***,this most effective treatment is recommended to mitigate the stress effects of salinity and Hms on common bean production while minimizing Hms in the edible part.

关键词： Antioxidant defense system Biostimulants Heavy metals microalgae extracts Saline soil Soil pollution

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A critical review of microbially induced carbonate precipitation for soil stabilization:The global experiences and future prospective

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Pedosphere 2023年第5期33卷 717-730页

作者： safaa m.EZZAT microbiology Department Central Laboratory for Environmental Quality Monitoring(CLEQM)National Water Research Center(NWRC)El-Kanater 13621/6Egypt

microbially induced carbonate precipitation(mICP)is a new technology having the potential to induce soil stabilization and provide a green and sustainable comprehensive solution to some geotechnical engineering problems in the *** present article is dedicated to present a critical review of this technology and discuss its mechanisms of action and the key factors influencing its *** global experiences and national participation from Egypt are demonstrated,in addition to attempts for real life *** review provides an insight into the practical steps taken to mitigate some of the current limitations of mICP application and the identified gaps in analogous *** was concluded that integrating mICP with existing technologies would favor both engineering needs and market *** addition,providing effective solutions to mICP limitations would highlight this technology as an eco-friendly and cost-effective option to several engineering ***,recommendations focused on encouraging global collaboration for knowledge transfer about this technology among different countries,as well as positive financial support from industrial entities to aid in the progress of scientific research and achieving large-scale applications in the near future,are provided.

关键词： biocementation calcite geotechnical engineering urease activity ureolytic bacteria

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Distribution and ecological risk assessment of some heavy metals in coastal surface sediments along the Red Sea,Egypt

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International Journal of Sediment Research 2016年第2期31卷 164-172页

作者： Ahmed el Nemr Ghada F.el-Said Azza Khaled safaa Ragab Environmental Division National Institute of Oceanography and Fisheries

The ecological risk assessment for Al,Zn,Cu,Ni,V,Pb,Cd,and Hg in surface sediment collected from the Egyptian Red Sea coast was evaluated using the Geo-accumulation Index(Igeo).Sediment Enrichment Factor（SEF） and Potential Ecological Risk Index（PERI） *** predominant heavy metal,aluminum,showed high concentrations along both of Aqaba Gulf（4378.8 ± 2554.1 μg/g） and southern part of the Red Sea（2972.8 + 1527.5 μg/g）.while it recorded the lowest concentration in Suez Gulf（829.7 ± 398.2 μg/g）.The determined heavy metal concentrations had the order of Al > Zn >-Ni > V > Pb > Cu > Cd > *** statistical analyses showed some correlations among the heavy metals *** international sediment quality guidelines were used to estimate the quality of the collected ***,the recorded average heavy metals concentrations were lower than those of the permissible contents for sediment quality *** Geo-accumulation index calculations(Igeo) proved that the investigated region could be classified as an unpolluted *** Enrichment Factor(KSEF) study showed high values in Suez Gulf *** single pollution index analysis of heavy metals in the sediments（Ci_f） indicated that Al,Zn,V,and Pb were of natural origin,while Ni,Cd and Hg were seriously affected by human ***,amongst,all the determined heavy metals,Cd and Hg gave moderate ecological risk indicators.

关键词： Heavy metals Coastal surface sediments Ecological risk assessment Suez and Aqaba Gulfs Red Sea

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Treating wastewater under zero waste principle using wetland mesocosms

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Frontiers of Environmental Science & Engineering 2021年第4期15卷 155-168页

作者： safaa m.Ezzat mohammed T.moustafa microbiology Deptartment Central Laboratory for Environmental Quality Monitoring(CLEQM)National Water Research Center(NWRC)CairoEgypt

The present investigation demonstrates the synergistic action of using a sedimentation unit together with Cyperus papyrus(L.)wetland enriched with zeolite mineral in one-year round experiment for treating *** system was designed to support a horizontal surface flow pattern and showed satisfactory removal efficiencies for both physicochemical and bacteriological contaminants within 3 days of residence *** removal efficiencies ranged between 76.3%and 98.8%for total suspended solids,turbidity,iron,biological oxygen demand,and *** bacterial indicators(total and fecal coliforms,as well as fecal streptococci)and the potential pathogens(Escherichia coli,Staphylococcus aureus,and Pseudomonas aeruginosa)showed removal efficiencies ranged between 96.9%and 99.8%.We expect the system to offer a smart management for every component according to zero waste *** treated effluent was reused to irrigate the landscape of pilot area,and the excess sludge was recycled as fertilizer and soil *** zeolite mineral did not require regeneration for almost 36 weeks of operation,and enhanced the density of shoots(14.11%)and the height of shoots(15.88%).The harvested plant biomass could be a profitable resource for potent antibacterial and antioxidant bioactive *** could certainly offset part of the operation and maintenance costs and optimize the system implementation *** the experiment was designed under local conditions,its results could provide insights to upgrade and optimize the performance of other analogous large-scale constructed wetlands.

关键词： Wastewater Dynamic roughing filter Cyperus papyrus(L.) Zeolite Zero waste

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New Ulva lactuca Algae Based Chitosan Bio-composites for Bioremediation of Cd(II)Ions

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Journal of Bioresources and Bioproducts 2021年第3期6卷 223-242页

作者： Eman m.Saad Reda F.elshaarawy safaa A.mahmoud Khalid m.el-moselhy Department of Chemistry Faculty of ScienceSuez UniversitySuezEgypt National Institute of Oceanography and Fisheries NIOFEgypt

The current article covers the production of chitosan(CS)from shells of shrimp waste and its utilization in the preparation of eco-friendly imprinting and non-imprinting composites with Ulva lactuca algae(Alg).These bio-composites na.ely(Imp-Alg-25wt%CS)and(NImp-Alg-25wt%CS)were used for removal of Cd(II)*** transform infrared(FT-IR)spectra,scanning electron microscope(SEm)equipped with electron dispersive X-ray(EDX),X-ray diffraction(XRD),and elemental analysis measurements were performed to characterize these bio-composites *** highest adsorption of these sorbents towards Cd(II)ions was determined as a function of solutions pH,contact time,Cd(II)ion concentration,beads dose,and *** equilibrium experimental data were treated using various mathematical isotherm and kinetic models to approve the maximum bio-sorption capacities of NImp-Alg-25wt%CS and Imp-Alg-25wt%CS(in mg/g).The results exhibited that Imp-Alg-25wt%CS gave higher removal capacity than NImp-Alg-25wt%CS at the same optimum ***-2nd order dynamic and Langmuir isotherm models were well described in these biosorption ***,the removal behavior of Cd(II)using both bio-composites was spontaneous at room *** reusability of the sorbents,NImp-Alg-25wt%CS and Imp-Alg-25wt%CS,showed three *** addition,comparative study was also conducted for Cd(II)removal onto some reported sorbents.

关键词： Cadmium Bio-sorbent Chitosan Algae Bio-composites

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Changing dietary n-6:n-3 ratio using different oil sources affects performance,behavior,cytokines mRNA expression and meat fatty acid profile of broiler chickens

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Animal Nutrition 2018年第1期4卷 -页

作者： Doaa Ibrahim Rania.el-Sayed safaa I.Khater Enas N.Said Shefaa A.m.el-mandrawy Department of Nutrition and Clinical Nutrition Faculty of Veterinary MedicineZagazig University Department of Biochemistry Faculty of Veterinary MedicineZagazig University Department of Veterinary Public Health Faculty of Veterinary MedicineZagazig University Department of Clinical Pathology Faculty of Veterinary MedicineZagazig University

Typical formulated broiler diets are deficient in n-3 poly-unsaturated fatty acids(PUFA) due to widening n-6:n-3 PUFA ratio which could greatly affect performance,immune system of birds and,more importantly,meat *** study was conducted to evaluate the effect of modifying dietary n-6:n-3 PUFA ratio from plant and animal oil sources on performance,behavior,cytokine m RNA expression,antioxidative status and meat fatty acid profile of broiler ***(n=420) were fed 7 diets enriched with different dietary oil sources and ratios as follows: sunflower oil in control diet(C); fish oil(FO); 1:1 ratio of sunflower oil to FO(C1 FO1); 3:1 ratio of sunflower oil to fish oil(C3 FO1); linseed oil(LO); 1:1 ratio of sunflower oil to linseed oil(C1 LO1); 3:1 ratio of sunflower oil to linseed oil(C3 LO1),resulting in dietary n-6:n-3 ratios of approxima.ely 40:1,1.5:1,4:1,8:1,1:1,2.5:1 and 5:1,*** best final body weight,feed conversion ratio as well as protein efficiency ratio of broilers were recorded in the C1 FO1 and C1 LO1 *** with the control group,the dressing percentage and breast and thigh yield were highest in the C1 FO1 and C1 LO1 *** the dietary n-6:n-3 ratio increased(P meat contents of eicosapentaenoic acid and docosahexaenoic acid increased(P m FO and LO clearly decreased(P m total cholesterol,triglycerides and very low-density lipoproteins and enhanced antioxidative *** feeding frequency was decreased(P mpared to plant oil,to broiler diets enhanced the relative m RNA expression of interferon gamma,interleukin-1 beta,interleukin-2 and

关键词： Broiler n-6:n-3 PUFA ratio Performance Antioxidant status meat Immunity

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Cancelable Speaker Identification System Based on Optical-Like Encryption Algorithms

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Computer Systems Science & Engineering 2022年第10期43卷 87-102页

作者： safaa el-Gazar Walid el-Shafai Ghada.el-Banby Hesham F.A.Hamed Gerges m.Salama mohammed Abd-elnaby Fathi E.Abd el-Samie Department of electrical Engineering Faculty of EngineeringEgyptian-Russian UniversityCairoEgypt Department of electronics and electrical Communications Engineering Faculty of Electronic EngineeringMenoufia UniversityMenouf32952Egypt Security Engineering Laboratory Department of Computer SciencePrince Sultan UniversityRiyadh11586Saudi Arabia Department of Industrial electronics and Control Engineering Faculty of Electronic EngineeringMenoufia UniversityMenouf32952Egypt Department of Computer Engineering College of Computers and Information TechnologyTaif UniversityTaif21944Saudi Arabia Department of Information Technology College of Computer and Information SciencesPrincess Nourah Bint Abdulrahman UniversityRiyadh84428Saudi Arabia

Biometric authentication is a rapidly growing trend that is gaining increasing attention in the last *** achieves safe access to systems using biometrics instead of the traditional *** utilization of a biometric in its original format makes it usable only ***,a cancelable biometric template should be used,so that it can be replaced when it is *** biometrics aims to enhance the security and privacy of biometric *** encryption is an efficient technique to be used in order to generate cancelable biometric *** this paper,a highly-secure encryption algorithm is proposed to ensure secure biometric data in verification *** considered biometric in this paper is the speech *** speech signal is transformed into its ***,the spectrogram is encrypted using two cascaded optical encryption *** first algorithm is the Optical Scanning Holography(OSH)for its efficiency as an encryption *** OSH encrypted spectrogram is encrypted using Double Random Phase Encoding(DRPE)by implementing two Random Phase masks(RPms).After the two cascaded optical encryption algorithms,the cancelable template is *** verification is implemented through correlation estimation between enrolled and test templates in their encrypted *** the correlation value is larger than a threshold value,the user is *** threshold value can be determined from the genuine and imposter correlation distribution curves as the midpoint between the two *** implementation of optical encryption is adopted using its software rather than the optical *** efficiency of the proposed cancelable biometric algorithm is illustrated by the simulation *** can improve the biometric data security without deteriorating the recognition *** results give close-to-zero This values for the Equal Error Rate(EER)and close-to-one values for the Area under Receiver Operator Charact

关键词： Cancelable biometrics spectrogram OSH DRPE EER AROC

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Characterization and Catalytic Activity of New metal-organic Frameworks Resulted from Self-assembly of Ph3SnCI, K[Cu（CN）2] and Nitrogen Donor Ligands

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Chinese Journal of Chemistry 2011年第7期29卷 1401-1410页

作者： Etaiw, safaa el-din H. elsherbiny, Abeer S. Badr el-din, Ahmed S. Chemistry Department Faculty of Science Tanta University Tanta Egypt

Five new metal-organic frameworks （mOFs） of the general composition [Ph3SnCu（CN）2.L], where L= pyrazine （pyz）（1）, methylpyrazine （mepyz）（2）, 4,4＇-bipyridine （bpy）（3）, trans-l,2-bis（4-pyridyl）ethene （tbpe）（4） or 1,2-bis（4-pyridyl）ethane （bpe）（5）, have been synthesized and characterized to test their potential applications as catalysts. The structures of the mOFs 1--5 mainly consist of Cu（CN）2 building blocks connected by the Ph3Sn cations and the bipodal ligand forming polymeric networks. They exhibit strong fluorescence in the solid state. Also, they are used as heterogeneous catalysts for the degradation of azo-dyes, metanil yellow （mY） by diluted solution of hydrogen peroxide as oxidant. The reaction is first order with respect to mY dye, while the factors affecting the rate constant of the degradation reaction are investigated. The activation parameters of the reaction have been estimated and a possible mechanism has been proposed.

关键词： copper tin heterogeneous catalyst metanil yellow hydrogen peroxide

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