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Journal of Rare Earths 2024年第9期42卷 1629-1645,I0001页

作者： lianjie Bi Hua Yan Peilei Zhang Haichuan Shi Zhiyuan li ruidi li School of Materials Science and Engineering Shanghai University of Engineering ScienceShanghai201620China College of Agricultural Science and Engineering Hohai UniversityNanjing211100China Department of Mechanics and Maritime Science Chalmers University of TechnologyGothenburSE41296Sweden State Key Laboratory of Powder Metallurgy Central South UniversityChangsha410083China

In this paper,the effects of rare earth oxides on the micro structure and mechanical properties of nickelbased superalloys prepared by high-energy beam processing technology were critically *** focus is on the optimal amount of rare earth oxides that can produce ideal *** attention was paid to their main strengthening mechanisms,including solid solution strengthening mainly in the form of solid solution dissolved in the nickel-based alloy and improving the microstructure of the alloy by grain refinement or fine grain strengthening produced by homogenizing the distribution phase.Y_(2)O_(3),La_(2)O_(3) and CeO_(2) rare earth oxides can also improve the fluidity of the alloy molten pool and reduce the segregation of alloying *** advantages can significantly improve the mechanical properties of the ***,this paper outlines the future research directions of rare earth oxides,aiming to expand their application potential.

关键词： Rare earths High energy beam Nickel-based superalloys Microstructure Mechanical properties

Review on laser directed energy deposited aluminum alloys

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International Journal of Extreme Manufacturing 2024年第2期6卷 84-131页

作者： Tian-Shu liu Peng Chen Feng Qiu Hong-Yu Yang Nicholas Tan Yew Jin Youxiang Chew Di Wang ruidi li Qi-Chuan Jiang Chaolin Tan Singapore Institute of Manufacturing Technology(SIMTech) Agency for ScienceTechnology and Research(A∗STAR)5 Cleantech LoopSingapore 636732Singapore State Key Laboratory of Automotive Simulation and Control Jilin UniversityChangchun 130025People’s Republic of China Key Laboratory of Automobile Materials Ministry of Education and Department of Materials Science and EngineeringJilin UniversityChangchun 130025People’s Republic of China School of Mechanical&Automotive Engineering South China University of TechnologyGuangzhou 510640People’s Republic of China State Key Laboratory of Powder Metallurgy Central South UniversityChangsha 410083People’s Republic of China

lightweight aluminum(Al)alloys have been widely used in frontier fields like aerospace and automotive industries,which attracts great interest in additive manufacturing(AM)to process high-value Al *** a mainstream AM technique,laser-directed energy deposition(LDED)shows good scalability to meet the requirements for large-format component manufacturing and ***,LDED Al alloys are highly challenging due to their inherent poor printability(*** laser absorption,high oxidation sensitivity and cracking tendency).To further promote the development of LDED high-performance Al alloys,this review offers a deep understanding of the challenges and strategies to improve printability in LDED Al *** porosity,cracking,distortion,inclusions,element evaporation and resultant inferior mechanical properties(worse than laser powder bed fusion)are the key challenges in LDED Al *** parameter optimizations,in-situ alloy design,reinforcing particle addition and field assistance are the efficient approaches to improving the printability and performance of LDED Al *** underlying correlations between processes,alloy innovation,characteristic microstructures,and achievable performances in LDED Al alloys are *** benchmark mechanical properties and primary strengthening mechanism of LDED Al alloys are *** review aims to provide a critical and in-depth evaluation of current progress in LDED Al *** opportunities and perspectives in LDED high-performance Al alloys are also outlined.

关键词： additive manufacturing laser directed energy deposition(LDED) aluminum alloys printability aluminum matrix composite auxiliary fields mechanical properties

激光定向能量沉积Al-Mg-Sc-Zr修复5083-H112铝合金的组织和性能

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材料工程 2024年第2期52卷 40-49页

作者：徐荣王文军祝弘滨李瑞迪折洁袁铁锤中南大学粉末冶金国家重点实验室长沙410083 浙江力博实业股份有限公司浙江绍兴312000 中车工业研究院有限公司北京100070

激光定向能量沉积增材修复技术具有时间短、效率高、成本低、力学性能好等优点,具有很大的发展潜力。采用Al-7.5Mg-0.3Sc-0.28Zr作为修复材料对轨道交通用5083-H112铝合金进行激光修复实验,得到了致密、无缺陷的修复试样,并对其组织和... 详细信息

激光定向能量沉积增材修复技术具有时间短、效率高、成本低、力学性能好等优点,具有很大的发展潜力。采用Al-7.5Mg-0.3Sc-0.28Zr作为修复材料对轨道交通用5083-H112铝合金进行激光修复实验,得到了致密、无缺陷的修复试样,并对其组织和性能进行研究,探讨了激光修复铝合金的可行性。结果表明,熔合线附近过渡区可划分为修复区、部分熔化区、热影响区和母材。修复区为完全等轴晶,由平均晶粒尺寸为4.95μm的细晶带和18.34μm的粗晶区组成。从修复区到部分熔化区再到热影响区的过渡区域,Al元素含量逐渐升高,Mg元素含量逐渐下降,硬度逐渐下降,修复后母材未被软化。由于激光增材制造技术的快速凝固,在熔合线附近的细晶带有较大的应力集中,由于较小的热输入在部分熔化区、热影响区的残余应力较小。修复试样的屈服强度为(152±2)MPa,为母材的89.4%;抗拉强度为(305±5)MPa,为母材抗拉强度的100%;伸长率为(15.5±0.5)%,为母材的85.2%;断裂发生在强度较弱的母材。高性能的激光修复铝合金是可实现的,具有广泛的应用前景。

关键词： 5083-H112 激光定向能量沉积激光修复铝合金过渡区显微组织拉伸性能

织构对激光定向能量沉积Ni_(50.8)Ti形状记忆合金超弹性的影响

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粉末冶金材料科学与工程 2024年第1期29卷 63-73页

作者：吴慧婷李瑞迪康景涛郑聃中南大学粉末冶金国家重点实验室长沙410083

NiTi形状记忆合金由于热弹性马氏体相变而表现出优异的超弹性和形状记忆效应,被广泛应用在医疗器械、航空航天等领域。采用激光定向能量沉积工艺制备Ni_(50.8)Ti形状记忆合金,通过室温压缩实验和循环压缩实验分析成形角度对合金超弹性... 详细信息

NiTi形状记忆合金由于热弹性马氏体相变而表现出优异的超弹性和形状记忆效应,被广泛应用在医疗器械、航空航天等领域。采用激光定向能量沉积工艺制备Ni_(50.8)Ti形状记忆合金,通过室温压缩实验和循环压缩实验分析成形角度对合金超弹性及其稳定性的影响规律,借助X射线衍射分析、电子背散射衍射等表征手段分析不同成形角度合金的微观组织和织构特征,进而深入研究微观组织和织构对Ni_(50.8)Ti形状记忆合金超弹性及其稳定性的影响。结果表明:采用激光定向能量沉积制备的Ni_(50.8)Ti形状记忆合金由B2奥氏体相组成,基体成分均匀,无开裂现象。与Y轴呈90°的合金在室温下呈现出最佳的超弹性,0°的合金超弹性最差。同时,45°的合金呈现出强〈112〉织构,90°的合金呈现出强〈110〉织构,强织构合金的超弹性比弱织构(60°)和不利取向(0°)合金的超弹性更好,织构对于Ni_(50.8)Ti形状记忆合金的微观组织和超弹性具有显著的影响。

关键词：增材制造定向能量沉积 NiTi 形状记忆合金织构

Microstructure and Mechanical Properties of TiC-Reinforced Al–Mg–Sc–Zr Composites Additively Manufactured by Laser Direct Energy Deposition

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Acta Metallurgica Sinica(English Letters) 2022年第3期35卷 411-424页

作者： Rong Xu ruidi li Tiechui Yuan Hongbin Zhu Ping li State Key Laboratory of Powder Metallurgy Central South UniversityChangsha 410083.China CRRC Industrial Academy Co. LtdBeijing 100070China

In order to refine the microstructure and improve the performance of direct energy deposited(DED)additively manufactured Al–Mg–Sc–Zr alloy,TiC-modified Al–Mg–Sc–Zr composites were prepared by DED and the effect of TiC content on the microstructure and performance was *** the absence of TiC particle,the microstructure of Al–Mg–Sc–Zr alloy prepared by DED consisted of fine grains with average size of 8.36μm,and well-dispersed nano-Al;(Sc,Zr)particles inside the grains and Mg;Si phase along the grain *** the addition of 1 wt%TiC,the microstructure of TiC/Al–Mg–Sc–Zr prepared by DED became finer apparently compared with that without TiC;while the further increase of TiC content to 3 wt%,the microstructure of TiC/Al–Mg–Sc–Zr prepared by DED became coarser with appearance of a new kind of needle-like(Ti,Zr);Si;***,the addition of TiC decreased the porosity of Al–Mg–Sc–Zr prepared by ***,after the addition of TiC,the tensile strength increased from 283.25 MPa to 344.98–361.51 MPa,and the elongation increased from 3.61%to 9.58–14.10%.The potential mechanism of the microstructure evolution and strength improvement was *** research will provide new insights into the available metal matrix composites by laser additive manufacturing(LAM).

关键词： Laser additive manufacturing Aluminum matrix composites Mechanical property Microstructure

粉末冶金Ti-Al-Mo-Cr-Fe-B体系的组织与力学性能

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中南大学学报（自然科学版） 2024年第8期55卷 2961-2969页

作者：方浩煜李健徐学军周翔幸李瑞迪袁铁锤伍秋美中南大学粉末冶金国家重点实验室湖南长沙410083 杭州屹通新材料股份有限公司浙江杭州311600 江西天奇汽车零部件有限公司江西萍乡337000

采用粉末冶金技术制备Ti-Al-Mo-Cr-Fe-B合金,通过扫描电镜(SEM)、X射线衍射(XRD)、准静态拉伸测试和显微硬度测试等方法研究Mo、Cr、Fe含量对钛合金显微组织、烧结致密化和力学性能的影响。研究结果表明,所有合金均由α相、β相和金属... 详细信息

采用粉末冶金技术制备Ti-Al-Mo-Cr-Fe-B合金,通过扫描电镜(SEM)、X射线衍射(XRD)、准静态拉伸测试和显微硬度测试等方法研究Mo、Cr、Fe含量对钛合金显微组织、烧结致密化和力学性能的影响。研究结果表明,所有合金均由α相、β相和金属间化合物组成,Mo、Cr、Fe的添加降低了钛合金体系在缓慢冷却过程中形成α相的倾向,增加了β相和金属间化合物的比例。其中,Ti-3A1-1.5Mo-4Cr-1Fe-0.1B的性能最优,其致密度、显微硬度、极限抗拉强度和伸长率分别为(99.29±0.06)%、438.40±13.69(HV)、(1124±119)MPa和(1.93±0.04)%。所有合金均以脆性断裂为主,其力学性能与残余孔隙率密切相关,孔隙率越高,合金强度和塑性越低。合金的致密化主要受到Cr、Fe原子快速扩散带来的综合影响,即快速扩散促进烧结致密化的积极效果与快速扩散导致孔隙形成的消极效果之间的交互作用。

关键词：钛合金粉末冶金混合元素显微组织力学性能

A Comparative Study on the Microstructure and Properties of ITO Targets and Thin Films Prepared from Two Different Powders

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Acta Metallurgica Sinica(English Letters) 2021年第5期34卷 675-693页

作者： Fangsheng Mei Tiechui Yuan ruidi li Jingwei Huang Powder Metallurgy Research Institute Central South UniversityChangsha410083China Science and Technology on High Strength Structural Materials Laboratory Central South UniversityChangsha410083China

With the rapid development of indium tin oxide(ITO)in the electronic display industry,choosing which raw powders to prepare high-quality ITO targets has always been a controversial *** the work,in order to clearly understand the effect of the raw powders on the microstructure and properties of ITO targets and thin films,tin-doped indium oxide(dITO)and In_(2)O_3-SnO_(2)mixed(mITO)powders were chosen to prepare ITO targets for depositing the films and a comparative study on their microstructure and properties was *** is found that,(1)dITO targets possess a higher solid solubility of tin in indium oxide and more uniform elemental distribution,while there are a higher density,a finer grain size and a higher mass ratio of In_(2)O_3 to SnO_(2)for the mITO targets;(2)dITO films with more coarser columnar grains and a rougher surface prefer to grow along the[100]direction in an Ar atmosphere;(3)the conductive property of ITO films only depends on the doping amount of tin and is independent of the raw powders and the preparation process of the target source;(4)dITO films possess the superior optical property and narrower optical band gap;(5)the etching property of mITO films is superior to that of dITO films due to the lower solid solubility of tin in indium oxide.

关键词： Tin-doped indium oxide In_(2)O_3-SnO_(2) mixed powder Solid solubility of tin in indium oxide Photoelectric property Etching property

Microstructure and mechanical properties of Al-Si-Ni coating on Cu-Cr substrate prepared by multi-permeation and friction stir processing

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Nano Materials Science 2019年第3期1卷 224-228页

作者： Yin Wang ruidi li Tiechui Yuan State Key Laboratory of Powder Metallurgy Shenzhen Institute of Central South University Central South University

The surface of copper-chromium alloy was processed by Al-Si-Ni multi-permeation and friction stir processing,and the microstructure and mechanical properties of the surface layer were tested by scanning electron microscopy(SEM),energy dispersive spectroscopy(EDS),microhardness tester and friction testing *** results show that Al,Si and Ni elements are fully permeated into the surface of copper-chromium alloy after multielement co-infiltration and friction stir *** the observation of the microstructures,we found that the reticular structure is fragmented and distributed in the stir zone *** becomes finer and grains *** micro hardness of the copper-chromium alloy increased to 129 HV,44.9%higher than that of the original *** main reasons of microhardness enhancement are solid solution strengthening,fine grains strengthening and dispersion *** friction test results show that the friction coefficient is basically stable at 0.69 and the wear mass is only 0.0017 g after 10 min of friction *** improvement of wear resistance was attributed to the increase of microhardness of the alloy surface.

关键词： Copper-chromium alloy Al-Si-Ni multi-permeation Friction stir processing Microstructure Mechanical properties

Microstructure and Mechanical Properties of Selective Laser Melted Al–2.51Mn–2.71Mg–0.55Sc–0.29Cu–0.31Zn Alloy Designed by Supersaturated Solid Solution

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Acta Metallurgica Sinica(English Letters) 2022年第3期35卷 354-368页

作者： Minbo Wang ruidi li Tiechui Yuan Haiou Yang Pengda Niu Chao Chen State Key Laboratory of Powder Metallurgy Shenzhen Research Institute of CSUCentral South UniversityChangsha 410083China State Key Laboratory of Solidification Processing Northwestern Polytechnical UniversityXi'an 710072China

Selective laser melting(SLM)of aluminium alloys for lightweight application is arousing widespread interest,but the available alloy compositions are limited due to unsatisfactory mechanical *** rapid solidifi cation of SLM provides a pathway to design a novel alloy composition with extended *** strategy is demonstrated by an additively manufactured novel Al–2.51 Mn–2.71 Mg–0.55 Sc–0.29 Cu–0.31 Zn alloy with the supersaturated solid solution in the present *** microstructure of as-build sample is characterized with multi-modal grains with the fi ne equiaxed grain(FEG,~800 nm)at molten pool boundaries,coarse equiaxed grain(CEG,~2μm)and columnar dendrites(CD,~4μm)inside the molten pool,which relates to the precipitations type and *** is observable that Al 3(Sc,Zr)precipitation particles with the size of~50 nm are dispersed in the FEG zone,while the interior of CEG shows no Al3(Sc,Zr)particle which only exists at the CEG *** of FEG,CEG or CD,the slender Al6 Mn precipitation with the length of~500 nm is distributed along the grain ***,a lot of vacancies and thickness fringes are detected in the FEG zone,which confi rms the supersaturated solid solution in laser rapid solidifi *** ultimate tensile strength and yield strength of the as-printed sample are~380 MPa and~330 MPa,respectively,with elongation~14%,which increase to~440 MPa and~410 MPa with a reduction of elongation to~9%after heat treatment.

关键词： Selective laser melting Al–2.51Mn–2.71Mg–0.55Sc–0.29Cu–0.31Zn Supersaturated solid solution Microstructure Mechanical property Precipitation

激光定向能量沉积Ti-6Al合金的组织与性能研究

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铸造技术 2024年第9期45卷 838-846页

作者：袁晓慧李瑞迪柯林达候亚平肖鹏中南大学冶金国家重点实验室湖南长沙410083 上海航天精密机械研究所上海201600 湖南省计量检测研究院湖南长沙410000 湖南云箭集团有限公司湖南长沙410100

激光定向能量沉积成形钛合金具有高效快速、材料利用率高等优势,但其较大的冷却速率及温度梯度等固有特性使得成形的钛合金容易出现各向异性,因此有必要对激光定向能量沉积钛合金不同平面及不同方向上的组织与性能进行研究。选定Ti-6Al... 详细信息

激光定向能量沉积成形钛合金具有高效快速、材料利用率高等优势,但其较大的冷却速率及温度梯度等固有特性使得成形的钛合金容易出现各向异性,因此有必要对激光定向能量沉积钛合金不同平面及不同方向上的组织与性能进行研究。选定Ti-6Al合金作为研究对象,采用光学显微镜、X射线衍射仪、扫描电镜和电子背散射衍射对激光定向能量沉积Ti-6Al合金物相、微观组织形貌和晶粒特征进行研究。结果表明,合金中只存在单一的α相,该物相为HCP结构;Ti-6Al合金不同成形高度表现出不同的微观组织特征,即沿着构建方向,底部为细小的等轴晶,中间为柱状晶,顶部为等轴晶/近等轴晶。在XOY面的平均晶粒尺寸最小,为22.2519μm;YOZ面存在最大的晶粒尺寸,为38.9408μm。在3个不同平面中,XOY面的小角度晶界体积分数最高,为19.5%;YOZ面小角度晶界体积分数最低,为12.2%。沿Z方向上,即与建造方向平行时抗拉强度最高,为669.94 MPa,相应的伸长率为13.9%;沿X方向上抗拉强度为560.55 MPa,其相应的伸长率最低,为11.4%。

关键词： Ti-6Al合金激光定向能量沉积各向异性微观组织力学性能