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Quantitation of Pesticide Residue in Water and Food in Louisiana, USA

Journal of Water Resource and Protection 2016年第12期8卷 1145-1157页

作者： olubode adeniyi Amy Hernandez Mark LeBlanc Joan King Marlene Janes School of Nutrition and Food Science AgCenter Louisiana State University Baton Rouge USA Agricultural Chemistry Department AgCenter Louisiana State University Baton Rouge USA Agricultural Chemistry Division Louisiana State Department of Agriculture and Forestry Baton Rouge USA

Pesticides can remain in the environment for decades and contaminate surface water that is used for irrigation of produce. This study examined pesticide residues in some surface waters and foods in Louisiana. Samples of 8 foods (tomato, corn, rice, blueberry, cucumber, cabbage, wheat and melon) and 35 surface waters were studied using a QuEChERS extraction method for food samples and liquid-liquid extraction method for the water samples. Gas chromatography-mass spectrometry was used to analyze water and food samples. Nine pesticides were detected in the surface water samples and 5 in the food samples. Pesticides detected in foods were below FDA tolerance limit but 0.18 ppm cypermethrin found in tomato was within 90% of the FDA limit (0.2 ppm). Four water samples had atrazine levels that were above the FDA limit for potable water. This study suggests the need to intermittently monitor pesticide contamination in our food and water.

关键词： Gas Chromatography Mass Spectrometry QuEChERS Cypermethrin Atrazine Pesticide FDA

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Alleviation of Pesticide Residue in Surface Water

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Journal of Water Resource and Protection 2017年第5期9卷 523-535页

作者： olubode adeniyi Amy Hernandez Mark LeBlanc Joan M. King Marlene Janes Agricultural Chemistry Department Ag Center Louisiana State University Baton Rouge Louisiana USA Pesticide Unit Louisiana State Department of Agriculture and Forestry Baton Rouge Louisiana USA School of Nutrition and Food Science Ag Center Louisiana State University Baton Rouge Louisiana USA

Reduction of environmental pollution incurred from pesticide use is very important. Zeolite is a natural mineral capable of removing certain chemical contaminants from water. This study was carried out to test the effect of zeolite treatment on pesticide residue alleviation in surface water. Ten surface water samples were treated with natural zeolite by filtering through. An EPA method was used to extract pesticide residue from the water samples and the surfactant used to modify the net charge on the zeolite was hexadecyltrimethylammonium chloride (HDTMA-Cl). Gas chromatography-mass spectrometry was used to analyze water samples. Alleviation was achieved in all the 10 water samples that were filtered through zeolite. The highest removal of pesticides from water with zeolite included 100% of bifenthrin in sample CLC, atrazine in BPH, CDG and LBT;metolachlor in CLC, LBT, BCH, TRH2 and BPI;acetolachlor in BBH and BCH;azoxystrobin in BBH;desethylatrazine in BCH and BPI;metribuzin in BCH, TRH2 and BPI;and both clomazone and bromacil in sample BDC. A minimum reduction of 10.9% was found for metolachlor in sample BRH. Further reduction of pesticide residues up to 50% was recorded in the SMZ treatment as the concentrations of 4 out of 8 pesticide residues were reduced. This study confirms the potential of both the natural zeolite-Clinoptilolite, and SMZ of alleviating pesticide residues in water.

关键词： EPA (United States Environmental Protection Agency) Gas Chromatography Mass Spectrometry Zeolite Hexadecyltrimethylammonium Chloride (HDTMA-Cl) Surface-Modified-Zeolite (SMZ) Bifenthrin Metolachlor Metribuzin Acetolachlor Azoxystrobin Desethylatrazine Clomazone Bromacil Atrazine Clinoptilolite Alleviation

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