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Physico-chemical parameters for the assembly of moxifloxacin hydrochloride and cetyltrimethylammonium chloride mixture in aqueous and alcoholic media

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Chinese Journal of Chemical Engineering 2023年第5期57卷 280-289页

作者： Arnop Dutta Md.Tuhinur R.Joy Sk.Md.Ali Ahsan Mansour K.Gatasheh Dileep Kumar Malik abdul Rub Md.Anamul Hoque Mohammad Majibur rahman Nasrul Hoda D.M.Shafiqul Islam Department of Chemistry Jahangirnagar UniversitySavarDhaka 1342Bangladesh Department of Chemistry Jashore University of Science and TechnologyJashore 7408Bangladesh Department of Biochemistry College of ScienceKing Saud UniversityP.O.Box 2455Riyadh 11451Saudi Arabia Laboratory for Chemical Computation and Modeling Institute for Computational Science and Artificial IntelligenceVan Lang UniversityHo Chi Minh CityViet Nam Faculty of Applied Technology Van Lang UniversityHo Chi Minh CityViet Nam Center of Excellence for Advanced Materials Research King Abdulaziz UniversityJeddah 21589Saudi Arabia Chemistry Department Faculty of ScienceKing Abdulaziz UniversityJeddah 21589Saudi Arabia Department of Environmental Sciences Jahangirnagar UniversitySavarDhaka 1342Bangladesh Department of Neurology Henry Ford Health SystemDetroitMI 48292USA

The aggregation behavior of the mixture of cetyltrimethylammonium chloride(CTAC), a cationic surfactant, and moxifloxacin hydrochloride(MFH), a fourth-generation fluoroquinolone antibiotic drug, has been studied using the conductivity technique in aqueous and alcoholic(EtOH, 1-PrOH, and 2-BuOH)media. The study was performed at several temperatures between 298.15 and 323.15 K at 5 K *** assembly has been characterized by evaluating the micellar parameters, such as the critical micelle concentration(CMC) and the counter ion binding(β), of the CTAC + MFH mixture. The values of the CMC for the assembly of the CTAC + MFH mixture were reliant on the composition of alcohols in the mixed solvents and the temperature. The CMC values of the CTAC + MFH mixture increased with increasing temperature;that is, assembly was delayed by increased temperature. The micellization of the CTAC + MFH mixed system was delayed in alcoholic media. The observed-ΔG0mvalues for the association of the CTAC + MFH mixed system demonstrated a spontaneous aggregation process under all study *** on the-ΔH^(0)_(m) and +ΔS^(0)_(m) values, the association of the CTAC + MFH mixture is exothermic and the interaction forces acting between the CTAC and MFH species are hydrophobic, ion–dipole, and electrostatic interactions. The transfer properties and enthalpy–entropy compensation were also assessed and described comprehensively.

关键词： Moxifloxacin hydrochloride drug Aggregation Alcohol Hydrophobic interaction Critical micelle concentration Thermodynamic properties

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Effect of Strain Rate on Tensile Behavior of Sn-9Zn-xAg-ySb;{(x, y) = (0.2, 0.6), (0.2, 0.8), (0.6, 0.2), (0.8, 0.2)} Lead-Free Solder Alloys

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Materials Sciences and Applications 2023年第4期14卷 273-283页

作者： Shihab Uddin Md. abdul Gafur Mohammad Obaidur rahman Department of Physics Jahangirnagar University Savar Dhaka Bangladesh Pilot Plant and Process Development Centre Dhaka Bangladesh

The tensile properties of Sn-9Zn-xAg-ySb;{(x, y) = (0.2, 0.6), (0.2, 0.8), (0.6, 0.2), (0.8, 0.2)} lead-free solders were investigated. All the test samples were annealed at 150°C for 1 hour. The tests are carried out at room temperature at the strain rate of 4.17 × 10-3 s-1, 20.85 × 10-3 s-1, and 208.5 × 10-3 s-1. It is seen that the tensile strength increases and the ductility decrease with increasing the strain rate over the investigated range. From the strain rate change test results, the strain sensitivity values are found in the range of 0.0831 to 0.1455 due to the addition of different alloying elements.

关键词： Lead-Free Solder Strain Rate Strain Sensitivity Ductility Tensile Properties

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Control of iron nanoparticle size by manipulating PEG-ethanol colloidal solutions and spin-coating parameters for the growth of single-walled carbon nanotubes

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Particuology 2013年第4期11卷 394-400页

作者： Choon-Ming Seah Siang-Piao Chai Satoshi Ichikawa abdul rahman Mohamed School of Chemical Engineering Engineering CampusUniversiti Sains Malaysia Chemical Engineering Discipline School of EngineeringMonash University Institute for NanoScience Design Osaka University

Iron catalyst nanoparticles were prepared on silicon wafers by spin-coating colloidal solutions containing iron nitrate, polyethylene glycol （PEG） and absolute ethanol. The effects of various spin-coating conditions were investigated. The findings showed that the size of the iron particles was governed by the composition of the colloidal solution used and that a high angular speed was responsible for the formation of a thin colloidal *** effect of angular acceleration on the size and distribution of the iron particles were found to be insignificant. It was observed that a longer spin-coating duration provoked the agglomeration of iron particles, leading to the formation of large particles. We also showed that single-walled carbon nanotubes could be grown from the smallest iron catalyst nanoparticles after the chemical vapor deposition of methane.

关键词： Iron nanoparticleSpin coatingColloidSingle-walled carbon nanotube

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The role of nickel oxide additive in lowering the carbon dioxide sorption temperature of CaO

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Journal of Energy Chemistry 2015年第2期24卷 225-231页

作者： Zhi Hua Lee Satoshi Ichikawa Keat Teong Lee abdul rahman Mohamed Low Carbon Economy (LCE) Research Group School of Chemical EngineeringEngineering Campus Universiti Sains Malaysia 14300 Nibong Tebal Pulau Pinang Malaysia Department of Chemical Engineering Faculty of Engineering and ScienceUniversiti Tunku Abdul Rahman Jalan Genting Kelang 53300 Setapak Kuala Lumpur Malaysia Institute for Nano Science Design Osaka University 1-3 Machikaneyama Toyonaka Osaka 560-8531 Japan

A new type of calcium-based regenerable carbon dioxide （CO_2） sorbent, CaO-NiO, was synthesized via the sol-gel method. The as synthesized CO_2 sorbent was in the form of nanoparticles. The CO_2 sorption temperature and capacity of the sorbent were examined using thermogravi- metric analysis （TGA）. The CaO-NiO sorbent is able to capture CO_2 at a lower sorption temperature （465 ℃） than pure calcium oxide （CaO）（600 ℃）. The role of NiO in the CaO-NiO sorbent in lowering the CO_2 sorption temperature was also investigated. The sorbent was char- acterized by X-ray diffractometer （XRD）, N_2 adsorption-desorption analysis, high resolution transmission electron microscopy （HRTEM） and scanning electron microscopy （SEM）. CaO and NiO were found to coexist in the sorbent. Neither solid solution nor mixed metal oxide was formed. NiO did not react with CO_2 in the sorption process; but it worked like a catalyst to promote the CaO carbonation reaction. It is suggested that this new CaO-NiO sorbent may have a promising application as an effective CO_2 sorbent with lower energy consumption.

关键词： carbon dioxide calcium oxide nickel oxide sorption temperature

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Trichomonas vaginalis infection in a low-risk women attended in Obstetrics and Gynaecology Clinic, Universiti Kebangsaan Malaysia Medical Centre

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Asian Pacific Journal of Tropical Biomedicine 2016年第8期6卷 702-705页

作者： norhayati Moktar nor Liyana Ismail Phoy Cheng Chun Mohamad Asyrab Sapie nor Farahin abdul Kahar Yusof Suboh noraina abdul Rahim nor Azlin Mohamed Ismail Tengku Shahrul Anuar Department of Parasitology and Medical Entomology Universiti Kebangsaan Malaysia Medical Centre Department of Obstetrics and Gynaecology Universiti Kebangsaan Malaysia Medical Centre Department of Medical Laboratory Technology Faculty of Health Sciences Universiti Teknologi MARAPuncak Alam Campus

Objective: To investigate the presence of trichomoniasis among women attending the Obstetrics and Gynaecology Clinic, Universiti Kebangsaan Malaysia Medical ***: A total of 139 high vaginal swabs were taken from the subjects and sent to the laboratory in Amies gel transport media. The specimens were examined for the presence of Trichomonas vaginalis using wet mount, Giemsa staining and cultured in Diamond's medium. Sociodemographic characteristics and gynaecological complaints were obtained in private using structured questionnaire applied by one ***: The median age was 32 years, with an interquartile interval of 9.96. Most of the subjects were Malays(76.9%) and the remaining were Chinese(15.1%), Indians(2.2%)and other ethnic groups(5.8%). One hundred and thirty eight(99.3%) of the women were married and 98.6% had less than 6 children. More than half(75.5%) of the women's last child birth was less than 6 years ago. Forty seven percent of them were involved in supporting administrative work and 64.7% of the women gave a history of previous or current vaginal ***: The present study reported zero incidence rate of trichomoniasis. The low incidence rate was postulated due to all women who participated in this study were categorized into a low-risk group.

关键词： Trichomoniasis Incidence rate Wet mount Giemsa staining Culture

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Interaction of cetyltrimethylammonium bromide with cefixime trihydrate drug at different temperatures and compositions: Effect of different electrolytes

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Chinese Journal of Chemical Engineering 2019年第8期27卷 1895-1903页

作者： Marzia rahman Md.Anamul Hoque Malik abdul Rub Mohammed abdullah Khan Department of Chemistry Jahangirnagar UniversitySavarDhaka 1342Bangladesh Chemistry Department Faculty of ScienceKing Abdulaziz UniversityJeddah 21589Saudi Arabia Center of Excellence for Advanced Materials Research King Abdulaziz UniversityJeddah 21589Saudi Arabia

Herein,conductivity measurements have been carried out to explore the interaction between cetyltrimethylammonium bromide(CTAB,a cationic surfactant) and antibiotic drug(cefixime trihydrate(CMT)) in water and also in occurrence of inorganic salts(NaCl,Na2 SO4 and Na3 PO4) over the temperature range of 303.15-323.15 K with an interval of 5 *** all cases,two critical micelle concentrations(c^*) were achieved for the CMT-surfactant *** of CMT drug to CTAB solution decreases the values of c^* which indicates the interaction between CMT and *** values of c^* for CMT-CTAB mixture in the presence of salts are lower in magnitude compared to the aqueous medium which indicates that micellization of the CMT-CTAB mixed system is favorable in salt *** values of △Gm^0 were obtained to be negative indicating the spontaneity of the micellization process and the extent of spontaneity further increases by means of rising *** obtained outcomes from the ΔHm^0 and ΔSm^0 values disclose that the interactions between CMT and CTAB are mostly electrostatic along with hydrophobic in *** thermodynamic parameters of transfer and enthalpy-entropy compensation phenomenon were also determined and discussed in detail.

关键词： Cefixime trihydrate CTAB Critical micelle concentration Compensation temperature Free energy of transfer

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Integration of CityGML and Oracle Spatial for implementing 3D network analysis solutionsand routing simulation within 3D-GIS environment

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Geo-Spatial Information Science 2013年第4期16卷 221-237页

作者： Umit ATILA Ismail Rakip KARAS Alias abdul-rahman Department of Computer Engineering Karabuk UniversityKarabukTurkey Department of Geoinformatics Universiti Teknologi MalaysiaJohorMalaysia

3D navigation within a 3D-GIS environment is increasingly getting more popular and spreading to various *** thelast decade,especially after the 9/11 disaster,evacuating the complex and tall buildings of today in case of emergencyhas been an important research area for *** of the current navigation systems are still in the 2D environmentand that is insufficient to visualize 3D objects and to obtain satisfactory solutions for the 3D ***,there is currently still a lack of implementation of 3D network analysis and navigation for indoor spaces in respect *** objective of this paper is to investigate and implement 3D visualization and navigation techniques andsolutions for indoor spaces within *** realizing this,we have proposed a GIS implementation that is capable ofcarrying out 3D visualization of a building model stored in the CityGML format and perform analysis on a networkmodel stored in Oracle *** proposed GUI also provides routing simulation on the calculated shortest paths withvoice commands and visual instructions.

关键词： 3D-GIS 3D network analysis indoor navigation evacuation

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Conventional processes and membrane technology for carbon dioxide removal from natural gas:A review

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Journal of Natural Gas Chemistry 2012年第3期21卷 282-298页

作者： Zee Ying Yeo Thiam Leng Chew abdul rahman Mohamed Siang-Piao Chai Chemical Engineering Discipline School of EngineeringMonash University46150 Bandar SunwaySelangorMalaysia Faculty of Engineering and Green Technology(FEGT) Perak CampusUniversiti Tunku Abdul RahmanJalan UniversitiBandar Barat31900 KamparPerakMalaysia School of Chemical Engineering Engineering CampusUniversiti Sains MalaysiaSeri Ampangan14300 Nibong TebalPenangMalaysia

Membrane technology is becoming more important for CO,_ separation from natural gas in the new era due to its process simplicity, relative ease of operation and control, compact, and easy to scale up as compared with conventional processes. Conventional processes such as absorption and adsorption for CO2 separation from natural gas are generally more energy demanding and costly for both operation and maintenance. Polymeric membranes are the current commercial membranes used for CO2 separation from natural gas. However, polymeric membranes possess drawbacks such as low permeability and selectivity, plasticization at high temperatures, as well as insufficient thermal and chemical stability. The shortcomings of commercial polymeric membranes have motivated researchers to opt for other alternatives, especially inorganic membranes due to their higher thermal stability, good chemical resistance to solvents, high mechanical strength and long lifetime. Surface modifications can be utilized in inorganic membranes to further enhance the selectivity, permeability or catalytic activities of the membrane. This paper is to provide a comprehensive review on gas separation, comparing membrane technology with other conventional methods of recovering CO2 from natural gas, challenges of current commercial polymeric membranes and inorganic membranes for CO2 removal and membrane surface modification for improved selectivity.

关键词： membrane technology inorganic membrane CO2 separation natural gas: surface modification

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CO_x-Free Hydrogen and Carbon Nanofibers Produced from Direct Decomposition of Methane on Nickel-Based Catalysts

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Journal of Natural Gas Chemistry 2006年第4期15卷 253-258页

作者： Siang-Piao Chai Sharif Hussein Sharif Zein abdul rahman Mohamed School of Chemical Engineering Universiti Sains MalaysiaEngineering Campus Seri Ampangan14300 Nibong TebalSPS Penang Malaysia

Direct decomposition of methane was carried out using a fixed-bed reactor at 700 ℃ for the production of COx-free hydrogen and carbon nanofibers. The catalytic performance of NiO-M/SiO2 catalysts （where M=AgO, CoO, CuO, FeO, MnOx and MoO） in methane decomposition was investigated. The experimental results indicate that among the tested catalysts, NiO/SiO2 promoted with CuO give the highest hydrogen yield. In addition, the examination of the most suitable catalyst support, including Al2O3, CeO2, La2O3, SiO2, and TiO2, shows that the decomposition of methane over NiO-CuO favors SiOx support. Furthermore, the optimum ratio of NiO to CuO on SiO2 support for methane decomposition was determined. The experimental results show that the optimum weight ratio of NiO to CuO fell at 8：2 （w/w） since the highest yield of hydrogen was obtained over this catalyst.

关键词： methane decomposition hydrogen carbon nanofibers supported catalyst

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Risk Assessment of Metal Contamination in Soil and Groundwater in Asia： A Review of Recent Trends as well as Existing Environmental Laws and Regulations

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Pedosphere 2016年第4期26卷 431-450页

作者： Tianlik TEH Nik abdul rahman NIK norULAINI Mohammad SHAHADAT Yoonsing WONG abdul Kadir MOHD OMAR Department of Environmental Technology School of Industrial Technology Universiti Sains Malaysia 11800 Penang School of Distance Education Universiti Sains Malaysia 11800 Penang

Asia is experiencing a more rapid economic growth compared to any other regions. The contamination of soil and groundwater with metals can mainly be attributed to human activities; therefore, risk assessments to characterize the nature and magnitude of risks to humans and ecological receptors from contaminants are important. Risk assessments are often iterative processes, which involve identification and filling data gap. Experimental samplings, geostatistical and multivariate statistical methods as well as multimedia risk assessment modeling are the three major methodologies used in the assessment of metal contamination in soil and *** review highlights a number of measurements for improving risk calculation methods and expounds scientific approaches that involve the identification of the major source of contamination, exposure pathways and bioavailability of metals. In general, risk assessments of metals in soil and groundwater worldwide are mainly focused on the levels of contamination, identification of exposure pathways, and prediction of the probability of contamination. To date, very limited studies have reported the development of relevant environmental laws and policies in the regulation of soil and groundwater contamination in Asia. The development, variations and limitations in the regulations of soil and groundwater contamination among developed countries may provide helpful guidance for the developing countries in Asia.

关键词：风险评估模型地下水污染环境法律法规金属污染土壤亚洲多元统计方法人类活动

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