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Synthesis,Crystal Structure and Spectroscopic Properties of 1,2-Benzothiazine Derivatives:An Experimental and DFT Study

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Chinese Journal of Structural Chemistry 2015年第1期34卷 15-25页

作者： MUHAMMAD Nadeem Arshad TARIQ Mahmood ATHER Faroque Khan MUHAMMAD Zia-Ur-Rehman ABDULLAH M.Asiri ISLAM Ullah Khan RIFFAT-Un-Nisa KHURSHID Ayub azam mukhtar MUHAMMAD Tariq Saeed Chemistry Department Faculty of ScienceKing Abdulaziz University Centre of Excellence for Advanced Materials Research (CEAMR) King Abdulaziz University Department of Chemistry COMSATS Institute of Information TechnologyAbbottabad IRCBM COMSATS Institute of Information Technology Applied Chemistry Research Center PCSIR Laboratories ComplexFerozpur RoadLahore 54600Pakistan Materials Chemistry Laboratory Department of ChemistryGC University Department of Chemistry College of ScienceKing Faisal University Department of Chemistry University of EducationOkara CampusOkara-Pakistan

1,2-Benzothiazine derivatives methyl 3-methoxy-4-oxo-3,4-dihydro-2H-benzo[e] [1,2]thiazine-3-carboxylate 1,1-dioxide（1） and methyl 2-ethyl-3-hydroxy-4-oxo-3,4-dihydro-2Hbenzo[e][1,2]thiazine-3-carboxylate 1,1-dioxide（2） were synthesized, and characterized by spectroscopic techniques; 1H-NMR and infrared（IR） spectroscopy. Crystals of 1 and 2 were grown by slow evaporation of methanol and ethyl acetate, respectively and their crystal structures were investigated by single-crystal X-ray diffraction analysis. Geometric properties were calculated by the B3 LYP method of density functional theory（DFT） at the 6-31G＋（d） basis set to compare with the experimental data. Simulated properties were found in strong agreement with the experimental ones. Intermolecular forces have also been modeled in order to investigate the strength of packing and strong hydrogen bonding was observed in both compounds 1 and 2. Electronic properties such as Ionization Potential（IP）, Electron Affinities（EA） and coefficients of the highest occupied molecular orbital（HOMO） and the lowest unoccupied molecular orbital（LUMO） of com- pounds 1 and 2 were simulated for the first time.

关键词： 1,2-benzothiazine B3LYP/6-31+G (d) density functional theory (DFT) HUMO-LUMO crystal structures

Dynamic transcriptional programs define distinct mammalian cortical lineages

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Neural Regeneration Research 2024年第2期19卷 387-389页

作者： Tanzila mukhtar Verdon Taylor Department of Biomedicine University of BaselBaselSwitzerland Eli and Edythe Broad Center of Regeneration Medicine and Stem Cell Research University of CaliforniaSan FranciscoCAUSA

The cerebral cortex is composed of billions of neurons and glia that are generated sequentially during *** cells are generated in an organized fashion during *** early stages of brain development,neural stem cells(NSC... 详细信息

关键词： cortex cerebral development

Lap-Shear Performance of Weld-Bonded Mg Alloy and Austenitic Stainless Steel in Three-Sheet Stack-Up

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Chinese Journal of Mechanical Engineering 2024年第4期37卷 342-353页

作者： Sunusi Marwana Manladan mukhtar Fatihu Hamza Singh Ramesh Zhen Luo School of Materials Science and Engineering Tianjin UniversityTianjin 300350China Department of Mechanical Engineering Faculty of EngineeringBayero UniversityKano 3011Nigeria Department of Mechanical Engineering College of EngineeringPrince Sattam bin Abdulaziz University11942 AlkharjSaudi Arabia Department of Mechanical Engineering Faculty of EngineeringUniversity of Malaya50603 Kuala LumpurMalaysia

With the growing interest in utilizing Mg and austenitic stainless steel(ASS)in the automotive sector,joining them together in three-sheet configuration is ***,achieving this task presents considerable challenges due to the large differences in their physical,metallurgical and mechanical *** overcome these challenges,the feasibility of using weld-bonding to join Mg alloy/ASS/ASS was *** nugget formation,interface characteristics,microstructure and mechanical properties of the joints were *** results show that the connection between the Mg alloy and upper ASS was achieved through the combined effect of the cured adhesive and weld-brazing in the weld *** the other hand,a metallurgical bond was formed at the ASS/ASS *** Mg nugget microstructure exhibited fine columar grains composed predominantly of primaryα-Mg grains along with a eutectic mixture ofα-Mg andβ-*** nugget formed at the ASS/ASS interface consisted largely of columnar grains of austenite,with some equiaxed dendritic grains formed at the centerline of the *** weld-bonded joints exhibited an average peak load and energy absorption of about 8.5 kN and 17 J,respectively(the conventional RSW joints failed with minimal or no load application).The failure mode of the joints changed with increasing welding current from interfacial failure via the Mg nugget/upper ASS interface to partial interfacial failure(part of the Mg nugget was pulled out of the Mg sheet).Both failure modes were accompanied by cohesive failure in the adhesive zone.

关键词： Weld-bonding Resistance spot welding Austenitic stainless steel Mg alloy Failure mode

AGGREGATE SPECIAL FUNCTIONS TO APPROXIMATE PERMUTING TRI-HOMOMORPHISMS AND PERMUTING TRI-DERIVATIONS ASSOCIATED WITH A TRI-ADDITIVEψ-FUNCTIONAL INEQUALITY IN BANACH ALGEBRAS

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Acta Mathematica Scientia 2024年第1期44卷 311-338页

作者： Safoura Rezaei ADERYANI azam AHADI Reza SAADATI Hari M.SRIVASTAVA School of Mathematics Iran University of Science and TechnologyNarmakTehranIran Department of Mathematics and Statistics Universtity of VictoriaVictoriaCanada Department of Medical Research China Medical University HospitalChina Medical UniversityTaichung40402China Department of Mathematics and Informatics Azerbaijan University71 Jeyhun Hajibeyli StreetAZ1007BakuAzerbaijan Section of Mathematics International TelematicUniversity UninettunoI-00186RomeItaly

In this paper,we define a new class of control functions through aggregate special *** class of control functions help us to stabilize and approximate a tri-additiveψ-functional inequality to get a better estimation for permuting tri-homomorphisms and permuting tri-derivations in unital C*-algebras and Banach algebras by the vector-valued alternative fixed point theorem.

关键词： permuting tri-homomorphism in Banach algebra permuting tri-derivation on C*-algebra fixed point theorem Ulam-Hyers-Rassias stability aggregate special functions tri-additiveψ-functional inequality

Enhanced Topic-Aware Summarization Using Statistical Graph Neural Networks

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Computers, Materials & Continua 2024年第8期80卷 3221-3242页

作者： Ayesha Khaliq Salman Afsar Awan Fahad Ahmad Muhammad azam Zia Muhammad Zafar Iqbal Department of Computer Science University of Agriculture FaisalabadFaisalabadPunjab37300Pakistan School of Computing Faculty of TechnologyUniversity of PortsmouthSouthseaPortsmouthPO12UPUK Department of Mathematics and Statistics University of Agriculture FaisalabadFaisalabadPunjab37300Pakistan

The rapid expansion of online content and big data has precipitated an urgent need for efficient summarization techniques to swiftly comprehend vast textual documents without compromising their original *** approaches in Extractive Text Summarization(ETS)leverage the modeling of inter-sentence relationships,a task of paramount importance in producing coherent *** study introduces an innovative model that integrates Graph Attention Networks(GATs)with Transformer-based Bidirectional Encoder Representa-tions from Transformers(BERT)and Latent Dirichlet Allocation(LDA),further enhanced by Term Frequency-Inverse Document Frequency(TF-IDF)values,to improve sentence selection by capturing comprehensive topical *** approach constructs a graph with nodes representing sentences,words,and topics,thereby elevating the interconnectivity and enabling a more refined understanding of text *** model is stretched to Multi-Document Summarization(MDS)from Single-Document Summarization,offering significant improvements over existing models such as THGS-GMM and Topic-GraphSum,as demonstrated by empirical evaluations on benchmark news datasets like Cable News Network(CNN)/Daily Mail(DM)and *** results consistently demonstrate superior performance,showcasing the model’s robustness in handling complex summarization tasks across single and multi-document *** research not only advances the integration of BERT and LDA within a GATs but also emphasizes our model’s capacity to effectively manage global information and adapt to diverse summarization challenges.

关键词： Summarization graph attention network bidirectional encoder representations from transformers Latent Dirichlet Allocation term frequency-inverse document frequency

Contemporary Study for Detection of COVID-19 Using Machine Learning with Explainable AI

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Computers, Materials & Continua 2024年第7期80卷 1075-1104页

作者： Saad Akbar Humera azam Sulaiman Sulmi Almutairi Omar Alqahtani Habib Shah Aliya Aleryani Department of Computer Science University of KarachiKarachi75270Pakistan Department of Computing Faculty of Engineering Science and TechnologyHamdard UniversityKarachi75540Pakistan Department of Health Informatics College of Applied Medical SciencesQassim UniversityQassim51452Saudi Arabia Department of Computer Science College of Computer ScienceKing Khalid UniversityAbha61421Saudi Arabia

The prompt spread of COVID-19 has emphasized the necessity for effective and precise diagnostic *** this article,a hybrid approach in terms of datasets as well as the methodology by utilizing a previously unexplored dataset obtained from a private hospital for detecting COVID-19,pneumonia,and normal conditions in chest X-ray images(CXIs)is proposed coupled with Explainable Artificial Intelligence(XAI).Our study leverages less preprocessing with pre-trained cutting-edge models like InceptionV3,VGG16,and VGG19 that excel in the task of feature *** methodology is further enhanced by the inclusion of the t-SNE(t-Distributed Stochastic Neighbor Embedding)technique for visualizing the extracted image features and Contrast Limited Adaptive Histogram Equalization(CLAHE)to improve images before extraction of ***,an AttentionMechanism is utilized,which helps clarify how the modelmakes decisions,which builds trust in artificial intelligence(AI)*** evaluate the effectiveness of the proposed approach,both benchmark datasets and a private dataset obtained with permissions from Jinnah PostgraduateMedical Center(JPMC)in Karachi,Pakistan,are *** 12 experiments,VGG19 showcased remarkable performance in the hybrid dataset approach,achieving 100%accuracy in COVID-19 *** classification and 97%in distinguishing normal ***,across all classes,the approach achieved 98%accuracy,demonstrating its efficiency in detecting COVID-19 and differentiating it fromother chest disorders(Pneumonia and healthy)while also providing insights into the decision-making process of the models.

关键词： COVID-19 detection deep neural networks support vector machine CXIs InceptionV3 VGG16 VGG19 t-SNE embedding CLAHE attention mechanism XAI

Dual-wavelength all-fiber Q-switched fiber laser using bismuth-doped fiber as saturable absorber

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Optoelectronics Letters 2024年第3期20卷 147-151页

作者： Aruna Ghosh Abdulkadir mukhtar Diblawe Uttam Kumar Samanta Moh Yasin Sulaiman Wadi Harun Mukul Chandra Paul Fiber Optics and Photonics Division CSIR-Central Glass and Ceramic Research InstituteKolkata 700032India Physics Department Jadavpur UniversityKolkata 700032India Photonics Engineering Laboratory Department of Electrical EngineeringUniversity of MalayaKuala Lumpur 50603Malaysia Department of Physics Faculty of Science and TechnologyAirlangga UniversitySurabayaIndonesia

A passively Q-switched all-fiber laser is demonstrated using a 10-cm-long bismuth-doped fiber(BDF) as a saturable absorber(SA). The dual-wavelength operation was obtained due to the nonlinear effect inside the fabricated BDF, which has a high germanium content. Stable Q-switched pulses were obtained at the dual synchronous wavelengths of 1 530.1 nm and 1 531.1 nm. When the pump power is tuned from 105.3 mW to 191.0 mW, the repetition rate can be varied from 82.6 kMz to 117.6 kHz. The maximum pulse energy and average output power were 83.4 nJ and 9.8 mW, respectively while the minimum pulse width was 8.5 μs at the maximum pump power of 191.0 mW. Our results indicate that BDF could be a promising alternative optical modulator for pulsed fiber laser application.

关键词： fiber switched pump

Changes in sexual activity in young women during pregnancy

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Asian pacific Journal of Reproduction 2024年第5期13卷 213-218页

作者： Ghazal Mansouri Mina Zakeri Fatemeh Karami Robati Leila Allahqoli azam Dehghani Department of Obstetrics and Gynecology School of MedicineAfzalipour HospitalKerman University of Medical SciencesKermanIran Clinical Research Development Unit Afzalipour HospitalKerman University of Medical SciencesKermanIran School of Public Health Iran University of Medical Sciences(IUMS)TehranIran Gastroenterology and Hepatology Research Center Institute of Basic and Clinical Physiology SciencesKerman University of Medical SciencesKermanIran

Objective:To conduct changes in sexual activity during pregnancy and its related factors in pregnant ***:The present descriptive cross-sectional study was conducted in 2017 on pregnant women who referred to the women's clinic of Afzalipour Hospital in the southeast of *** were included in the study through convenient *** data collection tool was a researcher-made questionnaire consisting of two parts of personal social information of the couple and questions to measure the level of sexual activity and the attitude of the subjects during pregnancy compared to before ***:201 Pregnant women were *** average age of pregnant women was(27.3±6.1)years and their average gestational age was(24.7±11.8)*** than 62%of women had decreased sexual *** was a significant relationship between the amount of changes in sexual activity and delivery time(P=0.013),abortion history(P=0.001)and premature birth history(P=0.002).Most pregnant women believed that sex during pregnancy caused damage to the fetus(67.7%).A decrease in the intensity of sexual desire was reported in 63%of pregnant *** than 60%of the subjects did not consult with doctors and midwives with regards to sexual issues(63.5%).The most common reason for not consulting was not feeling the need(32%).Most women experienced back pain during(42.8%)and after(39.8%)***:Changes in sex life during pregnancy are often caused by the lack of sexual knowledge and the increase in misconceptions among couples,which can affect the quality of *** role of education is ***,it is suggested that by including sexual counseling along with pregnancy care,wrong beliefs and information among women will be corrected.

关键词： Sexual behavior Women Pregnancy Midwifery Sex counseling Fetus

Construction of robust and durable Cu_(2)Se-V_(2)O_(5) nanosheet electrocatalyst for alkaline oxygen evolution reaction

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Frontiers of Chemical Science and Engineering 2024年第6期18卷 71-83页

作者： Tauseef Munawar Ambreen Bashir Khalid Mujasam Batoo Saman Fatima Faisal mukhtar Sajjad Hussain Sumaira Manzoor Muhammad Naeem Ashiq Shoukat Alim Khan Muammer Koc Faisal Iqbal Institute of Physics The Islamia University of BahawalpurBahawalpur 63100Pakistan King Abdullah Institute for Nanotechnology King Saud UniversityRiyadh 11451Saudi Arabia Hybrid Materials Center(HMC) Sejong UniversitySeoul 05006Republic of Korea Department of Nanotechnology and Advanced Materials Engineering Sejong UniversitySeoul 05006Republic of Korea Institute of Chemical Sciences Bahauddin Zakariya UniversityMultan 60800Pakistan Division of Sustainable Development College of Science and EngineeringHamad Bin Khalifa UniversityQatar FoundationDoha 34110Qatar

Reducing the production costs of clean energy carriers such as hydrogen through scalable water electrolysis is a potential solution for advancing the hydrogen *** the various material candidates,our group demonstrated transition-metal-based materials with tunable electronic characteristics,various phases,and ***,electrochemical water oxidation using Cu_(2)Se-V_(2)O_(5) as a non-precious metallic electrocatalyst via a hydrothermal approach is *** water-splitting performance of all the fabricated electrocatalysts was evaluated after direct growth on a stainless-steel *** electrochemically tuned Cu_(2)Se-V_(2)O_(5) catalyst exhibited a reduced overpotential of 128 mV and provided a reduced Tafel slope of 57 mV·dec^(−1) to meet the maximum current density of 250 mA·cm^(−2).The optimized strategy for interfacial coupling of the fabricated Cu_(2)Se-V_(2)O_(5) catalyst resulted in a porous structure with accessible active sites,which enabled adsorption of the intermediates and afforded an effective charge transfer rate for promoting the oxygen evolution ***,the combined effect of the catalyst components provided long-term stability for over 110 h in an alkaline solution,which makes the catalyst promising for large-scale practical *** aforementioned advantages of the composite catalyst overcome the limitations of low conductivity,agglomeration,and poor stability of the pure catalysts(Cu2Se and V2O5).

关键词： oxygen evolution reaction Cu_(2)Se-V_(2)O_(5)composite nanosheets metal-diffused ions accessible adsorption sites