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Silver modified Cu/SiO2 catalyst for the hydrogenation of methyl acetate to ethanol

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Chinese Journal of Chemical Engineering 2020年第6期28卷 1612-1622页

作者： Zhiheng Ren muhammad naeem Younis Hui Zhao Chunshan Li Xiangui Yang Erqiang Wang Gongying Wang Chengdu Institute of Organic Chemistry Chinese Academy of SciencesChengdu 610041China National Engineering Laboratory for VOCs Pollution Control Material&Technology University of Chinese Academy of SciencesBeijing 101408China CAS Key Laboratory of Green Process and Engineering State Key Laboratory of Multiphase Complex SystemsThe National Key Laboratory of Clean and Efficient Coking TechnologyBeijing Key Laboratory of Ionic Liquids Clean ProcessInstitute of Process EngineeringChinese Academy of SciencesBeijing 100190China Zhongke Langfang Institute of Process Engineering Langfang 065000China Zhongke Langfang Institute of Process Engineering Zhengzhou 450000China School of Chemical Science University of Chinese Academy of SciencesBeijing 100049China

A series of silver modified Cu/SiO2 catalysts were synthesized with ammonia-evaporation method and applied in vapor-phase hydrogenation of methyl acetate to *** influence of additive‘Ag’on the structural evolution of catalyst was systematically studied by several characterization techniques,such as N2 adsorption–desorption,N2O titration,PXRD,FTIR,in-situ FTIR,H2-TPR,H2-TPD,XPS and *** showed that incorporation of a small amount of Ag could enhance the structural stability,and the strong interaction between Cu and Ag species was conducive to increase the dispersion of copper species and create a suitable Cu+/(Cu0+Cu+)ratio,which was proposed to be responsible for the improved catalytic *** maximum conversion of MA(94.1%)and selectivity of ethanol(91.3%)over optimized Cu-0.5 Ag/SiO2 and 120 h on stream without deactivation under optimal conditions demonstrates its excellent stability.

关键词： Copper Silver Hydrogenation Methyl acetate Ethanol Kinetic

Synthesis, Crystal Structure and Antimicrobial Activity of {[Bis(pyridine-κN)bis(3,5-dinitrosalicylato κ-O,O')Zn(Ⅱ)][bis(pyridine-κN)Zn(Ⅱ)]}

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Chinese Journal of Structural Chemistry 2016年第5期35卷 705-712页

作者： CHANG Fouzia MEMON Najma AHMED muhammad naeem TAHIR muhammad Nawaz MEMON Shahabuddin CHANG Abdul Sattar BHANGER muhammad Iqbal CHANDIO Anwer National Centre of Excellence in Analytical Chemistry University of Sindh Department of Chemistry The University of Azad Jammu and Kashmir Department of Physics University of Sargodha HEJ Research Institute of Chemistry ICCBS University of Karachi

A novel {[bis（pyridine-κN）bis（3,5-dinitrosalicylato κ-O,O＇）Zn（Ⅱ）][bis（pyridine-κN）Zn（Ⅱ）]}（C_（34）H_（24）N_8O_（14）Zn_2） was synthesized by a self-assemble method at room temperature. The molecular structure was determined by single-crystal X-ray analysis. The compound crystallizes in the monoclinic system, space group P2_1/n with a = 12.2156, b = 13.5696, c = 22.5602 A, β = 90.061o, Z = 4 and V = 3739.6（3）A^3. The new 1D binuclear coordination polymer {[bis（py-κN）bis（3,5-dinitrosal κ-O,O′） Zn（Ⅱ）][bis（py-κN）Zn（Ⅱ）]} resulted from two different types of moieties. The polymer [bis（py-κN）bis（3,5-dinitrosal κ-O,O′）Zn（Ⅱ）] unit is connected with [bis（py-κN） Zn（Ⅱ）] by zigzag topology. One zinc（Ⅱ） cation has a six-fold coordination environment, in which the metal atom is connected with four oxygen atoms of two 3,5-dinitrosalicylic acids to form equatorial bonds and two nitrogen atoms of pyridine to generate the axial bonds. Other four-fold nucleus contain two Zn-O bonds from different 3,5-dinitrosalicylic acids and two bonds with the Natom of pyridine. Antimicrobial assay results indicated that the compound showed moderate activities against different bacterial and fungal strains.

关键词： crystal structure antimicrobial pyridine C-H…π interactions

Deep Learning-Enhanced Brain Tumor Prediction via Entropy-Coded BPSO in CIELAB Color Space

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Computers, Materials & Continua 2023年第11期77卷 2031-2047页

作者： Mudassir Khalil muhammad Imran Sharif Ahmed naeem muhammad Umar Chaudhry Hafiz Tayyab Rauf Adham E.Ragab Department of Computer Engineering Bahauddin Zakariya UniversityMultan60000Pakistan Department of Computer Science Kansas State UniversityManhattanKS66506USA Department of Computer Science University of Management and TechnologyLahore54000Pakistan Centre for Smart Systems AI and CybersecurityStaffordshire UniversityStoke-on-TrentST42DEUK Industrial Engineering Department Collage of EngineeringKing Saud UniversityPO Box 800Riyadh11421Saudi Arabia

Early detection of brain tumors is critical for effective treatment *** tumors in their nascent stages can significantly enhance the chances of patient *** there are various types of brain tumors,each with unique characteristics and treatment protocols,tumors are often minuscule during their initial stages,making manual diagnosis challenging,time-consuming,and potentially *** techniques predominantly used in hospitals involve manual detection via MRI scans,which can be costly,error-prone,and *** automated system for detecting brain tumors could be pivotal in identifying the disease in its earliest *** research applies several data augmentation techniques to enhance the dataset for diagnosis,including rotations of 90 and 180 degrees and inverting along vertical and horizontal *** CIELAB color space is employed for tumor image selection and ROI *** deep learning models,such as DarkNet-53 and AlexNet,are applied to extract features from the fully connected layers,following the feature selection using entropy-coded Particle Swarm Optimization(PSO).The selected features are further processed through multiple SVM kernels for *** study furthers medical imaging with its automated approach to brain tumor detection,significantly minimizing the time and cost of a manual *** method heightens the possibilities of an earlier tumor identification,creating an avenue for more successful treatment planning and better overall patient outcomes.

关键词： Brain tumor deep learning feature extraction feature selection feature fusion transfer learning

Optimizing Power Allocation for D2D Communication with URLLC under Rician Fading Channel:A Learning-to-Optimize Approach

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Intelligent Automation & Soft Computing 2023年第9期37卷 3193-3212页

作者： Owais muhammad Hong Jiang Mushtaq muhammad Umer Bilal muhammad naeem muhammad Ahtsam School of Information Engineering Southwest University of Science and TechnologyMianyang621010China School of Software Engineering Northeastern UniversityShenyang110167China School of Information and Software Engineering University of Electronic Sciences and TechnologyChengdu610000China

To meet the high-performance requirements of fifth-generation(5G)and sixth-generation(6G)wireless networks,in particular,ultra-reliable and low-latency communication(URLLC)is considered to be one of the most important communication scenarios in a wireless *** this paper,we consider the effects of the Rician fading channel on the performance of cooperative device-to-device(D2D)communication with *** better performance,we maximize and examine the system’s minimal rate of D2D *** to the interference in D2D communication,the problem of maximizing the minimum rate becomes non-convex and difficult to *** solve this problem,a learning-to-optimize-based algorithm is proposed to find the optimal power *** conventional branch and bound(BB)algorithm are used to learn the optimal pruning policy with supervised *** learning is used to train the multiple *** address the imbalanced problem,we used the supervised undersampling *** are made with the conventional BB algorithm and the heuristic *** outcome of the simulation demonstrates a notable performance improvement in power *** proposed algorithm has significantly low computational complexity and runs faster as compared to the conventional BB algorithm and a heuristic algorithm.

关键词： D2D URLLC rician fading supervised learning

Asymmetric nexus between commercial policies and consumption‑based carbon emissions:new evidence from Pakistan

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Financial Innovation 2023年第1期9卷 865-888页

作者： muhammad Zubair Chishti Hafiz Syed muhammad Azeem muhammad kamran Khan School of Business Zhengzhou UniversityZhengzhouHenanChina School of Economics Quaid I Azam UniversityIslamabadPakistan Department of Economic University of ChakwalChakwalPunjabPakistan Ministry of Finance Government of PakistanIslamabadPakistan Management studies department Bahria Business SchoolBahria UniversityIslamabadPakistan

The current study extends the previous literature by exploring the effects of a newly discovered driver,i.e.,import taxes(as a proxy for commercial policies),on the consumption-based carbon emissions(CCO2e)for *** empirical analysis,several tests and methods,including Augmented Dickey–Fuller unit root test,Zivot–Andrews unit root test,asymmetric cointegration bound testing approach,non-linear ARDL,Wald-test,Granger causality test and wavelet quantile correlation(WQC)method are ***,NARDL technique estimates reveal that contractionary commercial policy enhances the environmental quality by disrupting the detrimental effects of ***,expansionary commercial policy escalates the environmental pollution by boosting the carbon ***,the exports and the renewable energy improve the ecological quality;however,GDP deteriorates the atmospheric quality by increasing the ***,WQC method and the trivariate Granger causality test are deployed to confirm the robustness of the *** on the findings,some crucial policies are also recommended for sustainable and green development in Pakistan.

关键词： Commercial policies Consumption-based carbon emissions Asymmetric ARDL Wavelet quantile correlation(WQC) Pakistan

V-Shaped Monopole Antenna with Chichena Itzia Inspired Defected Ground Structure for UWB Applications

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Computers, Materials & Continua 2020年第10期65卷 19-32页

作者： naeem Ahmad Jan Saad Hassan Kiani Fazal muhammad Daniyal Ali Sehrai Amjad Iqbal muhammad Tufail Sunghwan Kim Department of Electrical Engineering Iqra National UniversityPeshawar25000Pakistan Department of Electrical Engineering City University of Science and Information TechnologyPeshawar25000Pakistan Department of Electrical Engineering Multimedia UniversityCyberjaya63100Malaysia Department of Mechatronics Engineering University of Engineering and TechnologyPeshawar25000Pakistan Department of Electrical Engineering University of UlsanUlsan44610Korea

Due to rapid growth in wireless communication technology,higher bandwidth requirement for advance telecommunication systems,capable of operating on two or higher bands with higher channel capacities and minimum distortion losses is *** this paper,a compact Ultra-Wideband(UWB)V-shaped monopole antenna is *** response is achieved by modifying the ground plane with Chichen Itzia inspired rectangular staircase *** proposed V-shaped is designed by incorporating a rectangle,and an inverted isosceles triangle using FR4 *** size of the antenna is 25 mm×26 mm×1.6 *** proposed V-shaped monopole antenna produces bandwidth response of 3 GHz Industrial,Scientific,and Medical(ISM),Worldwide Interoperability for Microwave Access(WiMAX),(IEEE 802.11/HIPERLAN band,5G sub 6 GHz)which with an additional square cut amplified the bandwidth response up to 8 GHz ranging from 3.1 GHz to 10.6 GHz attaining UWB defined by Federal Communications Commission(FCC)with a maximum gain of 3.83 *** antenna is designed in Ansys *** for key performance parameters of the antenna are *** measured results are in good agreement with the simulated *** to flat gain,uniform group delay,omni directional radiation pattern characteristics and well-matched impedance,the proposed antenna is suitable for WiMAX,ISM and heterogeneous wireless systems.

关键词： V-shape monopole gain staircase ultra-wideband omni-directional defected ground structure

One-pot Synthesis,Characterization and Crystal Structure Determination of Novel 1,4,5-Trisubstituted 1,2,3-Triazole with Two Conformational Isomers:1-Benzyl-5-((4-methoxyphenyl)ethynyl)-4-phenyl-1H-1,2,3-triazole

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Chinese Journal of Structural Chemistry 2016年第1期35卷 55-60页

作者： AHMED muhammad naeem YASIN Khawaja Ansar KHAN Bilal Ahmad RIAZ muhammad SADIQ-UR-REHMAN LO Kong Mun NASEER muhammad Moazzam ARSHAD Ifzan IRSHAD muhammad Department of Chemistry The University of Azad Jammu and Kashmir Department of Chemistry University of Malaya Department of Chemistry Quaid-i-Azam University Department of Chemistry University of Poonch Rawalakot Azad Kashmir

The title compound l-benzyl-5-（（4-methoxyphenyl）ethynyl）-4-phenyl-1H-1,2,3-triazole（C24H19N3O） was designed and synthesized using one-pot strategy and structural characterization was done by single-crystal X-ray diffraction,NMR,IR and *** compound was crystallized out from an ethanolic solution in triclinic system,space group P1 with a =9.9038（9）,b = 10.2928（9）,c = 18.8715（19）A°,α = 103.541（6）,β = 90.507（7）,γ = 97.157（7）°,V =1854.2（3） A°3,Z = 4,crystal size（mm） = 0.25 × 0.1 × 0.1 and R（int） = *** asymmetric unit contains two independent *** crystal structure of the title compound is stabilized by intramolecular interactions of types C-H…N and C-H…***,X-ray analysis reveals obvious C-H…π,π-π stacking interactions between two adjacent aromatic ring planes.

关键词： click chemistry trisubstituted triazole alkyne crystal structure C–H…π interactions

Influence of Y^(3+),Yb^(3+),Gd^(3+) cations on structural and electromagnetic properties of CuFe_(2)O_(4) nanoferrites prepared via one step sol-gel method

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Journal of Rare Earths 2021年第10期39卷 1224-1231,I0003页

作者： Aleena Kiran Majid Niaz Akhtar muhammad Yousaf Khalid Mujassam Batoo Omar MAldossary Salman naeem Khan Department of Physics COMSATS University IslamabadLahore CampusDefence Road Off RaiwindLahore54000Pakistan Department of Physics Mohammad Nawaz Sharif University of Engineering and TechnologyMultan60000Pakistan School of Energy and Environment Southeast UniversityNo2 Si Pai LouNanjing 210096China King Abdullah Institute for Nanotechnology King Saud UniversityP.O.Box 2455Riyadh11458Saudi Arabia Department of Physics and Astronomy College of ScienceKing Saud UniversityP.O.Box-2455Riyadh11451Saudi Arabia Micro-mm Wave Laboratory(M2L) Department of PhysicsCOMSATS University IslamabadLahore CampusDefence Road Off RaiwindLahore54000Pakistan

Rare earths(REs) play a key role in distorting spinel structure by creating some defects at the lattice sites and make them suitable for magnetodielectric *** the present study,the nanoferrites of CuRE0.02Fe1.98O4,where REs=Y^(3+),Yb^(3+),Gd^(3+),were prepared using one step sol-gel *** prepared samples are copper ferrite(CFO),yttrium doped copper ferrite(Y-CFO),ytterbium doped copper ferrite(Yb-CFO) and gadolinium doped copper ferrite(Gd-CFO),*** single-phase structure of all the REs doped nanoferrites was determined by X-ray diffraction(XRD) *** porosity,agglomerations and grain size of the REs doped copper ferrite were examined using field emission scanning electron microscopy(FESEM) *** transform infrared spectroscopy(FTIR)elaborates the phase formation and environmental effects on the REs doped nanoparticles(NPs).The recorded room temperature M-H loops from a vibrating sample magnetometer(VSM) elucidate the magnetic properties of the REs doped spinel *** magnetic saturation(Ms) was calculated in the range of 23.08 to 51.78 emu/*** calculated coercivity values(272.6 to 705.60 Oe) confirm the soft magnetic behavior of REs doped copper ***,the electromagnetic and dielectric properties were assessed using a Vector network analyzer(VNA) from 1 to 6 *** permeability,permittivity,dielectric tangent loss and electric modulus of the REs doped spinel ferrites illustrate that the prepared NPs may be suitable for microwave and high frequency applications.

关键词： Rare earth elements Nanoparticles Spinel ferrites VSM VNA Magnetodielectric applications

The Spherical q-Linear Diophantine Fuzzy Multiple-Criteria Group Decision-Making Based on Differential Measure

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Computer Modeling in Engineering & Sciences 2024年第2期138卷 1925-1950页

作者： Huzaira Razzaque Shahzaib Ashraf muhammad naeem Yu-Ming Chu Institute of Mathematics Khwaja Fareed University of Engineering&Information TechnologyRahim Yar Khan64200Pakistan Department of Mathematics Deanship of Applied SciencesUmm Al-Qura UniversityMeccaSaudi Arabia Department of Mathematics Huzhou UniversityHuzhou313000China

Spherical q-linearDiophantine fuzzy sets(Sq-LDFSs)provedmore effective for handling uncertainty and vagueness in multi-criteria decision-making(MADM).It does not only cover the data in two variable parameters but is also beneficial for three parametric *** Pythagorean fuzzy sets,the difference is calculated only between two parameters(membership and non-membership).According to human thoughts,fuzzy data can be found in three parameters(membership uncertainty,and non-membership).So,to make a compromise decision,comparing Sq-LDFSs is *** measures of different fuzzy sets do,however,can have several flaws that can lead to counterintuitive *** instance,they treat any increase or decrease in the membership degree as the same as the non-membership degree because the uncertainty does not change,even though each parameter has a different *** the Sq-LDFSs comparison,this research develops the differentialmeasure(DFM).Themain goal of the DFM is to cover the unfair arguments that come from treating different types of FSs opposing criteria *** to their relative positions in the attribute space and the similarity of their membership and non-membership degrees,two Sq-LDFSs formthis preference connectionwhen the uncertainty remains same in both *** to the degree of superiority or inferiority,two Sq-LDFSs are shown as identical,equivalent,superior,or inferior over one *** suggested DFM’s fundamental characteristics are *** on the newly developed DFM,a unique approach tomultiple criterion group decision-making is *** suggestedmethod verifies the novel way of calculating the expert weights for Sq-LDFSS as in *** proposed technique in three parameters is applied to evaluate solid-state drives and choose the optimum photovoltaic cell in two applications by taking uncertainty parameter *** method’s applicability and validity shown by the findings are contrasted with those obtained using various

关键词： Multi-criteria group decision-making spherical q-linear Diophantine fuzzy sets differencemeasures photovoltaic cells medical diagnosis