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Improved Method for the Total Synthesis of Azaperone and Investigation of Its Electrochemical Behavior in Aqueous Solution

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Chemical Research in Chinese Universities 2022年第2期38卷 546-551页

作者： mohammad javad taghizadeh Maryam Saleh mohammadNIA Masoumeh GHALKHANI Esmail SOHOULI Department of Chemistry Faculty of ScienceUniversity of Imam HosseinTehranIran Drug Applied Research Center Tabriz University of Medical SciencesTabrizIran Electrochemical Sensors Research Laboratory Department of ChemistryFaculty of ScienceShahid Rajaee Teacher Training UniversityLavizanP.O.Box ***TehranIran Young Researchers and Elites Club Science and Research BranchIslamic Azad UniversityTehranIran

Azaperone,with anti-anxiety and anti-aggressive activities used in veterinary medicine,is a member of the butyrophenone *** is ordinarily utilized for a wide range of indications,such as sedation,obstetrics,and *** this research,an improved synthetic route is presented for azaperone using a phase-transfer catalyst(PTC).In general,it was synthesized as a dopamine antagonist in four *** bis(2-chloroethyl)amine intermediate is easily obtained after the conversion of the alcohol groups into the chloride leaving group using thionyl chloride(95%yields).The alkylation of commercially available 2-amino pyridine in the presence of PTC was then carried out,giving 1-(pyridin-2-yl)piperazine with 75%yield.1-(Pyridin-2-yl)piperazine was finally alkylated using 4-chloro-1-(4-fluorophenyl)butan-1-one to achieve azaperone with 60%*** butyrophenone intermediate was obtained via the Friedel-Crafts reaction of fluorobenzene with 4-chlorobutyryl chloride in the presence of *** efficiency,gentle reaction conditions,and fast and simple procedure are the advantages of this ***,the electrochemical oxidation behaviour of azaperone was investigated using cyclic and differential pulse voltammetry *** voltammetric studies indicated an irreversible process for azaperone electro-oxidation with a peak potential of 0.78 V in a phosphate buffer solution(pH=7.0)***/AgCl(saturated KCl)*** value of the peak current *** azaperone concentration was enhanced linearly in the range of 10―70μmol/L,and the detection limit was found to be 3.33μmol/L.

关键词： Azaperone Anesthetic drug Chemical synthesis Butyrophenone class Electrochemical behavior

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An efficient chemoselective synthesis of O-vinylaryl systems using acetylenic esters and dihydroxybenzenes in the presence of triphenylphosphine or alkyl isocyanides

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Chinese Chemical Letters 2010年第2期21卷 175-178页

作者： Robabeh Baharfar mohammad javad taghizadeh Majid Ahmadian Seyed Meysam Baghbanian Department of Chemistry University of MazandaranBabolsar 47415Iran

The addition of 2,4-dihydroxyaceto(and benzo)phenone to propiolic ester is catalyzed by triphenylphosphine or tert-butyl isocyanide to form O-vinyl aryl derivatives in fairly good yields.

关键词： 2 4-Dihydroxyaceto(and benzo)phenone Triphenylphosphine Propiolic ester tert-Butyl isocyanide

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A Nonlinear Coordinated Approach to Enhance the Transient Stability of Wind Energy-Based Power Systems

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IEEE/CAA Journal of Automatica Sinica 2020年第4期7卷 1087-1097页

作者： mohammad javad Morshed the Department of Electrical and Computer Engineering University of Louisiana at LafayetteLafayetteLA 70504 USA

This paper proposes a novel framework that enables the simultaneous coordination of the controllers of doubly fed induction generators(DFIGs) and synchronous generators(SGs).The proposed coordination approach is based on the zero dynamics method aims at enhancing the transient stability of multi-machine power systems under a wide range of operating conditions. The proposed approach was implemented to the IEEE39-bus power systems. Transient stability margin measured in terms of critical clearing time along with eigenvalue analysis and time domain simulations were considered in the performance assessment. The obtained results were also compared to those achieved using a conventional power system stabilizer/power oscillation(PSS/POD) technique and the interconnection and damping assignment passivity-based controller(IDA-PBC). The performance analysis confirmed the ability of the proposed approach to enhance damping and improve system’s transient stability margin under a wide range of operating conditions.

关键词： Doubly fed induction generator(DFIG) excitation controller multi-machine power system synchronous generator(SG) transient stability zero dynamics

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Rhizobacteria facilitate physiological and biochemical drought tolerance of Halimodendron halodendron (Pall.) Voss

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Journal of Arid Land 2023年第2期15卷 205-217页

作者： mohammad Hossein taghizadeh mohammad FARZAM Jafar NABATI Department of Range and Watershed Management Ferdowsi University of MashhadMashhad ***Iran Legume Department Research Center for Plant SciencesFerdowsi University of MashhadMashhad ***Iran

Growth-promoting bacteria(GPB)have shown promising effects on serving plants against environmental constraints such as ***,simultaneous effects of different GPB have less been considered for arid land plants and under field *** investigated the effects of single and combined application of GPB,including free-living nitrogen-fixing bacteria(NFB),phosphate solubilizing bacteria(PSB),potassium solubilizing bacteria(KSB),a combination of NFB,PSB,and KSB(NPK),and control,at three drought stress *** order to better understand the interactions between drought and GPB,we measured the morphological,biochemical,and physiological plant *** target plant was salt tree(Halimodendron Halodendron(Pall.)Voss),a legume shrub native to arid lands of Central and West *** biofertilizer treatments enhanced the growth,physiology,and biochemistry of salt tree seedlings,and there were significant differences among the *** and PSB treatments increased photosynthetic pigments,but KSB treatment was more efficient in transpiration rate and stomatal regulation and increased the soluble *** treatment had the highest effect on root traits,such as taproot length,root volume,cumulative root length,and the ratio of root to *** treatment enhanced root diameter and induced biomass translocation between root ***,only the application of mixed biofertilizer(i.e.,NPK treatment)was the most significant treatment to improve all plant morphological and physiological characteristics of salt tree under drought ***,our results provided improvement of some specific plant traits simultaneous with application of three biofertilizers to increase growth and establishment of salt tree seedlings in the degraded arid lands.

关键词： growth-promoting bacteria physiological traits drought stress biofertilizer root traits Halimodendron Halodendron(Pall.)Voss

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Fuzzy TOPSIS method to primary crusher selection for Golegohar Iron Mine(Iran)

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Journal of Central South University 2014年第11期21卷 4352-4359页

作者： mohammad javad Rahimdel mohammad Karamoozian Department of Mining Engineering Sahand University of TechnologyTabriz 51335-1996 Iran Faculty of Mining Engineering Petroleum and Geophysics Shahrood University of TechnologyShahrood 361999 5161 Iran

Selection of the crusher required a great deal of design regarding to the mine planning. Selection of suitable primary crusher from all of available primary crushers is a multi-criterion decision making(MCDM) problem. The present work explores the use of technique for order performance by similarity to ideal solution(TOPSIS) with fuzzy set theory to select best primary crusher for Golegohar Iron Mine in Iran. Gyratory, double toggle jaw, single toggle jaw, high speed roll crusher, low speed sizer, impact crusher, hammer mill and feeder breaker crushers have been considered as alternatives. Also, the capacity, feed size, product size, rock compressive strength, abrasion index and application of primary crusher for mobile plants were considered as criteria for solution of this MCDM problem. To determine the order of the alternatives, closeness coefficient is defined by calculating the distances to the fuzzy positive ideal solution(FPIS) and fuzzy negative ideal solution(FNIS). Results of our work based on fuzzy TOPSIS method show that the gyratory is the best primary crusher for the studied mine.

关键词： primary crusher multi-criterion decision making(MCDM) technique for order performance by similarity to ideal solution fuzzy set theory Golegohar Iron Mine gyratory crusher

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Application of Statistical Methods to Biomarkers for Geochemical Evaluation and Genetic Type Determination of Gas Condensates in the Persian Gulf and Coastal Fars,Southern Iran

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Acta Geologica Sinica(English Edition) 2022年第4期96卷 1246-1256页

作者： mohammad javad SEIDY mohammad Hossein SABERI Petroleum Engineering Department Semnan UniversitySemnanIran The New Technology Campus Petroleum Engineering DepartmentSemnan UniversitySemnanIran

In a comprehensive geochemical study,the genetic relationships among 14 samples of gas condensates from the Persian Gulf were investigated for the purpose of evaluating the respective source rocks in terms of both age and sedimentary *** analysis was used for categorization and determination of a certitude range to determine the genetic type of the condensate families in the studied *** samples were collected from Late Permian-Triassic reservoirs(Dalan and Kangan formations)located in 6 gasfields(gas condensate)hosting some of Iran’s most important gas/gas condensate *** by gas chromatography-mass spectrometry(GC-MS),a total of 16 biomarker parameters(10 maturity-related parameters and 6 sedimentary environment-related parameters)were used to evaluate the samples in terms of thermal maturity(and hence their positions in the maturity chart),the sedimentary environment of the source rock and the *** of Hierarchical Clustering Analysis(HCA)and Principal Component Analysis(PCA)to the collected data led to the categorization of the samples into three main genetic groups,Ⅰ-Ⅲ.GroupsⅠandⅢwere found to be located in the east and the west of the Persian Gulf,respectively,while GroupⅡwas developed between the two other groups.

关键词： gas condensate satistical methods genetic linkage thermal maturation Persian Gulf Coastal Fars

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A Sliding Mode Approach to Enhance the Power Quality of Wind Turbines Under Unbalanced Voltage Conditions

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IEEE/CAA Journal of Automatica Sinica 2019年第2期6卷 566-574页

作者： mohammad javad Morshed Afef Fekih IEEE the Department of Electrical and Computer Engineering University of Louisiana at Lafayette

An integral terminal sliding mode-based control design is proposed in this paper to enhance the power quality of wind turbines under unbalanced voltage conditions. The design combines the robustness, fast response, and high quality transient characteristics of the integral terminal sliding mode control with the estimation properties of disturbance observers. The controller gains were auto-tuned using a fuzzy logic *** effectiveness of the proposed design was assessed under deep voltage sag conditions and parameter variations. Its dynamic response was also compared to that of a standard SMC *** performance analysis and simulation results confirmed the ability of the proposed approach to maintain the active power,currents, DC-link voltage and electromagnetic torque within their acceptable ranges even under the most severe unbalanced voltage conditions. It was also shown to be robust to uncertainties and parameter variations, while effectively mitigating chattering in comparison with the standard SMC.

关键词： Doubly fed induction generators(DFIG) fuzzy approach integral terminal sliding mode control(ITSMC) observer power quality voltage unbalances wind turbines

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A novel hybrid algorithm based on a harmony search and artificial bee colony for solving a portfolio optimization problem using a mean-semi variance approach

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Journal of Central South University 2016年第1期23卷 181-188页

作者： Seyed mohammad Seyedhosseini mohammad javad Esfahani Mehdi Ghaffari Department of Industrial Engineering Iran University of Science and Technology Young Researchers and Elite Club Naragh BranchIslamic Azad University Department of Industrial Engineering Naragh BranchIslamic Azad University

Portfolio selection is one of the major capital allocation and budgeting issues in financial management, and a variety of models have been presented for optimal selection. Semi-variance is usually considered as a risk factor in drawing up an efficient frontier and the optimal portfolio. Since semi-variance offers a better estimation of the actual risk portfolio, it was used as a measure to approximate the risk of investment in this work. The optimal portfolio selection is one of the non-deterministic polynomial(NP)-hard problems that have not been presented in an exact algorithm, which can solve this problem in a polynomial time. Meta-heuristic algorithms are usually used to solve such problems. A novel hybrid harmony search and artificial bee colony algorithm and its application were introduced in order to draw efficient frontier portfolios. Computational results show that this algorithm is more successful than the harmony search method and genetic algorithm. In addition, it is more accurate in finding optimal solutions at all levels of risk and return.

关键词： portfolio optimizations mean-variance model mean semi-variance model harmony search and artificial bee colony efficient frontier

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Viscosity prediction in selected Iranian light oil reservoirs:Artificial neural network versus empirical correlations

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Petroleum Science 2013年第1期10卷 126-133页

作者： mohammad Soleimani Lashkenari Majid taghizadeh Bahman Mehdizadeh Chemical Engineering Department Babol University of Technology National Iranian South Oil Company

Viscosity is a parameter that plays a pivotal role in reservoir fluid estimations. Several approaches have been presented in the literature （Beal, 1946; Khan et al, 1987; Beggs and Robinson, 1975; Kartoatmodjo and Schmidt, 1994; Vasquez and Beggs, 1980; Chew and Connally, 1959; Elsharkawy and Alikhan, 1999; Labedi, 1992） for predicting the viscosity of crude oil. However, the results obtained by these methods have significant errors when compared with the experimental data. In this study a robust artificial neural network （ANN） code was developed in the MATLAB software environment to predict the viscosity of Iranian crude oils. The results obtained by the ANN and the three well-established semi-empirical equations （Khan et al, 1987; Elsharkawy and Alikhan, 1999; Labedi, 1992） were compared with the experimental data. The prediction procedure was carried out at three different regimes： at, above and below the bubble-point pressure using the PVT data of 57 samples collected from central, southern and offshore oil fields of lran. It is confirmed that in comparison with the models previously published in literature, the ANN model has a better accuracy and performance in predicting the viscosity of Iranian crudes.

关键词： Viscosity crude oil artificial neural network empirical equations

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Micromechanical simulation and experimental investigation of aluminum-based nanocomposites

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Defence Technology（防务技术） 2021年第1期17卷 196-201页

作者： mohammad javad Ghasemi mohammad Silani Ali Maleki Mostafa Jamshidian Department of Mechanical Engineering Isfahan University of TechnologyIsfahan84156-83111Iran

Ceramic reinforced metal matrix nanocomposites are widely used in aerospace and auto industries due to their enhanced mechanical and physical *** this research,we investigate the mechanical properties of aluminum/Nano-silica composites through experiments and ***/Nanosilica composite samples with different weight percentages of silica nanoparticles are prepared via powder *** this method,Nano-silica and aluminum powders are mixed and compressed in a mold,followed by sintering at high *** tensile testing of the nanocomposite samples shows that adding one percent of Nano-silica causes a considerable increase in mechanical properties of nanocomposite compared to pure aluminum.A computational micromechanical model,based on a representative volume element of aluminum/silica nanocomposite,is developed in a commercial finite element *** model employs an elastoplastic material model along with a ductile damage model for aluminum matrix and linear elastic model for nano-silica *** careful determination of model parameters from the experimental results of pure aluminum samples prepared by powder metallurgy,the proposed computational model has shown satisfactory agreement with *** validated computational model can be used to perform a parametric study to optimize the microstructure of nanocomposite for enhanced mechanical properties.

关键词： Aluminum/nano-silica composites Powder metallurgy Micromechanics

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