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Ba substitution for enhancement of the thermoelectric properties of LaCoO_(3) ceramics(0≤x≤0.75)

Journal of Advanced Ceramics 2019年第4期8卷 519-526页

作者： mohamed Ali bousnina Fabien GIOVANNELLI Loic PERRIERE Guillaume GUEGAN Fabian DELORME Université Francois Rabelais de Tours CNRSINSA CVLGREMAN UMR7347IUT de Blois15 rue de la chocolaterieCS2903F-41029 Blois CedexFrance UniversitéParis 13 Sorbonne Paris CiteLaboratoire des Sciences des Procédés et des MatériauxCNRSUPR 340799 avenue J.B.ClémentF-93430 VilletaneuseFrance Institut de Chimie et des Matériaux Paris-Est UMR 7182 CNRS-UPEC2-8 Rue Henri Dunant94320 ThiaisFrance ST Microelectronics 16 Rue Pierre et Marie CurieTours 37100France

In the present work, dense perovskite ceramics were successfully prepared from a series of La1-xBaxCoO3 solid solutions in the range of substitution 0 ≤ x ≤ 0.75 using solid state reaction and conventional sintering. Structural properties of La1-xBaxCoO3 were systematically investigated and thermoelectric properties were measured in the temperature range of 330–1000 K. The results show that the thermoelectric properties of Ba-substituted LaCoO3 depend on x. Indeed, at 330 K, electrical conductivity presents an optimum value for x = 0.25 with a value of σmax ≈ 2.2×105 S·m–1 whereas the Seebeck coefficient decreases when x and/or the temperature increases. The Ba-substituted LaCoO3 samples exhibit p-type semiconducting behaviour. The best power factor value found is 3.4×10–4 W·m–1·K–2 at 330 K for x = 0.075, which is 10% higher than the optimum value measured in La1–xSrxCoO3 for x = 0.05. The thermal diffusivity and thermal conductivity increase with increasing temperature and Ba concentration. La1-xBaxCoO3 shows a maximum figure of merit(ZT = 0.048) for x = 0.05 at 330 K, 25% higher than the best value in La1–xSrxCoO3 compounds.

关键词： perovskite Ba-substituted LaCoO_(3) oxide thermoelectric p-type semiconductor

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Influence of Bi on the thermoelectric properties of SrTiO_(3-d)

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Journal of Materiomics 2019年第1期5卷 88-93页

作者： Cong Chen mohamed bousnina Fabien Giovannelli Fabian Delorme Universite de Tours CNRSINSA CVLGREMAN UMR 7347IUT de Blois15 rue de la chocolaterieCS 290341029Blois CedexFrance Bundesanstalt für Materialforschung und eprüfung(BAM) Unter den Eichen 8712205BerlinGermany

The thermoelectric properties of Sr1-xBixTiO_(3-δ)(0≤x≤0.07)have been *** ceramics of Sr1-xBixTiO_(3-δ) and Sr0.95TiO_(3-δ) have been prepared by solid-state reaction and conventional sintering in air followed by annealing in a reducing *** and SEM analyses show that the rutile TiO_(2 i)n Sr_(0.95)TiO_(3) formed after sintering becomes Magneli phase of TinO_(2n-1) after ***,Bi resolves from Sr1-xBixTiO_(3 )after annealing,resulting in the formation of Sr1-xBixTiO_(3-δ)/Bi/TinO_(2n-1) *** increasing Bi content in Sr1-xBixTiO_(3-δ),the electrical conductivity increases while the absolute values of the Seebeck coefficient decrease as a result of increasing carrier *** thermal conductivity of SrTiO_(3-δ) is reduced by doping Bi up to x=*** ZT~0.13 is obtained in Sr0.93Bi0.07TiO_(3-δ) at 1000 K.

关键词： Thermoelectrics SrTiO_(3) Composite Bi Magneli phase

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Monitoring the variation of soil quality with sewage sludge application rates in absence of rhizosphere effect

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International Soil and Water Conservation Research 2020年第3期8卷 245-252页

作者： Rahma Inès Zoghlami Helmi Hamdi Sonia Mokni-Tlili Sarra Hechmi mohamed Naceur Khelil Nadhira Ben Aissa mohamed Moussa Habib bousnina Saoussen Benzarti Naceur Jedidi Arid Regions Institute University of GabèsMèdenine4119Tunisia Water Research and Technology Center University of CarthageP.O.Box 273Soliman8020Tunisia Center for Sustainable Development College of Arts and SciencesQatar UniversityP.O.Box 2713DohaQatar National Institute for Research in Rural Engineering Water and ForestryP.O.Box 10Ariana2080Tunisia National Institute of Agronomy 43 Av.Charles NicolleTunis1082Tunisia College of Agriculture at Mograne University of Carthage1121MograneTunisia

Agricultural soils in semi-arid regions have frequently been degraded due to adverse climatic conditions,organic matter depletion,and poor farming *** enhance soil quality,this study examines the reuse of sewage sludge(SS)as an available source of organic matter in a typical Mediterranean sandy-loam ***,we studied the cumulative effect of two annual applications of 40,80 and 120 tons of sludge per ha on soil quality in absence of *** dose-dependent improvement of organic matter content was the most significant event that reflected sludge application rates,and consequently influenced other soil ***,soil structural stability increased by 13.3%,28.8%and 59.4%for treatments SS-40,SS-80 and SS-120 respectively as compared to unamended *** stability improvement was also confirmed by the dose-dependent variation of other edaphic factors including calcium content,the microbial quotient as well as Welt and C:N *** param-eters are involved in cementing soil aggregates by cation bridging,the formation of microbial mucilage,and clay-humic *** magnetic susceptibility(SMS)was measured in situ as a possible rapid tool to evaluate soil *** showed significant correlation with sludge dose and stability amelioration testifying to the aggregation role that can play Al2O3 and particularly Fe2O3 minerals added by the hematite-rich ***,analytical results and field observations revealed no trends of soil salinization or acidification by excessive sludge *** avoiding the rhizosphere effect,outcomes could reflect the resilience and intrinsic capacity of the soil to cope with excessive sludge loads.

关键词： Sandy loam soil Urban sewage sludge Structural stability Soil degradation Aggregation Magnetic susceptibility

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