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Adsorption of Malachite Green Using Activated Carbon from Mangosteen Peel: Optimization Using Box-Behnken Design

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Journal of Renewable Materials 2024年第5期12卷 981-992页

作者： Nabila Eka Yuningsih latifa Ariani Suprapto Suprapto Ita Ulfin Harmami Harmami Hendro Juwono Yatim lailun Ni’mah Department of Chemistry Faculty of Science and Data AnalyticsInstitute Technology of Sepuluh NopemberSurabaya60111Indonesia

In this research,activated carbon from mangosteen peel has been synthesized using sulfuric acid as an *** adsorption performance of the activated carbon was optimized using malachite green dye as ***-chite green dye waste is a toxic and non-biodegradable material that damages the *** of adsorption processes was carried out using Response Surface Methodology(RSM)with a Box-Behnken Design(BBD).The synthesized activated carbon was characterized using FTIR and SEM *** FTIR spectra conﬁrmed the presence of a sulfonate group(-SO_(3)H)in the activated carbon,indicating that the activation pro-cess using sulfuric acid was *** characterization shows that activated carbon has porous *** was carried out for three adsorption parameters,namely contact time(20,60,and 120 min),adsor-bent mass(0.005,0.025,and 0.05 g),and initial concentration of malachite green solution(5,50,and 100 mg·l^(-1)).The concentration of the malachite green solution was determined using a UV-Vis spectrophotometer at the max-imum wavelength of malachite green,618 *** optimum of malachite green adsorption using mangosteen peel activated carbon was obtained at a contact time of 80 min,an adsorbent mass of 0.032 g,and malachite green initial concentration of 25 mg·l^(-1),with a maximum removal percentage and maximum adsorption capacity of 93.66%and 19.345 mg·g^(-1),respectively.

关键词： Response surface methodology dyes activated carbon experimental design

男性雄激素性脱发患者毛囊皮脂腺单位的转录组学分析显示其细胞间连接网络发生改变

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中华皮肤科杂志 2024年第10期57卷 967-967页

作者： Elias Bou Samra Yann Franck mahé Mickael le Balch Nükhet Cavusoglu Pierre Bouhanna Khalid Bakkar l'Oréal Research and Innovation Aulnay-sous-Bois France Bouhanna Hair Transplant Clinic Paris France

随着研究的不断深入,越来越多的证据表明,脱发的发病机制涉及多种生理途径,包括引起直接损伤的炎症细胞因子和趋化因子、调节形态发生的以Wnt/β-联蛋白(catenin)为主的信号通路以及系统性炎症和脂质代谢相关通路。根据个体的遗传背景... 详细信息

随着研究的不断深入,越来越多的证据表明,脱发的发病机制涉及多种生理途径,包括引起直接损伤的炎症细胞因子和趋化因子、调节形态发生的以Wnt/β-联蛋白(catenin)为主的信号通路以及系统性炎症和脂质代谢相关通路。根据个体的遗传背景、生活方式、性别和年龄,上述效应因子和靶点先后被不同程度地激活。因此,深入解析脱发患者特异性的病理生理机制,对于制定精准的治疗方案尤为重要。

关键词：病理生理机制雄激素性脱发炎症细胞因子细胞间连接系统性炎症趋化因子脂质代谢形态发生

Upcycling the spent graphite/liCoO_(2) batteries for high-voltage graphite/liCoPO_(4)-co-workable dual-ion batteries

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International Journal of Minerals,Metallurgy and Materials 2024年第7期31卷 1745-1751页

作者： Miao Du Hongyan lü Kaidi Du Shuohang Zheng Xiaotong Wang Xiaotong Deng Ronghua Zeng Xinglong Wu Key laboratory for UV light-Emitting Materials and Technology of Ministry of Education Northeast Normal UniversityChangchun 130024China Faculty of Chemistry Northeast Normal UniversityChangchun 130024China School of Chemistry South China Normal UniversityGuangzhou 510006China

The worldwide proliferation of portable electronics has resulted in a dramatic increase in the number of spent lithium-ion batteries(lIBs).However,traditional recycling methods still have limitations because of such huge amounts of spent ***,we proposed an ecofriendly and sustainable double recycling strategy to concurrently reuse the cathode(liCoO_(2))and anode(graphite)materials of spent lIBs and recycled liCoPO_(4)/graphite(RlCPG)in li^(+)/PF^(-)_(6) co-de/intercalation dual-ion *** recycle-derived dualion batteries of li/RlCPG show impressive electrochemical performance,with an appropriate discharge capacity of 86.2 mah·g^(-1) at25 mA·g^(-1) and 69%capacity retention after 400 *** recycling of the cathode and anode from spent lIBs avoids wastage of resources and yields cathode materials with excellent performance,thereby offering an ecofriendly and sustainable way to design novel secondary batteries.

关键词： recycle lithium cobalt oxide lithium cobalt phosphate graphite dual-ion batteries spent lithium-ion batteries

AAV8 transduction capacity is reduced by prior exposure to endosome-like pH conditions

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Neural Regeneration Research 2021年第5期16卷 851-855页

作者： Jeffrey Alowell Kar Men mah John lBixby Vance Plemmon Miami Project to Cure Paralysis University of MiamiMiamiFLUSA Department of Neurological Surgery University of MiamiMiamiFLUSA Department of Molecular and Cellular Pharmacology University of MiamiMiamiFLUSA

Adeno-associated virus(AAV)is an essential instrument in the neuroscientist’s toolkit,which allows delivery of DNA to provide labeling with fluorescent proteins or genetic instructions to regulate gene *** the field of neural regeneration,the transduction of neurons enables the observation and regulation of axon growth and regeneration,and in the future will likely be a mechanism for delivering molecular therapies to promote sprouting and regeneration after central nervous system *** formulations of AAV preparations permit efficient viral transduction under physiologic conditions,but an improved understanding of the mechanistic limitations of AAV transduction may facilitate production of more resilient AAV strains for investigative and therapeutic *** studied AAV transduction in the context of prior exposure of AAV serotype 8(AAV8)to environmental pH within the range encountered during endosomal endocytosis(pH 7.4 to pH 4.4),during which low pH-triggered structural and autoproteolytic changes to the viral capsid are believed to be necessary for endosome escape and virus *** to the fundamental nature of these processes,we hypothesized that premature exposure of AAV8 particles to acidic pH would decrease viral transduction of HT1080 cells in vitro,as measured by fluorescent reporter gene expression using high-content imaging *** found that increasingly acidic incubation conditions were associated with concomitant reductions in transduction efficiency,and that quantitative levels of reporter gene expression in transduced cells were similarly *** biggest decrease in transduction occurred between pH 7.4 and pH 6.4,suggesting the possible co-occurrence of a pH-associated event and viral inactivation within that *** together,these findings indicate that exposure of AAV8 to acidic pH for as little as 1 hour is deleterious to transduction *** studies are necessary to understand the pH-associated

关键词： adeno-associated virus autolytic capsid low pH protease proteolytic temperature trafficking transduction viral inactivation

The Adsorption of Pb(II)Using Silica Gel Synthesized from Chemical Bottle Waste:Optimization Using Box-Behnken Design

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Journal of Renewable Materials 2023年第6期11卷 2913-2924页

作者： Yatim lailun Ni’mah Nabila Eka Yuningsih Suprapto Suprapto Department of Chemistry Faculty of Science and Data AnalyticsInstitut Teknologi Sepuluh NopemberSurabayaIndonesia

The adsorption of Pb(II)on silica gel synthesized from chemical glass bottle waste has been *** effect of independent variables(adsorbent dose,initial concentration of Pb(II),contact time,and pH)on the Pb(II)removal from water was evaluated and optimized using the Response Surface Methodology(RSM).Under optimized conditions(adsorbent dose:20 mg;contact time:30 min;initial Pb(II)concentration:120 mg.l^(−1);and pH:8),the removal of Pb(II)was 99.77%.The adsorption equilibrium data obtained from the batch experiment were investigated using different isotherm *** langmuir isotherm model fits the experimental *** shows that the surface of the silica gel synthesized from chemical bottles waste was covered by a Pb(II)*** analysis showed that the synthesized silica gel had a SiO_(2) content of 75.63%.Amorphous silica was observed from XRD ***-EDX characterization showed that Pb was adsorbed on the silica gel *** analysis showed that silica gel has irregular particles with a surface area of 297.08 m2.g^(−1) with a pore radius of 15.74 nm calculated from BET analysis.

关键词： Chemical bottle waste silica gel adsorption box-behnken design response surface methodology

Inheritance patterns of secondary symbionts during sexual reproduction of pea aphid biotypes

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Insect Science 2014年第3期21卷 291-300页

作者： Jean Peccoud Joêl Bonhomme Frédérique mahéo Manon de la Huerta Olivier Cosson Jean-Christophe Simon INRA Institut de Génétique Environnement et Protection des Plantes (UMR IGEPP) Domaine de La Motte 35653 le Rheu cedex France

Herbivorous insects frequently harbor bacterial symbionts that affect their ecol- ogy and evolution. Aphids host the obligatory endosymbiont Buchnera, which is requiredfor reproduction, together with facultative symbionts whose frequencies vary across aphid populations. These maternally transmitted secondary symbionts have been particularlystudied in the pea aphid, Acyrthosiphon pisum, which harbors at least 8 distinct bacterial species （not counting Buchnera） having environmentally dependent effects on host *** particular, these symbiont species are associated with pea aphid populations feeding on specific plants. Although they are maternally inherited, these bacteria are occasionallytransferred across insect lineages. One mechanism of such nonmaternal transfer is paternal transmission to the progeny during sexual reproduction. To date, transmission of secondarysymbionts during sexual reproduction of aphids has been investigated in only a handful of aphid lineages and 3 symbiont species. To better characterize this process, we investigatedinheritance patterns of 7 symbiont species during sexual reproduction of pea aphids through a crossing experiment involving 49 clones belonging to 9 host-specialized biotypes, and117 crosses. Symbiont species in the progeny were detected with diagnostic qualitative PCR at the fundatrix stage hatching from eggs and in later parthenogenetic *** found no confirmed case of paternal transmission of symbionts to the progeny, and we observed that maternal transmission of a particular symbiont species （Serratia symbiotica）was quite inefficient. We discuss these observations in respect to the ecology of the pea aphid.

关键词： bacteria Homoptera paternal inheritance phytophagous insects symbiosis transmission failure

The Fabrication of Water-Soluble Chitosan Capsule Shell Modified by Alginate and Gembili Starch(Dioscorea esculenta l)

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Journal of Renewable Materials 2022年第9期10卷 2365-2376页

作者： Yatim lailun Ni’mah Suprapto Suprapto Harmami Ita Ulfin Puput Asmaul Fauziyah Chemistry Department Faculty of Science and Analytical DataInstitut Teknologi Sepuluh NopemberSurabayaIndonesia

Capsule shells have been successfully fabricated from water-soluble chitosan(WSC)with the addition of alginate and Gembili *** was synthesized from crab shell chitosan by depolymerization *** capsule shells were made with the composition of WSC:Alginate,2:1,3:1 and 4:1(w/w)with and without the addition of Gembili *** starch was added with a ratio of Alginate:Starch,1:1(w/w).The capsule shell properties were evaluated according to Indonesian Pharmacopoeia *** solubility test showed that the capsule shells were comply with the *** highest degrees of swelling in water and HCl 0.1 N solution were 491.93%and 410.51%,*** highest degradation percentages in water and HCl 0.1 N solution were 57.80%and 21.44%,*** observation of physical appearance indicated that the capsule shell with WSC:Alginate:Starch in ratio of 3:1:1 has appearance close to commercial capsule shell.

关键词： Capsule shell water soluble chitosan capsule shell degradation capsule shell solubility

Silica Gel from Chemical Glass Bottle Waste as Adsorbent for Methylene Blue:Optimization Using BBD

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Journal of Renewable Materials 2023年第12期11卷 4007-4023页

作者： Suprapto Suprapto Putri Augista Nur Azizah Yatim lailun Ni’mah Chemistry Department Faculty of Science and Analytical DataInstitut Teknologi Sepuluh NopemberSurabayaIndonesia

This research focuses on the effective removal of methylene blue dye using silica gel synthesized from chemical glass bottle waste as an environmentally friendly and cost-effective *** adsorption process was optimized using Box-Behnken Design(BBD)and Response Surface Methodology(RSM)to investigate the influence of pH(6;8 and 10),contact time(15;30 and 45 min),adsorbent mass(30;50 and 70 mg),and initial concentration(20;50 and 80 mg/l)of the adsorbate on the adsorption *** BBD was conducted using Google Colaboratory software,which encompassed 27 experiments with randomly assigned *** silica gel synthesized from chemical glass bottle was characterized by XRD,FTIR,SEM-EDX and *** adsorption result was measured by spectrophotometer *** optimized conditions resulted in a remarkable methylene blue removal efficiency of 99.41%.Characterization of the silica gel demonstrated amorphous morphology and prominent absorption bands characteristic of *** langmuir isotherm model best described the adsorption behavior,revealing chemisorption with a monolayer coverage of methylene blue on the adsorbent surface,and a maximum adsorption capacity of 82.02 mg/***,the pseudo-second-order kinetics model indicated a chemisorption mechanism during the adsorption *** findings highlight the potential of silica gel from chemical glass bottle waste as a promising adsorbent for wastewater treatment,offering economic and environmental *** investigations can explore its scalability,regenerability,and reusability for industrial-scale applications.

关键词： Glass bottle waste silica gel adsorption waste treatment methylene blue Box-Behnken design

Improving cycling performance of the NaNiO_(2)cathode in sodium-ion batteries by titanium substitution

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Materials Futures 2024年第3期3卷 132-147页

作者： Siyu An leonhard Karger Sören l Dreyer Yang Hu Eduardo Barbosa Ruizhuo Zhang Jing lin Maximilian Fichtner Aleksandr Kondrakov Jürgen Janek Torsten Brezesinski Battery and Electrochemistry laboratory(BEllA) Institute of NanotechnologyKarlsruhe Institute of Technology(KIT)Kaiserstr.1276131 KarlsruheGermany Helmholtz Institute Ulm(HIU)Electrochemical Energy Storage Helmholtzstr.1189081 UlmGermany BASF SE Carl-Bosch-Str.3867056 LudwigshafenGermany Institute of Physical Chemistry&Center for Materials Research(ZfM/laMa) Justus-Liebig-University GiessenHeinrich-Buff-Ring 1735392 GiessenGermany

O3-type layered oxide cathodes,such as NaNi_(0.5)Mn_(0.5)O_(2),have garnered significant attention due to their high theoretical specific capacity while using abundant and low-cost sodium as intercalation *** the lithium analog(liNiO_(2)),NaNiO_(2)(NNO)exhibits poor electrochemical performance resulting from structural instability and inferior Coulomb *** enhance its cyclability for practical application,NNO was modified by titanium substitution to yield the O3-type NaNi_(0.9)Ti_(0.1)O_(2)(NNTO),which was successfully synthesized for the first time via a solid-state *** mechanism behind its superior performance in comparison to that of similar materials is examined in detail using a variety of characterization *** delivers a specific discharge capacity of∼190 mah g^(−1)and exhibits good reversibility,even in the presence of multiple phase transitions during cycling in a potential window of 2.0−4.2 V ***^(+)/*** behavior can be attributed to the substituent,which helps maintain a larger interslab distance in the Na-deficient phases and to mitigate Jahn–Teller activity by reducing the average oxidation state of ***,volume collapse at high potentials and irreversible lattice oxygen loss are still detrimental to the ***,the performance can be further enhanced through coating and doping *** not only positions NNTO as a promising next-generation cathode material,but also serves as inspiration for future research directions in the field of high-energy-density Na-ion batteries.

关键词： Ni-rich layered oxide cathode material substitution doping electro-chemo-mechanical degradation Na-ion battery