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Electrochemical anodization of cast titanium alloys in oxalic acid for biomedical applications

Frontiers of Chemical Science and Engineering 2024年第1期18卷 13-24页

作者： Engie M.Safwat Soha A.Abdel-Gawad madiha A.shoeib Shimaa El-Hadad Restorative and Dental Materials Department National Research CentreGiza 12622Egypt Chemistry Department Faculty of ScienceCairo UniversityGiza 12613Egypt Central Metallurgical Research and Development Institute Helwan 11421Egypt

Titanium and its alloys have numerous biomedical applications thanks to the composition and morphology of their oxide *** this study,the colorful oxide films were formed by anodizing cast Ti-6Al-4V and Ti-6Al-7Nb alloys in a 10%oxalic acid solution for 30 s at different voltages(20–80 V)of a direct current power *** force microscopy was used as an accurate tool to measure the surface roughness of thin films on the nanometer *** electron microscopy and X-ray diffraction were performed to analyze surface morphology and phase *** to the results,the produced titanium oxide layer showed high surface roughness,which increased with increasing anodizing *** impact of anodizing voltages on the color and roughness of anodized layers was *** corrosion resistance of the anodized samples was studied in simulated body fluid at pH 7.4 and a temperature of 37℃ utilizing electrochemical impedance spectroscopy and the potentiodynamic polarization *** anodized samples for both alloys at 40 V were at the optimal voltage,leading to a TiO_(2) layer formation with the best compromise between oxide thickness and corrosion ***,findings showed that TiO_(2) films produced on Ti-6Al-7Nb alloys had superior surface roughness properties compared to those of Ti-6Al-4V alloys,making them more appropriate for orthopedic *** the obtained data and the fruitful discussion,it was found that the utilized procedure is simple,low-cost,and ***,anodization in 10%oxalic acid proved a viable alternative for the surface finishing of titanium alloys for biomedical applications.

关键词： DC anodization Ti-6Al-4V alloy Ti-6Al-7Nballoy oxidefilm corrosion

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Influence of anodization conditions on deposition of Hydroxyapatite on α/β Ti alloys for Osseointegration: Atomic Force Microscopy Analysis

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Transactions of Nonferrous Metals Society of China 2024年

作者： Rania E.Hammam Engie M.Safwat Soha A.Abdel-Gawad madiha shoeib Shimaa El-Hadad Faculty of Engineering， Modern University for Technology and Information (MTI) Restorative and Dental Materials Department， National Research Centre Giza Chemistry Department， Faculty of Science， Cairo University Central Metallurgical Research and Development Institute P.O.87

Integrating titanium-based implants with the surrounding bone tissue remains challenging. This study aims to explore the impact of different anodization voltages （20-80V） on the surface topography of two-phase （α/β） Ti alloys and to produce TiO2films with enhanced bone formation abilities. Scanning electron microscopy coupled with energy dispersive spectroscopy （SEM-EDS） and atomic force microscopy （AFM） were applied to investigate the morphological， chemical， and surface topography of the prepared alloys and to confirm the growth of hydroxyapatite （HA） on their surfaces. Results disclosed that the surface roughness of TiO2films formed on Ti-6Al-7Nb alloys was superior to that of Ti–6Al–4V alloys. Ti-6Al-7Nb alloy anodized at 80 V had the highest yields of HA after immersion in SBF with enhanced HA surface coverage. The developed HA layer had a mean thickness of 128.38 ± 18.13 μm， suggesting its potential use as an orthopedic implantable material due to its promising bone integration and， hence， remarkable stability inside the human body.

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