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Infrared Spectroscopy and morphological Assessments on the nutritional Value of Prickly Pear Fruit

光谱学与光谱分析 2021年第2期41卷 648-653页

作者： m.am.n srefat amnah mAlsuhaibani mo hamed nagaty Department of Chemistry College of ScienceTaif UniversityTaif21944Saudi Arabia Department of Physical Sport Science Princess Nourah bint Abdulrahman UniversityRiyadh13415-7132Saudi Arabia

The prickly pear fruit helps in combating viral based *** is used to treat diabetes and declared to possess hypoglycemic *** is also record of the usage of the fruit in the olden days as a remedy for diabetes,lipid disorders,inflammation,ulcers,and pharmacologic side *** chemical composition and nutritional values of skin,flesh and seed of prickly pear fruit were investigated and discussed on a dry weight *** infrared spectra as well as scanning electron microscopy(SEm)techniques were used to identify the functional groups of carbohydrates,amino acids,and *** infrared spectral data of all three(skin,flesh,and seeds)species were recorded and assigned to the presence of distinguish peaks that referred to the three different sugars(glucose,fructose and saccharose)and cyclic aliphatic hydrocarbons *** the other hand,the SEm is a powerful tool to investigate the morphological features of the *** assays were examined on the surfaces of skin,flesh and seed branches showing a small particle that tends to form clusters with different shapes compared to each *** Energy-dispersive X-ray spectroscopy(EDX)is an analytical technique used for the elemental analysis or chemical characterization of a *** EDX spectral technique of the skin,flesh and seeds were confirmed the presence of different essential and useful elements such as carbon,oxygen,magnesium,calcium,potassium,sulfur,aluminum,silicon,chloride,and phosphorus.

关键词： Infrared spectroscopy SEm EDX Prickly pear fruit Skin Flesh Seed

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Synthesis,Spectroscopic Characterization,Thermogravimetric and Biological Activity Evaluation of Te(Ⅳ),Se(Ⅳ),V(Ⅲ),nb(Ⅴ),Ta(Ⅴ)Complexes With Indole-3-Acetic Acid Plant Hormone Ligand

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光谱学与光谱分析 2021年第2期41卷 658-664页

作者： Jehan YAl-Humaidi Foziah AAl-Saif Dalal nB injawhar Hanan ABakhsh m.am.n srefat Department of Chemistry College of SciencePrincess Nourah bint Abdulrahman UniversityRiyadh11671Saudi Arabia Department of Chemistry Faculty of ScienceTaif UniversityAl-Haweiah21974TaifSaudi Arabia

Te(Ⅳ),Se(Ⅳ),V(Ⅲ),nb(Ⅴ)and Ta(Ⅴ)complexes of indole-3-acetic acid(IAAH)ligand were synthesized,characterized by elemental analysis and various spectroscopic techniques like,IR,1H-nmR,X-ray powder diffraction,UV-Visible,thermogravimetry analysis,magnetic measurements,molar conductance and surface morphology using *** the synthesized complexes of IAAH ligand have 1∶2 stoichiometry of the types[Te(IAA)2(nH 3)2]·2Cl(Ⅰ),[Se(IAA)2(nH 3)2]·2Cl(Ⅱ),[V(IAA)2(nH 3)(Cl)](Ⅲ),[nb(IAA)2(Cl)3](Ⅳ),and[Ta(IAA)2(Cl)3](Ⅴ).Spectral analysis indicates octahedral geometry for the Te(Ⅳ),Se(Ⅳ)and V(Ⅲ)complexes,whereas both nb(Ⅴ)and Ta(Ⅴ)have a *** bonding sites are the oxygen atoms of carboxylate group for the deprotonated indole-3-acetic acid(IAA)*** thermogravimetry analysis studies gave evidence for the presence of other coordinated molecules(Cl or nH 3)in the composition of IAA complexes,which were further supported by IR and micro analytical *** higher molar conductance data of tellurium and selenium(Ⅳ)complexes reveal that these chelates are electrolytes,while low conductivity values for the vanadium(Ⅲ),niobium and tantalum(Ⅴ)chelates indicated a *** test the antibacterial property of the five complexes in this study,four bacterial strains Klebsiella(G-),Escherichia coli(G-),Staphylococcus aureus(G+)and Staphylococcus epidermidis(G+)were used in the *** effects of the five complexes in the cytotoxicity of Caco-2 and mcf-7 human cancer cell lines were studied neutral red uptake assay for the estimation of cell viability/cytotoxicity protocol.

关键词： Indole-3-acetic acid chelation IR metal ions TEm Antimicrobial test

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Synthesis, Spectroscopic Characterization and Thermogravimetric Analysis of Cr(Ⅱ), Cu(Ⅱ), Zn(Ⅱ) and mg(Ⅱ),Captopril Coordination Compounds

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光谱学与光谱分析 2020年第2期40卷 661-664页

作者： Asma SAl-Wasidi nawal mAl-Jafshar amal mAl-Anazi Ahmed m.naglah Robson Fde Farias Claudio Airoldi m.am.n srefat Department of Chemistry College of SciencePrincess Nourah Bint Abdulrahman UniversityRiyadh 11671Saudi Arabia Department of Pharmaceutical Chemistry Drug Exploration and Development Chair(DEDC)College of PharmacyKing Saud UniversityRiyadh 11451Saudi Arabia Peptide Chemistry Department Chemical Industries Research DivisionNational Research CentreCairo 12622-DokkiEgypt Departamento de Química Universidade Federal do Rio Grande do NorteCx.Postal 166459078-970 NatalRio Grande do NorteBrasil Instituto de Química Universidade Estadual de CampinasBrasil Chemistry Department Faculty of ScienceTaif UniversityP.O.Box 888Al-HawiahTaif 21974Saudi Arabia Department of Chemistry Faculty of SciencePort SaidPort Said UniversityEgypt

In this work,we have reported the synthesis and spectroscopic characterization of captopril(Cap)coordination compounds:Cu(Cap)·2H 2O,Cr(Cap)·H 2O,Zn(Cap)·3H 2O and mg(Cap)***,it is worthily mentioned that the FTIR spectroscopic technique was employed to recognized the nature of coordination between captopril ligand and copper,chromium,zinc and magnesium(Ⅱ)metal *** view of the infrared spectroscopic tool,the copper(Ⅱ)metal ion coordinated toward captopril drug ligand through sulfur atom of SH group dependent on the absent of stretching vibration band of—*** on this result,the stretching motion ofνa(COO)shifts clearly indicates that Cu 2+,Cr 2+,Zn 2+and mg 2+the carboxylic group is employed as coordinative site for all compounds as a metal-ligand coordinative *** a general behavior,it is verified that the coordination compound thermal stability(considering the release of captopril molecules,not the release of water molecules)is affected by the metal cation radius:minor radius is associated with higher thermal stability,probably due to a higher metal-captopril bond dissociation enthalpy.

关键词： Captopril Transition metals Spectroscopy Coordination compounds Thermogravimetry

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