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Rare Metals 2024年第5期43卷 2241-2250页

作者： Pei-Sen Wang Zi-Tong Wang Ya-Ya Tan Peng Chen Xue-Cheng zhang lu-nan zhang Yong-Ge Wei lu-Bin Ni School of Chemistry and Chemical Engineering Yangzhou UniversityYangzhou 225002China Key Lab of Organic Optoelectronics and Molecular Engineering of Ministry of Education Department of ChemistryTsinghua UniversityBeijing 100084China State Key Laboratory of Natural and Biomimetic Drugs Peking UniversityBeijing100191China

An inorganicDorganic hybrid crystalline material(SiMo_(12)O_(40))[Cu(2,2'-bipy)_(2)]_(2)·2H_(2)O(Complex 1,2,2'-bipy=2,2'-bipyridine)was synthesized for the first time by using 2,2'-bipy and transition metal copper to convert Waugh-type polyoxometalate[MnMo_(9)O_(3)_(2)]_(6-)into a Keggin polyoxometalate structure[SiMo_(12)O_(40)]^(4-)under hydrothermal conditions in glass *** crystal tests and a series of characterizations were carried out on Complex *** structure of Complex 1 is composed of[SiMo_(12)O_(40)]^(4-)and[Cu^(Ⅱ)(2,2'-bipy)_(2)]^(2+).The five-coordinated Cu is connected to two 2,2'-bipy through CuDN bonds,forming an approximately square ***,Complex 1 exhibited good photocatalytic performance for methylene blue degradation and electrocatalytic nitrite reduction properties simultaneously.

关键词： Polyoxometalates Inorganic-organic hybrid materials Photocatalytic Electrocatalytic

External quality assessment on detection of hepatitis C virus RNA in clinical laboratories of China

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Chinese Medical Journal 2008年第11期121卷 1032-1036页

作者： WANG lu-nan zhang Rui SHEN Zi-yu CHEN Wen-xiang LI Jin-ming National Center for Clinical Laboratory Beijing Hospital Beijing 100730 China

Background As with many studies carried out in European countries, a quality assurance program has been established by the National Center for Clinical Laboratories in China （NCCL）. The results showed that the external quality assessment significantly improves laboratory performance for quantitative evaluation of hepatitis C virus （HCV） RNA. Methods Serum panels were delivered twice annually to the clinical laboratories which performed HCV RNA detection in China. Each panel made up of 5 coded samples. All laboratories were requested to carry out the detection within the required time period and report on testing results which contained qualitative and/or quantitative test findings, reagents used and relevant information about apparatus. All the positive samples were calibrated against the first International Standard for HCV RNA in a collaborative study and the range of comparison target value （TG） designated as ±0.5 log. Results The numbers of laboratories reporting on qualitative testing results for the first and second time external quality assessment were 168 and 167 in the year of 2003 and increased to 209 and 233 in 2007; the numbers of laboratories reporting on quantitative testing results were 134 and 147 in 2003 and rose to 340 and 339 in 2007. Deviation between the mean value for quantitative results at home in 2003 and the target value was above 0.5 log, which was comparatively high. By 2007, the target value was close to the national average except for the low concentrated specimens （10^3 IU/ml）. The percentage of results within the range of GM±0.5 log10 varied from 8.2% to 93.5%. Some laboratories had some difficulties in the exact quantification of the lowest （3.00 log IU/ml） as well as of the highest viral levels （6.37 log IU/ml） values, very near to the limits of the dynamic range of the assays. Conclusions The comparison of these results with the previous study confirms that a regular participation in external quality assessment （EQA） assures

关键词： polymerase chain reaction hepatitis C external quality assessment

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P波作用下机场跑道的爆破安全振动速度研究

华南理工大学学报（自然科学版） 2018年第4期46卷 129-136页

作者：胡守云周传波蒋楠路世伟张震何如中国地质大学(武汉)工程学院湖北武汉430074

结合湖北省首例下穿机场跑道隧道钻爆法开挖工程背景,基于理论解析、数值模拟与现场监测相结合的研究方法,分析了下穿隧道爆破产生的入射P波对混凝土跑道的作用机理,研究了机场跑道的隧道爆破振动安全判据.结果表明:下穿跑道隧道爆破振... 详细信息

结合湖北省首例下穿机场跑道隧道钻爆法开挖工程背景,基于理论解析、数值模拟与现场监测相结合的研究方法,分析了下穿隧道爆破产生的入射P波对混凝土跑道的作用机理,研究了机场跑道的隧道爆破振动安全判据.结果表明:下穿跑道隧道爆破振动作用下,岩石与混凝土跑道交界面以拉伸破坏为主;随着入射P波入射角的增大,机场跑道的爆破安全振动速度呈现先增大后减小的趋势,其最小值出现在入射角为零时(即垂直入射的情况),表明爆破地震波垂直入射时机场跑道最容易发生破坏;基于机场跑道的重要性,选取1.7为重要性修正系数,依据爆破地震波以不同角度入射时确定的爆破安全振动速度,得到修正后的爆破安全振动速度在3.67~7.91 cm/s之间;与数值模拟和回归分析结果相比,由于应力波理论分析忽略了材料塑性变形的影响,其计算分析得到的爆破安全振动速度更小,具有更高的安全储备.

关键词：隧道掘进爆破振动安全振动速度入射P波混凝土跑道

Multi-Stage-Based Siamese Neural Network for Seal Image Recognition

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Computer Modeling in Engineering & Sciences 2025年第1期142卷 405-423页

作者： Jianfeng lu Xiangye Huang Caijin Li Renlin Xin Shanqing zhang Mahmoud Emam School of Computer Science and Technology Hangzhou Dianzi UniversityHangzhou310018China Shangyu Institute of Science and Engineering Hangzhou Dianzi UniversityShaoxing312300China Faculty of Artificial Intelligence Menoufia UniversityShebin El-Koom32511Egypt

Seal authentication is an important task for verifying the authenticity of stamped seals used in various domains to protect legal documents from tampering and *** seal inspection is commonly audited manually to ensure document ***,manual assessment of seal images is tedious and laborintensive due to human errors,inconsistent placement,and completeness of the *** image recognition systems are inadequate enough to identify seal types accurately,necessitating a neural network-based method for seal image ***,neural network-based classification algorithms,such as Residual Networks(ResNet)andVisualGeometryGroup with 16 layers(VGG16)yield suboptimal recognition rates on stamp ***,the fixed training data categories make handling new categories to be a challenging *** paper proposes amulti-stage seal recognition algorithmbased on Siamese network to overcome these ***,the seal image is pre-processed by applying an image rotation correction module based on Histogram of Oriented Gradients(HOG).Secondly,the similarity between input seal image pairs is measured by utilizing a similarity comparison module based on the Siamese ***,we compare the results with the pre-stored standard seal template images in the database to obtain the seal *** evaluate the performance of the proposed method,we further create a new seal image dataset that contains two subsets with 210,000 valid labeled pairs in *** proposed work has a practical significance in industries where automatic seal authentication is essential as in legal,financial,and governmental sectors,where automatic seal recognition can enhance document security and streamline validation ***,the experimental results show that the proposed multi-stage method for seal image recognition outperforms state-of-the-art methods on the two established datasets.

关键词： Seal recognition seal authentication document tampering siamese network spatial transformer network similarity comparison network

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相变蓄能抗冻太阳能平板集热器的设计与研究

中南大学学报（自然科学版） 2016年第10期47卷 3575-3581页

作者：赵静王智平王克振陆鑫张楠寇宗丽兰州理工大学材料科学与工程学院甘肃兰州730050 兰州理工大学能源与动力工程学院甘肃兰州730050

提出一种具有抗冻功能的相变蓄能太阳能平板集热器。该集热器在吸热板与保温层之间增加了一层相变潜热大、相变温度为277.15~281.15 K的相变蓄能材料。根据该集热器的传热机理,给出计算相变蓄能层设计厚度的公式。采用ANSYS Fluent软件... 详细信息

提出一种具有抗冻功能的相变蓄能太阳能平板集热器。该集热器在吸热板与保温层之间增加了一层相变潜热大、相变温度为277.15~281.15 K的相变蓄能材料。根据该集热器的传热机理,给出计算相变蓄能层设计厚度的公式。采用ANSYS Fluent软件建立该集热器的三维非稳态模型,模拟不同工况下集热器的出口温度及其内部水的最低温度。研究结果表明:在冬季环境温度最低日,相变蓄能抗冻集热器内水的最低温度高于275.15 K,能很好地起到抗冻作用;相变蓄能抗冻集热器与相同结构的普通集热器相比,冬季阴天和晴天代表日的净得热量分别高1.3 MJ/m^2和0.7 MJ/m^2。

关键词：相变蓄能层抗冻数值模拟太阳能平板集热器

疲劳-冻融多次交互作用下混凝土损伤特性试验研究

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混凝土 2018年第4期 46-49页

作者：逯静洲张楠国力童立强烟台大学土木工程学院山东烟台264005

通过对混凝土棱柱体试件进行疲劳荷载和冻融循环交互试验,分析疲劳荷载及冻融循环次数对试验后试件外观形貌、质量、相对动弹性模量和抗压强度的损伤劣化影响。试验结果表明:随着交互试验次数的增多,混凝土试件表面的坑洼面变多、孔洞变... 详细信息

通过对混凝土棱柱体试件进行疲劳荷载和冻融循环交互试验,分析疲劳荷载及冻融循环次数对试验后试件外观形貌、质量、相对动弹性模量和抗压强度的损伤劣化影响。试验结果表明:随着交互试验次数的增多,混凝土试件表面的坑洼面变多、孔洞变大,粗细骨料分离,质量出现先增加后减小的变化趋势,相对动弹性模量及试件的抗压强度下降速率明显加快。3个试验周期后,交互作用的试件与仅冻融循环的试件相比,试件的质量损失率增加0.36%,相对动弹性模量下降30.6%。混凝土的抗压强度降低18.1%。

关键词：疲劳荷载冻融循环交互作用相对动弹性模量抗压强度

9个能源柳无性系的生物量、热值和能量现存量

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北京林业大学学报 2016年第9期38卷 55-61页

作者：张英楠芦静张启昌王国胜邵殿坤施莹吉林省林业调查规划院北华大学林学院吉林省速生丰产林工作站

采用直接收获法、快速灰化法和量热法对引进的4种7个能源柳无性系(钻石柳AS625、AS287,旱×白柳AAUSC、AAUSL,欧洲红皮柳AFC190、AFC189,毛枝柳ASV1)和2个对照本地柳(旱柳和杞柳)的生物量、灰分含量、去灰分热值和能量现存量进行研究。... 详细信息

采用直接收获法、快速灰化法和量热法对引进的4种7个能源柳无性系(钻石柳AS625、AS287,旱×白柳AAUSC、AAUSL,欧洲红皮柳AFC190、AFC189,毛枝柳ASV1)和2个对照本地柳(旱柳和杞柳)的生物量、灰分含量、去灰分热值和能量现存量进行研究。结果表明:以AAUSC的生物量最高,为92.9 t/hm2,其次是AAUSL,生物量为65.13 t/hm^2,AS287的生物量最小,仅为4.31 t/hm^2。不同器官的灰分含量为:树叶8.28%~12.70%,树枝1.98%~4.17%,干2.51%~3.82%;去灰分热值为树叶15 636.29~18 840.77 J/g,树枝18 162.30~19 124.39 J/g,干17 219.71~18 756.31 J/g。7个能源柳无性系不同器官的灰分含量和去灰分热值差异均极显著(P<0.01)。引进的能源柳中能量现存量最高的无性系为AAUSC(15.84×108k J/hm2),其次为AAUSL(11.88×108k J/hm2),AS287最小(0.77×108k J/hm^2)。能源柳的能量现存量为乔木柳高于灌木柳,引进的能源柳高于本地柳。

关键词：能源柳灰分含量去灰分热值能量现存量

Inhibiting ceramide synthase 5 expression in microglia decreases neuroinflammation after spinal cord injury

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Neural Regeneration Research 2025年第10期20卷 2955-2968页

作者： Wei zhang Yubao lu Ruoqi Shen Yingjie Wu Chenrui Liu Xingxing Fang Liangming zhang Bin Liu Limin Rong Department of Spine Surgery The Third Affiliated HospitalSun Yat-sen UniversityGuangzhouGuangdong ProvinceChina National Medical Products Administration(NMPA)Key Laboratory for Quality Research and Evaluation of Cell Products GuangzhouGuangdong ProvinceChina Guangdong Provincial Center for Quality Control of Minimally Invasive Spine Surgery GuangzhouGuangdong ProvinceChina Guangdong Provincial Center for Engineering and Technology Research of Minimally Invasive Spine Surgery GuangzhouGuangdong ProvinceChina

Microglia,the resident monocyte of the central nervous system,play a crucial role in the response to spinal cord ***,the precise mechanism remains *** investigate the molecular mechanisms by which microglia regulate the neuroinflammatory response to spinal cord injury,we performed single-cell RNA sequencing dataset analysis,focusing on changes in microglial *** found that the MG1 subpopulation emerged in the acute/subacute phase of spinal cord injury and expressed genes related to cell pyroptosis,sphingomyelin metabolism,and neuroinflammation at high ***,we established a mouse model of contusive injury and performed intrathecal injection of siRNA and molecular inhibitors to validate the role of ceramide synthase 5 in the neuroinflammatory responses and pyroptosis after spinal cord ***,we established a PC12-BV2 cell co-culture system and found that ceramide synthase 5 and pyroptosis-associated proteins were highly expressed to induce the apoptosis of neuron *** ceramide synthase 5 expression in a mouse model of spinal cord injury effectively reduced ***,ceramide synthase 5-induced pyroptosis was dependent on activation of the NLRP3 signaling *** ceramide synthase 5 expression in microglia in vivo reduced neuronal apoptosis and promoted recovery of neurological ***2g7 formed a“bridge”between sphingolipid metabolism and ceramide synthase 5-mediated cell death by inhibiting the NLRP3 signaling ***,these findings suggest that inhibiting ceramide synthase 5 expression in microglia after spinal cord injury effectively suppressed microglial pyroptosis mediated by NLRP3,thereby exerting neuroprotective effects.

关键词： ceramide synthase 5 gasdermin D microglia neuroinflammation NLRP3 nuclear factor kappa B Pla2g7 pyroptosis sphingomyelin metabolism spinal cord injury

Catalyst–Support Interaction in Polyaniline‑Supported Ni_(3)Fe Oxide to Boost Oxygen Evolution Activities for Rechargeable Zn‑Air Batteries

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nano-Micro Letters 2025年第1期17卷 176-190页

作者： Xiaohong Zou Qian lu Mingcong Tang Jie Wu Kouer zhang Wenzhi Li Yunxia Hu Xiaomin Xu Xiao zhang Zongping Shao Liang An Department of Mechanical Engineering The Hong Kong Polytechnic UniversityHung HomKowloonHong Kong SARPeople’s Republic of China Jiangsu Key Laboratory of Atmospheric Environment Monitoring and Pollution Control Jiangsu Collaborative Innovation Center of Atmospheric Environment and Equipment TechnologySchool of Environmental Science and TechnologyNanjing University of Information Science and TechnologyNanjing 210044People’s Republic of China Department of Chemistry The Chinese University of Hong KongMa Lin BuildingShatinHong Kong SAR 999077People’s Republic of China WA School of Mines:Minerals Energy and Chemical Engineering(WASM‑MECE)Curtin UniversityPerthWA 6102Australia Research Institute for Advanced Manufacturing The Hong Kong Polytechnic UniversityHung HomKowloonHong Kong SARPeople’s Republic of China Research Institute for Smart Energy The Hong Kong Polytechnic UniversityHung HomKowloonHong Kong SARPeople’s Republic of China

Catalyst–support interaction plays a crucial role in improving the catalytic activity of oxygen evolution reaction(OER).Here we modulate the catalyst–support interaction in polyaniline-supported Ni_(3)Fe oxide(Ni_(3)Fe oxide/PANI)with a robust hetero-interface,which significantly improves oxygen evolution activities with an overpotential of 270 mV at 10 mA cm^(-2)and specific activity of 2.08 mA cm_(ECSA)^(-2)at overpotential of 300 mV,3.84-fold that of Ni_(3)Fe *** is revealed that the catalyst–support interaction between Ni_(3)Fe oxide and PANI support enhances the Ni–O covalency via the interfacial Ni–N bond,thus promoting the charge and mass transfer on Ni_(3)Fe *** the excellent activity and stability,rechargeable Zn-air batteries with optimum Ni_(3)Fe oxide/PANI are assembled,delivering a low charge voltage of 1.95 V to cycle for 400 h at 10 mA cm^(-2).The regulation of the effect of catalyst–support interaction on catalytic activity provides new possibilities for the future design of highly efficient OER catalysts.

关键词： Catalyst-support interaction Supported catalysts Heterointerface Oxygen evolution reaction Zn-air batteries

Storage time affects the level and diagnostic efficacy of plasma biomarkers for neurodegenerative diseases

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Neural Regeneration Research 2025年第8期20卷 2373-2381页

作者： Lifang Zhao Mingkai zhang Qimeng Li Xuemin Wang Jie lu Ying Han Yanning Cai Department of Clinical Biobank Xuanwu HospitalCapital Medical UniversityBeijingChina Beijing Geriatric Medical Research Center BeijingChina Department of Neurology Xuanwu HospitalCapital Medical UniversityBeijingChina Department of Radiology and Nuclear Medicine Xuanwu HospitalCapital Medical UniversityBeijingChina Beijing Key Laboratory of Magnetic Resonance Imaging and Brain Informatics BeijingChina Key Laboratory of Neurodegenerative diseases Ministry of EducationBeijingChina School of Biomedical Engineering Hainan UniversityHaikouHainan ProvinceChina Center of Alzheimer’s Disease Beijing Institute for Brain DisordersBeijingChina National Clinical Research Center for Geriatric Diseases BeijingChina Institute of Biomedical Engineering Shenzhen Bay LaboratoryGaoke Innovation CenterShenzhenGuangdong ProvinceChina Department of Neurobiology Xuanwu HospitalCapital Medical UniversityBeijingChina

Several promising plasma biomarker proteins,such as amyloid-β(Aβ),tau,neurofilament light chain,and glial fibrillary acidic protein,are widely used for the diagnosis of neurodegenerative ***,little is known about the long-term stability of these biomarker proteins in plasma samples stored at-80°*** aimed to explore how storage time would affect the diagnostic accuracy of these biomarkers using a large *** samples from 229 cognitively unimpaired individuals,encompassing healthy controls and those experiencing subjective cognitive decline,as well as 99 patients with cognitive impairment,comprising those with mild cognitive impairment and dementia,were acquired from the Sino Longitudinal Study on Cognitive Decline *** samples were stored at-80°C for up to 6 years before being used in this *** results showed that plasma levels of Aβ42,Aβ40,neurofilament light chain,and glial fibrillary acidic protein were not significantly correlated with sample storage ***,the level of total tau showed a negative correlation with sample storage ***,in individuals without cognitive impairment,plasma levels of total protein and tau phosphorylated protein threonine 181(p-tau181)also showed a negative correlation with sample storage *** was not observed in individuals with cognitive ***,we speculate that the diagnostic accuracy of plasma p-tau181 and the p-tau181 to total tau ratio may be influenced by sample storage ***,caution is advised when using these plasma biomarkers for the identification of neurodegenerative diseases,such as Alzheimer's ***,in cohort studies,it is important to consider the impact of storage time on the overall results.

关键词： Alzheimer’s disease amyloid-β diagnostic ability glial fibrillary acidic protein neurodegeneration neurofilament light chain plasma biomarkers single molecule array storage time tau