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Advances in additively manufactured titanium alloys by powder bed fusion and directed energy deposition:Microstructure,defects,and mechanical behavior

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Journal of Materials Science & Technology 2024年第16期183卷 32-62页

作者： H.Y.Ma J.C.wang P.qin Y.J.liu l.Y.Chen l.q.wang l.C.Zhang Centre for Advanced Materials and Manufacturing School of EngineeringEdith Cowan University270 Joondalup DriveJoondalupPerthWA 6027SA School of Engineering M050The University of Western Australia35 Stirling HighwayCrawleyPerthWA 6009SA Institute of Metals College of Material Science and EngineeringChangsha University of Science&TechnologyChangsha 410004China School of Material Science and Engineering Jiangsu University of Science and TechnologyZhenjiang 212100China State Key laboratory of Metal Matrix Composites School of Material Science and EngineeringShanghai Jiao Tong UniversityShanghai 200240China

Ti and its alloys have been broadly adopted across various industries owing to their outstanding proper-ties,such as high strength-to-weight ratio,excellent fatigue performance,exceptional corrosion resistance and so *** manufacturing(AM)is a complement to,rather than a replacement for,traditional manufacturing *** enhances flexibility in fabricating complex components and resolves machin-ing challenges,resulting in reduced lead times for custom ***,owing to distinctions among various AM technologies,Ti alloys fabricated by different AM methods usually present differences in mi-crostructure and defects,which can significantly influence the mechanical performance of built ***,having an in-depth knowledge of the scientific aspects of fabrication and material properties is crucial to achieving high-performance Ti alloys through different AM *** article reviews the mechanical properties of Ti alloys fabricated by two mainstream powder-type AM techniques:powder bed fusion(PBF)and directed energy deposition(DED).The review examines several key aspects,en-compassing phase formation,grain size and morphology,and defects,and provides an in-depth analysis of their influence on the mechanical behaviors of Ti *** review can aid researchers and engi-neers in selecting appropriate PBF or DED methods and optimizing their process parameters to fabricate high-performance Ti alloys for a wide range of industrial applications.

关键词： Powder bed fusion Directed energy deposition Titanium alloys Phase transformation Defects Mechanical property

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Comparison of microstructure and mechanical behavior of Ti-35Nb manufactured by laser powder bed fusion from elemental powder mixture and prealloyed powder

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Journal of Materials Science & Technology 2022年第10期105卷 1-16页

作者： J.C.wang Y.J.liu S.X.liang Y.S.Zhang l.q.wang T.B.Sercombe l.C.Zhang School of Engineering Edith Cowan University270 Joondalup DriveJoondalupPerthWA 6027Australia School of Engineering M050The University of Western Australia35 Stirling HighwayCrawleyPerthWA 6009Australia Northwest Institute for Nonferrous Metal Research Xi’an 710016China State Key laboratory of Metal Matrix Composites School of Material Science and EngineeringShanghai Jiao Tong UniversityShanghai 200240China

Although different types of powder feedstock are used for additive manufacturing via laser powder bed fusion(l-PBF),limited work has attempted to directly compare the microstructure and mechanical behavior of components manufactured from those powder *** work investigated the microstructure,phase composition,melt pool morphology,and mechanical properties of a prealloyed Ti-35Nb alloy manufactured using l-PBF and compared these to their counterparts produced from elemental powder *** samples manufactured from the powder mixture are composed of randomly distributed undissolved Nb in theα/βmatrix,resulting from the unstable melt pool during the melting of the powder *** contrast,parts produced from prealloyed powder display a homogeneous microstructure withβandαphases,owing to the full melting of prealloyed powder,therefore,a more stable melt pool to achieve a homogeneous *** Ti-35Nb manufactured from prealloyed powder exhibits large tensile ductility(about 10 times that of the counterparts using mixed powder),attributed to the high homogeneity in microstructure and chemical composition,strong interface bonding,relatively low oxygen content,and the existence of a large amount ofβ*** work sheds insights into understanding the effect of powder feedstock on the melt pool stability therefore the microstructure and mechanical behavior of the resultant parts.

关键词： Titanium-niobium Powder bed fusion Additive manufacturing Melt pool stability Microstructure Mechanical properties

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Establishment of Direct Plant Regeneration System from Petiole Explants of Swainsona salsula Taubert

Establishment of Direct Plant Regeneration System from Petio...

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2009中国植物学会植物细胞生物学学术年会

作者： G.D.Chen,J.Yang~*,l.q.wang,H.liu,S.Shen,F.qin College of life Sciences,China West Normal University,Nanchong,Sichuan 637009, P.R.China

Swainsona salsula Taubert is a traditional medicinal herb in China,belonging to the family of *** effective protocol was developed for plant regeneration from petioles explants of Swainsona salsula Taubert by overall ... 详细信息

关键词： Swainsona salsula Taubert Plant Regeneration System Petiole explants Vitrification

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EFFECT OF ElECTROlESS DEPOSITION CONDITIONS ON THE STRUCTURES AND THE MAGNETIC PERFORMANCES OF THE Co-Fe-P AllOY

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Acta Metallurgica Sinica(English letters) 2006年第4期19卷 307-312页

作者： S.l. wang F.q. Zeng Department of Applied Chemistry College of Materials Science and Engineering Huaqiao University Quanzhou 362021 China

Electroless Co-Fe-P alloys were deposited from an alkaline bath, containing boric acid as a buffer agent and sodium citrate as a complexing agent. As a result, with the increase of pH of the bath, the iron content of the deposit increased, whereas the cobalt and phosphorus contents decreased. The structure of the deposit was investigated using X-ray diffraction （XRD） and transmission electron microscope （TEM）. The deposit consisted of hexahedron phase Co, cubic phase Fe-Co, and amorphous phase （crystalline）. The magnetic performances of the deposit were studied using vibrating sample magnetometer （VSM）. The more the content of Fe and the less the content of P （the content of Co being less）, the better the magnetic performances of the deposit. The Co-Fe-P deposit was suitable for use as soft magnetic material.

关键词： electroless deposition Co-Fe-P structure magnetic performance

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Influence of Fe Addition on Products of Self-Propagating High-Temperature Synthesis Reaction in 3Ti-Si-2C System

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稀有金属材料与工程 2009年第A03期38卷 113-118页

作者： Guan q l wang H Y li S l Si W P Jiang q C Key laboratory of Automobile Materials of Ministry of Education Jilin University Changchun 130025 China

Influence of Fe addition on products of self-propagating high-temperature synthesis (SHS) reaction in 3Ti-Si-2C system was investigated in the present study. Without Fe addition, Ti5Si3 and TiC are the dominant phases along with a small amount of Ti3SiC2 phase and unreacted C left in the final products. As Fe content ranges from 10% to 30%, the products consist of TiC, Ti5Si3, Fe2Ti and unreacted C, but no trace of Ti3SiC2 phase is detected. Furthermore, the amounts of both Fe2Ti and C phases increase with Fe content increasing. Addition of Fe has a great effect on the reaction route and significantly restrains the formation of Ti3SiC2 during the combustion synthesis process, and therefore, the SHS is not an effective fabrication technique to synthesize the ternary Ti3SiC2 ceramic in either 3Ti-Si-2C or Fe-3Ti-Si-2C system. Besides, without Fe addition, Ti5Si3 presents as the coarse irregular appearance with an obviously sintered morphology. In contrast, the shape of Ti5Si3 exhibits more and more spherical (cobblestone-like) and the surface becomes increasingly smooth, because the amount of liquids formed during the SHS reaction increases with the increase of Fe content. On the other hand, with Fe content increasing from 0 to 30 wt.%, the particulate size of TiC decreases from more than 5 μm to 1 μm or less, mainly due to the fact that the combustion temperature decreases with the increase of Fe content in the preforms.

关键词：复合材料铁含量燃烧过程物理性能

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Snap-through of an elastica under bilateral displacement control at a material point

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Acta Mechanica Sinica 2020年第3期36卷 727-734页

作者： q.wang H.l.Zou Z.C.Deng Department of Engineering Mechanics Northwestern Polytechnical UniversityXi'an 710072China

Snap-through phenomenon widely occurs for elastic systems,where the systems lose stability at critical *** snapthrough of an elastica under bilateral displacement control at a material point is studied,by regarding the whole elastica as two components,i.e.,pinned-clamped ***,stiffness-curvature curves of two pinned-clamped elasticas are firstly efficiently located based on the second-order mode,which are used to determine the shapes of two *** transformations are used to assemble two components together to form the whole elastica,which reveals four kinds of *** advantage of this way compared with other methods such as the shooting method is that multiple coexisting solutions can be located accurately.O n the load-deflection curves,four branches correspond to four kinds of shapes and first two branches are symmetrical to the last two branches relative to the original *** the bilateral displacement control,the critical points can only appear at saddle-node bifurcations,which is different to that for the unilateral displacement ***,one critical point is found on the first branch and two critical points are found on the secondary *** addition,the snap-through among different branches can be well explained with these critical points.

关键词： Elastica Snap-through Critical points Buckling Displacement control

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[Recent progress in mass spectrometry imaging using nanospray desorption electrospray ionization]

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Se pu = Chinese journal of chromatography 2025年第1期43卷 43-49页

作者： Jing-Bo wang Xiao-lan li Rui-Xia Fan Ping lü Rui-Chuan Yin West China School of Pharmacy Sichuan University Chengdu 610041 China.

Ambient mass spectrometry imaging (MSI) enables hundreds of analytes in tissue sections to be directly mapped at atmospheric pressure with minimal sample preparation. This field is currently experiencing rapid growth, with numerous reported ambient ionization techniques resulting in a "hundred flowers bloom" situation. Nanospray desorption electrospray ionization (nano-DESI), developed by the laskin group in 2010, is a widely used liquid-extraction-based ambient ionization technique that was first used for mass spectrometry imaging of tissue in 2012. The nano-DESI probe comprises a primary capillary and a nanospray capillary, with the latter efficiently transferring analyte-containing droplets via a tiny liquid bridge formed between the probe and sample surface, thereby enabling nanoelectrospray ionization (nano-ESI) in front of the inlet of a mass spectrometer. The advantages of nano-DESI MSI include minimal sample preparation, high spatial resolution, and high sensitivity. These features are well-suited for imaging various sample types, including frozen tissue sections, microbial communities, and environmental samples. A PubMed-database search using the "nano-DESI" keyword revealed 72 related articles in the 2010-2024 period, with 34 of them published between 2021 and 2024, which indicates that nano-DESI has rapidly developed as an ambient ionization technique over recent years. Herein, we briefly introduce key nano-DESI-MSI research progress reported in the past three years with the aim of better understanding and facilitating the use of this technology. We first discuss advances in ion-source development. Since no commercial nano-DESI source exists, designing and constructing ion sources remain technical challenges that limit its development. Nano-DESI has been successfully coupled with various types of mass spectrometer, including lTq Orbitrap, quadrupole-Orbitrap (q Exactive), 6560 IM qTOF, timsTOF Pro2, triple quadrupole, and FTICR. These couplings have signi

关键词： ambient mass spectrometry imaging nanospray desorption electrospray ionization spatial proteomics structural characterization of lipid

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Effects of Current Stressing on Shear Properties of Sn-3.8Ag-0.7Cu Solder Joints

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Journal of Materials Science & Technology 2010年第8期26卷 737-742页

作者： X.J. wang q.l. Zeng q.S. Zhu Z.G. wang J.K. Shang Shenyang National laboratory for Materials Science Institute of Metal Research Chinese Academy of Sciences Shenyang 110016 China Department of Materials Science and Engineering University of Illinois at Urbana-Champaign Urbana IL 61801 USA

Effects of electromigration on microstructure, shear strength, and fracture behavior of solder joints were investigated by single-ball shear samples of eutectic Sn-3.8Ag-0.7Cu （SAC） joined by Cu plates at two sides. The electromigration tests were conducted at a current density of about 1.1×10^3 A/cm2 and a working temperature of about 83℃. The results showed that the shear strength and flow stress decreased greatly after current stressing. Such a decrease was associated with no significant loss of the fracture strain at short electromigration but a great reduction in the fracture strain after long-term current stressing. The variation of the fracture strain with the electromigration time was shown to result from the shift of the fracture surface from the center of the solder towards the intermetallic compound （IMC） interface at the cathode.

关键词： Strength Fracture strain Voids Solder

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Evolution of the Microstructure and Strength in the Nugget Zone of Friction Stir Welded SiCp/Al-Cu-Mg Composite

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Journal of Materials Science & Technology 2014年第1期30卷 54-60页

作者： D.wang B.l.Xiao q.Z.wang Z.Y.Ma Shenyang National laboratory for Materials Science Institute of Metal ResearchChinese Academy of Sciences University of Science and Technology of China

A 6 mm-thick SiCp/2009AI composite plate was successfully joined by friction stir welding （FSW） using an ultrahard material tool to investigate the evolution of the microstructure and the strength in the nugget zone （NZ）. While some SiC particles were broken up during FSW, most of them rotated in the matrix. large compound particles on the interfaces were broken off during FSW, whereas the amorphous layer and small compound particles remained on the interfaces. The dynamically recrystallized AI grains nucleated on the surface of fractured SiC particles during FSW, forming nano-sized grains around the SiC particles. The yield strength of the NZ decreased slightly due to the variation in the size, shape, and distribution of the SiC particles. The clean interfaces were beneficial to the load transfer between SiC particles and AI matrix and then increased the ultimate tensile strength of the NZ.

关键词： Metal-matrix composites Friction stir welding Microstructure Mechanical properties

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EXPERIMENTAl RESEARCH AND NUMERICAl SIMUlATION OF lASER SHOCK FORMING OF TA2 TITANIUM SHEET

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Acta Metallurgica Sinica(English letters) 2006年第5期19卷 347-354页

作者： F. wang Z. q. Yao J. Hu q.l. Deng School of Mechanical Engineering Shanghai Jiao Tong UniversityShanghai 200030 China

laser shock forming （ISF） was a new technique realized by applying an impulsive pressure generated by laser-induced shock wave on the surface of metal sheet. lSF of metal sheet was investigated with experiments and numerical simulation. The basic theories were introduced; the surface quality and deformation of the processed titanium sample （TA2） were examined; ABAqUS was used to simulate ISF and the central displacement of the shocked region was measured and compared with the simulation. Overlapped ISF treatment was experimentally carried out to produce groove and simulation. The results showed that the surface quality and the microstructure with single laser pulse had no remarkable change, and ablation was observed on the surface of the sample with overlapped pulses. The deformation observed in the numerical simulation agreeed with that observed in the experimental measurement quite well.

关键词： laser shock forming numerical simulation surface quality deformation

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