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Denaturation behavior of inclusions in industrial pure iron by calcium treatment

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Journal of Iron and Steel Research International 2023年第2期30卷 249-258页

作者： Xin Liu Yan-ping Bao Cheng-jian hua jian-hua Chu Chao Gu Min Wang State Key Lab of Advanced Metallurgy University of Science and Technology BeijingBeijing100083China

Only a few Chinese enterprises can produce high-quality industrial pure iron,and studies on the smelting process of industrial pure iron were *** inclusions in a melting process were characterized by means of electron microscopy and an automatic inclusion analysis system,and the evolution mechanism of inclusion was studied using thermodynamic calculation to optimize the calcium alloy addition in liquid *** results show that during the smelting process,inclusions mainly composed of Al_(2)O_(3)and spinel are formed before calcium *** calcium treatment,they continuously react with[Ca],[S]and[Ti],grow up,and are removed during refining and tundish *** the end,there are more small-sized inclusions containing CaS,and the contents of Al_(2)O_(3)and spinel are *** to thermodynamic calculations,the appropriate calcium treatment liquid window for the molten steel composition is(10-38)×10^(-6).Calcium treatment has changed the main types of inclusions in industrial pure iron from Al_(2)O_(3)to small-sized inclusions containing CaS and effectively reduces the influence of Al_(2)O_(3)inclusions on the quality of industrial pure iron.

关键词： Industrial pure iron Calcium treatment Inclusion Thermodynamic CaS

Transient stochastic response of quasi integerable Hamiltonian systems

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Acta Mechanica Sinica 2013年第4期29卷 602-611页

作者： Zhong-hua Liu jian-hua Geng Wei-Qiu Zhu Department of Civil Engineering Xiamen University Department of Mechanics State Key Laboratory of Fluid Power Transmission and Control Zhejiang University

The approximate transient response of quasi in- tegrable Hamiltonian systems under Gaussian white noise excitations is investigated. First, the averaged It6 equa- tions for independent motion integrals and the associated Fokker-Planck-Kolmogorov （FPK） equation governing the transient probability density of independent motion integrals of the system are derived by applying the stochastic averag- ing method for quasi integrable Hamiltonian systems. Then, approximate solution of the transient probability density of independent motion integrals is obtained by applying the Galerkin method to solve the FPK equation. The approxi- mate transient solution is expressed as a series in terms of properly selected base functions with time-dependent coeffi- cients. The transient probability densities of displacements and velocities can be derived from that of independent mo- tion integrals. Three examples are given to illustrate the ap- plication of the proposed procedure. It is shown that the re- suits for the three examples obtained by using the proposed procedure agree well with those from Monte Carlo simula- tion of the original systems.

关键词： Transient response ~ Stochastic averagingmethod ~ Galerkin method ~ Quasi integrable Hamiltoniansystem

On Boolean elements and derivations in 2-dimension linguistic lattice implication algebras

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Applied Mathematics(A Journal of Chinese Universities) 2023年第2期38卷 274-292页

作者： ZHU hua ZHAO jian-bin School of Mathematics and Statistics Zhengzhou UniversityZhengzhou 450001China Henan Academy of Big Data Zhengzhou UniversityZhengzhou 450001China Henan Key Laboratory of Financial Engineering Zhengzhou 450001China Key Laboratory of Big Data Analysis and Application Zhengzhou 450001China

A 2-dimension linguistic lattice implication algebra(2DL-LIA)can build a bridge between logical algebra and 2-dimension fuzzy linguistic *** this paper,the notion of a Boolean element is proposed in a 2DL-LIA and some properties of Boolean elements are *** derivations on 2DL-LIAs are introduced and the related properties of derivations are ***,it proves that the derivations on 2DL-LIAs can be constructed by Boolean elements.

关键词： derivation Boolean element Lattice implication algebra(LIA) 2-dimension linguistic lattice implication algebra(2DL-LIA) 2-dimension fuzzy linguistic information

基于深度学习的基础设施表面裂纹检测方法研究进展

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计算机工程与应用 2025年第1期61卷 1-23页

作者：胡翔坤李华冯毅雄钱松荣李键李少波贵州大学公共大数据国家重点实验室贵阳550025 清华大学机械工程系北京100084 浙江大学流体动力基础件与机电系统全国重点实验室杭州310058

民用基础设施在长期使用后容易发生物理结构或性能状态的改变,对其功能和使用安全造成一定的损害,因此,对这类设施的结构健康监测是十分必要的。裂纹检测是结构健康监测中极其重要的一部分,及时检测并识别这类损伤,能有效避免事故的发... 详细信息

民用基础设施在长期使用后容易发生物理结构或性能状态的改变,对其功能和使用安全造成一定的损害,因此,对这类设施的结构健康监测是十分必要的。裂纹检测是结构健康监测中极其重要的一部分,及时检测并识别这类损伤,能有效避免事故的发生。基于计算机视觉的表面裂纹检测方法操作简单、检测速度快、准确率高,被广泛应用于民用基础设施的表面裂纹检测。从图像分类、目标检测、语义分割三个不同的检测方向综述了基于深度学习的基础设施表面裂纹检测方法,总结了常见的数据采集方法和常用的公共裂纹数据集。最后讨论了基于深度学习的基础设施表面裂纹检测方法存在的困难与挑战,并展望了未来可能的发展方向。

关键词：结构健康监测裂纹检测计算机视觉深度学习

基于反应气混合物的ICP-MS/MS测定原油中的钒和镍

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光谱学与光谱分析 2025年第1期45卷 101-106页

作者：蔡松韬黄莹秀袁亮代宇宣莫垚坤黄建华湖南工学院材料科学与工程学院湖南衡阳421002 湖南省中医药研究院中药研究所湖南长沙410013

原油中金属元素钒和镍(V和Ni)的含量和比值可为深入了解原油的沉积环境特征和有机质类型发挥重要作用。在原油炼制过程中,V和Ni作为原油催化裂化过程中的有害金属元素,会降低催化剂的活性,严重时会导致催化剂中毒,会严重腐蚀设备,在精... 详细信息

原油中金属元素钒和镍(V和Ni)的含量和比值可为深入了解原油的沉积环境特征和有机质类型发挥重要作用。在原油炼制过程中,V和Ni作为原油催化裂化过程中的有害金属元素,会降低催化剂的活性,严重时会导致催化剂中毒,会严重腐蚀设备,在精炼之前必须对原油中的V和Ni进行脱除处理。V和Ni具有致突变性和致癌性,识别或监测原油中V和Ni进入环境的潜在危险变得越来越重要,对原油中V和Ni的含量进行高灵敏精准测定具有重要意义。采用电感耦合等离子体串联质谱(ICP-MS/MS)测定原油中V和Ni的新策略。原油样品经航空煤油简单稀释后直接采用ICP-MS/MS进行分析,针对V和Ni受到的质谱干扰,在MS/MS模式下,采用由NH_(3)/He(He为缓冲气)和H_(2)组成的反应气混合物(NH_(3)/He/H_(2))作为反应气,基于V^(+)与NH_(3)/He/H_(2)不发生反应,而V^(+)的干扰离子与NH_(3)/He/H_(2)发生反应,采用原位质量法消除干扰,选择V^(+)进行测定;基于Ni^(+)与NH_(3)/He/H_(2)发生反应,采用质量转移法消除干扰,选择无干扰团簇离子Ni(NH_(3))_(3)^(+)进行测定。通过与NH_(3)/He反应模式进行对比研究发现,对于V的测定,加入H_(2)为反应气能快速去除氩基离子的干扰,并能协同NH_(3)消除氧化物离子的干扰;对于Ni的测定,加入H_(2)为反应气能促进全氢加合物(-NH_(3))的形成,从而提高生成Ni(NH_(3))_(3)^(+)的产率。在NH_(3)/He/H_(2)反应模式下,V和Ni的背景等效浓度(BEC)更低,Ni的灵敏度更高,V和Ni的检出限(LOD)分别低至0.83和3.76 ng·kg^(-1),定量限(LOQ)分别为2.77和12.5 ng·kg^(-1)。通过分析标准参考物质NIST SRM 1634c并进行加标回收实验评价方法的准确度和精密度,结果显示,方法的测定结果与标准参考物质的认证值基本一致,V和Ni的加标回收率分别为97.7%和103%,相对标准偏差(RSD)分别为1.8%和1.9%。所建立的分析方法避免了繁琐的样品预处理过程,具有操作简单快速、灵敏度高、准确度和精密度好的特点,适用于原油中V和Ni的检测,能为原油深加工中V和Ni的脱除提供理论依据。

关键词：原油电感耦合等离子体串联质谱钒(V) 镍(Ni) 氨气/氦气/氢气(NH_(3)/He/H_(2))

Efficient AcrH2 Catalyzed β-Trifluoromethylation of Carbonyl Compounds by Atom Transfer Radical Addition Reactions

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Chinese Journal of Chemistry 2019年第10期37卷 1025-1030页

作者： Zi-Peng rao Yu-Yang Sun Xin-Feng Zhou Qiang Xie Hui-Xia Zhu jian-Jun Dai Jun Xu hua-jian Xu School of Food and Biological Engineering Hefei University of TechnologyHefeiAnhui 230009China PET-CT Center The First Affiliated Hospital of USTCHefeiAnhui 230001China

The use of organic catalysis AcrH2 enables the direct β-trifluoromethylation of carbonyl compounds by atom transfer radical addition reactions with broad substrate scopes under mild *** operationally simple and robust protocol successfully converts a variety of β-chloro carbonyl compounds into the corresponding α-chloro-β-fluoroalkylcarbonyl products.A significant advantage of this method is that it does not require the use of a metal catalyst,thereby avoiding metal residue problems in drug synthesis.

关键词： synthesis. conditions. carbonyl

System optimization-oriented spare parts dynamic configuration model for multi-echelon multi-indenture system

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Journal of Systems Engineering and Electronics 2017年第5期28卷 923-933页

作者： Minzhi Ruan hua Li jian Fu Office of Research & Development Naval University of Engineering Department of Weaponry Engineering Naval University of Engineering

In order to optimize the spares configuration project at different stages during the life cycle, the factor of time is considered to relax the assumption of the spares steady demand in multi-echelon technique for recoverable item control (METRIC) theory. According to the method of systems analysis, the dynamic palm theorem is introduced to establish the prediction model of the spares demand rate, and its main influence factors are analyzed, based on which, the spares support effectiveness evaluation index system is studied, and the system optimization-oriented spares dynamic configuration method for multi-echelon multi-indenture system is proposed. Through the analysis of the optimization algorithm, the layered marginal algorithm is designed to improve the model calculation efficiency. In a given example, the multi-stage spares configuration project during its life cycle is gotten, the research result conforms to the actual status, and it can provide a new way for the spares dynamic optimization.

关键词： system optimization spare parts dynamic demand support effectiveness multi-echelon multi-indenture layered marginal algorithm

Nanoparticle nucleation and coagulation in a mixing layer

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Acta Mechanica Sinica 2010年第4期26卷 521-529页

作者： jian-Zhong Lin Yan-hua Liu China Jiliang University 310018 Hangzhou China Department of Mechanics Zhejiang University310027 Hangzhou China

Numerical simulation of nanoparticle nucleation and coagulation in a mixing layer with sulfuric acid vapor binary system is performed using the large eddy simulation and the direct quadrature method of moment. The distributions of number concentration, volume concentration, and average diameter of nanoparticles are obtained. The results show that the coherent structures have an important effect on the distributions of number concentration, volume concentration and average diameter of nanoparticles via continuously transporting and diffusing the nanoparticles to the area of low particle concentration. In the streamwise direction, the number concentration of nanoparticles decreases, while the volume concentration and the average diameter increase. The distributions of number concentration, volume concentration and average diameter of nanoparticles are spatially inhomogeneous. The characteristic time of nucleation is shorter than that of coagulation. The nucleation takes place more easily in the area of low temperature because where the number concentration of nanoparticles is high, while the intensity of coagulation is mainly affected by the number concentration. Both nucleation and coagulation result in the variation of average diameter of nanoparticles.

关键词： Nanoparticles Nucleation - Coagulation Mixing layer Direct quadrature method of moment

丹酚酸B介导Elovl6/Echs1/Acot1通路调节脂肪酸代谢减轻H9c2细胞OGD/R损伤

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中国药理学通报 2025年第3期41卷 482-490页

作者：曹策宋鉴书杨丽丽李浩然刘子馨李磊付建华刘建勋中国中医科学院西苑医院基础医学研究所中药药理北京市重点实验室国家中医心血管疾病临床医学研究中心北京100091

目的观察丹酚酸B(salvianolic acid B,SalB)抗H9c2细胞氧糖剥夺/再复(oxygen glucose deprivation/re-oxygenation,OGD/R)损伤机制。方法CCK-8筛选SalB对OGD/R损伤H9c2细胞保护浓度;试剂盒检测SalB对乳酸脱氢酶(lactate dehydrogenase,LDH)、天冬氨酸转氨酶(aspartate transaminase,AST)、肌酸激酶(creatine kinase,CK)的影响;转录组测序探索SalB对OGD/R损伤H9c2作用机制;分子对接检测SalB和差异蛋白结合情况;ELISA法检测脂肪酸含量;RT-qPCR和Western blot验证差异基因表达水平;孟德尔随机化验证SalB作用靶点与HF因果关系。结果与模型组相比,SalB可保护OGD/R损伤后H9c2细胞,且明显降低CK、LDH和AST含量;转录组筛选差异基因100个,涉及脂肪酸延长、癌症中心碳代谢、色氨酸代谢通路;分子对接显示SalB与差异蛋白具有良好结合能;核心基因Elovl6、Echs1、Acot1 mRNA和蛋白表达与转录组一致;SalB可降低OGD/R损伤后脂肪酸含量;孟德尔随机化表明SalB可调节脂肪酸代谢,降低HF风险。结论 SalB下调Elovl6、Echs1、Acot1表达水平,通过脂肪酸代谢通路保护OGD/R损伤后H9c2细胞。

关键词：丹酚酸B 转录组高通量测序 H9c2心肌细胞 OGD/R 缺血/再灌注损伤脂肪酸代谢