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Optimisation of zeolite LTA synthesis from alum sludge and the influence of the sludge source

Journal of Environmental Sciences 2021年第1期33卷 130-142页

作者： Alexandra Rozhkovskaya jay rajapakse Graeme J.Millar School of Civil and Enuironmental Engineering Science and Engineering FacultyQueensland University oTechnologyBrisbaneQueensland 4000Australia Institute for Future Environments and School of Mechanical Medical and Process EngineeringQueensland Uniuersity of TechnologyBrisbaneQueensland 4000Australia

Generation of alum sludge(AS)at drinking water treatment plants represents an environmental liability and adds to the cost of water ***,this study explored the feasibility of using low and high carbon containing alum sludge from two water treatment plants to synthesize zeolite *** hypothesis was that zeolite LTA synthesis was dependant upon alum sludge source and that a range of strategies may be required to optimize zeolite *** characteristics such as morphology,phase composition,crystallinity,and particle size distribution were recorded."One pot"hydrothermal synthesis of precursor gel with molar composition 4.2 Na2O:Al2O3:1.2 SiO_(2):168 H2O at 80℃ for 3 hr resulted in 25 and 46 wt.%zeolite LTA from high and low carbonaceous sludge,*** to hydrothermal reaction stage it was discovered that ageing of the gel,addition of zeolite LTA seeds,ultrasonic treatment and calcination all promoted zeolite LTA *** of the alum sludge at 700℃ for 2 hr before hydrothermal synthesis resulted in particle size reduction and the highest amount of crystalline zeolite LTA:79 wt.%from low carbon sludge and 65 wt.%from high carbon ***,the zeolite crystallinity reported in this study was the higher than previous studies on this *** outlined approach may allow value adding of alum waste and produce a commodity which could be used locally by the water treatment plant as a water softener.

关键词： Alum sludge Zeolite LTA Ultrasonic Ageing Waste conversion

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Effect of struvite and organic acids on immobilization of copper and zinc in contaminated bio-retention filter media

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Journal of Environmental Sciences 2020年第11期32卷 35-44页

作者： Chathurani Moragaspitiya jay rajapakse Graeme J.Millar Science and Engineering Faculty Queensland University of Technology(QUT)Queensland 4000Australia

Few studies have been carried out to connect nutrient recovery as struvite from wastewater and sustainable utilization of the recovered struvite for copper and zinc immobilization in contaminated *** study revealed the effect of struvite on Cu and Zn immobilization in contaminated bio-retention soil in the presence of commonly exuded plant organic *** research hypothesis was that the presence of both struvite and organic acids may influence the immobilization of Cu and Zn in *** outcome of this research confirmed that more than 99%of Cu and Zn was immobilized in bio-retention filter media by struvite ***-soluble Cu and Zn concentrations of struvite treated soil were less than 1.83 and 0.86 mg/kg respectively,and these concentrations were significantly lower compared to the total Cu and Zn content of 747.05 mg/kg in the contaminated *** of struvite to Cu-and Zn-contaminated soil resulted in formation of compounds similar to zinc phosphate tetrahydrate(Zn3(PO4)2·4H2O)and amorphous Cu and Zn *** was effective in heavy metal remediation in acidic soil regardless of the presence of Ca impurities in struvite and the presence of plant organic acids in ***,this study revealed that struvite recovered from wastewater treatment plants has potential for use as an amendment for heavy metal remediation in contaminated bio-retention soil.

关键词： Immobilization Struvite Organic acids Heavy metal Contaminated soil Bio-retention

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维普期刊数据库

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Effect of Ca:Mg ratio and high ammoniacal nitrogen on characteristics of struvite precipitated from waste activated sludge digester effluent

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Journal of Environmental Sciences 2019年第12期31卷 65-77页

作者： Chathurani Moragaspitiya jay rajapakse Graeme J.Millar Science and Engineering Faculty Queensland University of Technology (QUT)

This study revealed the relationship between the presence of calcium impurities and ammoniacal nitrogen concentration upon crystallization of *** research hypothesis was that the presence of both calcium and high concentrations of ammoniacal nitrogen(328–1000 mg/L)in waste activated sludge may influence the struvite quality and acid ***,we studied the impact of Ca:Mg ratio upon morphology,particle size,purity and dissolution of struvite,in the presence of varying levels of excess ammoniacal nitrogen.X-ray diffraction revealed that up to 31.4%amorphous material was made which was assigned to *** the ammoniacal nitrogen concentration and elevation of the Mg:Ca ratio maximized the presence of *** particle size was also increased by ammoniacal nitrogen as was twinning of the *** with dilute solutions of organic acid revealed the sensitivity of struvite dissolution to the physical characteristics of the *** particles(21.2μm)dissolved at higher rates than larger particles(35.86μm).However,struvite dissolved rapidly as the p H was further reduced irrespective of the physical ***,addition of struvite to low p H soils was not viewed as beneficial in terms of controlled nutrient ***,this study revealed that waste activated sludge effluent with high ammoniacal nitrogen was prospective for synthesis of high quality struvite material.

关键词： Struvite Purity Calcium Ammoniacal nitrogen Waste activated sludge

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维普期刊数据库

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