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Acta Metallurgica Sinica(English Letters) 2024年第2期37卷 308-324页

作者： Gang Niu Rui Yuan R.D.K.Misra Na Gong Zhi-hui Zhang Hao-Xiu Chen hui-bin wu Cheng-Jia Shang Xin-Ping Mao Collaborative Innovation Center of Steel Technology University of Science and Technology BeijingBeijing100083China Laboratory for Excellence in Advanced Steel Research Department of MetallurgicalMaterials and Biomedical EngineeringUniversity of Texas at El PasoEl PasoTX79968USA Institute of Materials Research and Engineering Agency for ScienceTechnologyand ResearchSingapore138634Singapore Department of Materials Science and Engineering University of TorontoTorontoONM5S 3E4Canada

The corrosion behavior and mechanism of 3Ni weathering steel in a simulated oceanic atmospheric environment are investigated in order to comprehend the impacts of La,as determined through electrochemical analysis and rust layer *** results of this study demonstrate that the addition of La enhances the corrosion resistance of 3Ni weathering steel in the marine atmospheric environment,thereby reducing the corrosion rate and improving the protection of the rust *** influence of La on corrosion resistance can be attributed to two primary ***,La functions as a grain refiner,minimizing the potential difference of the micro-regions on the substrate surface,thereby significantly reducing the corrosion of bare steel in the marine ***,La inhibits the process of Fe_(3)O_(4) oxidation back toγ-FeOOH during corrosion at the local site,thus decreasing the formation ofγ-FeOOH and enhancing the charge transfer *** research work may serve as a reference for expanding the application of rare earth elements in the field of weathering steel.

关键词： Weathering steel Rare earth Rust layer Corrosion behavior Corrosion resistance

Characteristics of SEN clogging and adhesive behavior of oxide inclusion during continuous casting of Ti-stabilized ultra-pure ferritic stainless steels

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Journal of Iron and Steel Research International 2023年第10期30卷 1939-1951页

作者： Xue-feng Bai Yan-hui Sun hui-bin wu Collaborative Innovation Center of Steel Technology University of Science and Technology BeijingBeijing100083China

Submerged entry nozzle(SEN)clogging during continuous casting of Ti-stabilized ultra-pure ferritic stainless(Ti-UPFS)steels was systematically investigated via cross-sectional analysis and acid dissolution *** SEN deposit profile was characterized as occurring in three major layers:(1)an eroded refractory layer;(2)an initial adhesive layer comprised an Al_(2)O_(3)-ZrO_(2) composite sub-layer and a dense Al_(2)O_(3)-based deposit sub-layer;and(3)a porous multiphase deposit layer mainly consisting of MgO·Al_(2)O_(3),CaO-Al_(2)O_(3),and *** MgO·Al_(2)O_(3)-rich inclusions did not adhere directly to the eroded refractory but were entrapped during the deposit *** of inclusion characterization in the tundish revealed that the MgO·Al2O3-rich particles present in the tundish served as the primary source of clogging ***,a novel cavity-induced adhesion model by circular approximation was established to explain the effects of complex inclusion characteristics and refractory material type on adhesion force.A high number of small MgO·Al_(2)O_(3) inclusions were expected to accelerate the buildup of clogging *** the modification of MgO·Al_(2)O_(3)-rich inclusions in the size range of 2-4μm by Ca treatment was crucial to minimizing the risk of SEN clogging during the continuous casting of Ti-UPFS steels.

关键词： Ti-stabilized ultra-pure ferritic stainless steel Submerged entry nozzle clogging MgO·Al_(2)O_(3)-rich inclusion Adhesion Continuous casting

Precipitation and stability of reversed austenite in 9Ni steel

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International Journal of Minerals,Metallurgy and Materials 2010年第5期17卷 587-595页

作者： Yue-hui Yang Qing-wu Cai Di Tang hui-bin wu Research Institute of Metallurgical Engineering University of Science and Technology Beijing Beijing 100083 China

A new method was used to analyze the factors affecting the precipitation of reversed austenite during tempering. The samples were kept at various tempering temperatures for 10 min and their length changes were recorded. Then, the precipitation of reversed austenite which led to the length reduction was shown by thermal expansion curves. The results show that the effects of process parameters on the precipitation of reversed austenite can be determined more accurately by this method than by X-ray diffraction. When the quenching and tempering process is adopted, both the lower quenching temperature and higher tempering temperature can promote the precipitation of reversed austenite during tempering; and when the quenching, lamellarizing, and tempering process is used, intercritical quenching is considered beneficial to the precipitation of reversed austenite in the subsequent tempering because of Ni segregation during holding at the intercritical temperature.

关键词： cryogenic equipment low carbon steel reversed austenite precipitation stability thermal expansion measurement

Influence of Mo on Growth and Coarsening of Nanometer-sized Carbides in Low-alloy Ferritic Steels Containing Ti

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Journal of Iron and Steel Research International 2014年第9期21卷 878-885页

作者： bin-hao HU Qing-wu CAI hui-bin wu Engineering Research Institute University of Science and Technology Beijing

By optical microscopy, transmission electron microscopy and energy dispersive spectroscopy, the changes with aging time in size, composition and distribution of nanometer-sized （Ti, Mo）C precipitated in Ti-Mo low-alloy ferritc steel have been studied in comparison with that of nanometer-sized TiC precipitated in Ti low-alloy ferritc steel. It was found that the growth rate of （Ti,Mo）C in Ti-Mo steel was less than that of TiC in Ti steel. Nanometer- sized carbides formed at 650 ~C （or 550 ~C） for 55 h were at transitional stage from growth to coarsening. When aging time reaches 55 h, the coarsening rates of nanometer-sized carbides in Ti and Ti-Mo steel tend to be the same and in- variable. The influence of Mo on growth and coarsening of nanometer-sized carbides tends to decrease with increasing aging time, and Mo contents in nanometer-sized carbides with the same size at different aging time were different.

关键词： Ti-Mo low alloy ferritic steel nanometer-sized carbide precipitation strengthening Ostwald coarsening

Effect of cooling rate on microstructure, hardness, and residual stress of 0.28C-0.22Ti wear-resistant steel

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Journal of Iron and Steel Research International 2019年第8期26卷 866-874页

作者： Chen Dong hui-bin wu Xi-tao Wang Collaborative Innovation Center of Steel Technology University of Science and Technology Beijing Beijing 100083 China

The microstructure, hardness, and residual stress of 0.28C-0.22Ti wear-resistant steel produced with cooling rates varying from 80.0 to 0.3℃/s were determined using a dilatometer, scanning electron microscope, Vickers hardness tester, and nanoindentation tester. The results showed that the hardness of martensite decreased at a rate of approximately 0.935 HV/s with carbon diffusion time (the cooldown time required to transition from Ar3, 635-100℃). The range of the residual stress caused by the hard particles decreased with decreasing cooling rate, from - 400-300 MPa (cooling rate 40℃/s) to - 200-100 MPa (cooling rate 0.5℃/s), proving that the TiC particles significantly contributed to the residual stress in the high-titanium steels.

关键词： Cooling rate Microstructure Hardness TiC particle Residual stress

Reverse-transformation austenite structure control with micro/nanometer size

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International Journal of Minerals,Metallurgy and Materials 2017年第5期24卷 530-537页

作者： hui-bin wu Gang Niu Feng-juan wu Di Tang Collaborative Innovation Center of Steel Technology University of Science and Technology Beijing Beijing Engineering Technology Research Center of Special Steel for Traffic and Energy

To control the reverse-transformation austenite structure through manipulation of the micro/nanometer grain structure, the influences of cold deformation and annealing parameters on the microstructure evolution and mechanical properties of 316L austenitic stainless steel were investigated. The samples were first cold-rolled, and then samples deformed to different extents were annealed at different temperatures. The microstructure evolutions were analyzed by optical microscopy, scanning electron microscopy (SEM), magnetic measurements, and X-ray diffraction (XRD); the mechanical properties are also determined by tensile tests. The results showed that the fraction of stain-induced martensite was approximately 72% in the 90% cold-rolled steel. The micro/nanometric microstructure was obtained after reversion annealing at 820-870A degrees C for 60 s. Nearly 100% reversed austenite was obtained in samples annealed at 850A degrees C, where grains with a diameter ae 500 nm accounted for 30% and those with a diameter > 0.5 mu m accounted for 70%. The micro/nanometer-grain steel exhibited not only a high strength level (approximately 959 MPa) but also a desirable elongation of approximately 45%.

关键词： austenitic stainless steel structure control martensite reverse transformation grain refinement

Effects of Si on the stability of retained austenite and temper embrittlement of ultrahigh strength steels

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International Journal of Minerals,Metallurgy and Materials 2011年第5期18卷 543-550页

作者： Li-jun Wang Qing-wu Cai hui-bin wu Wei Yu National Engineering Research Center for Advanced Rolling Technology University of Science and Technology Beijing Beijing 100083 China

Effects of silicon （Si） content on the stability of retained austenite and temper embrittlement of ultrahigh strength steels were investigated using X-ray diffraction （XRD）,transmission electron microscopy （TEM）,and other experimental *** results show that Si can suppress temper embrittlement,improve temper resistance,and hinder the decomposition of retained *** austenite appears gradually with the increase of Si content during *** has a significant effect on enhancing carbon （C） partitioning and improving the stability of retained *** and C atoms are mutually exclusive in lath bainite,while they attract each other in austenite.ε-carbides are found in 1.8wt% Si steel tempered at 250℃,and they get coarsened obviously when tempered at 400℃,leading to temper *** ε-carbides but acicular or lath carbides lead to temper embrittlement in 0.4wt% Si steel,which can be inferred as cementites and composite *** embrittlement is closely related to the decomposition of retained austenite and the formation of reversed austenite.

关键词： silicon ultrahigh strength steel retained austenite temper embrittlement reversed austenite

Characterization of( Nb,Ti,Mo) C Precipitates in an Ultrahigh Strength Martensitic Steel

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Journal of Iron and Steel Research International 2016年第5期23卷 495-500页

作者： Biao JU hui-bin wu Di TANG Ning DANG National Engineering Research Center for Advanced Rolling Technology University of Science and Technology Beijing

A study on ultrahigh strength steel plate subjected to novel thermo-mechanical control process was presented. The mechanical properties examination showed that the investigated steel exhibited excellent combination of ultra-high strength（ 2 200 MPa） and toughness（ 26 J）. The microstructure of the experimental steel was observed by scanning electron microscope and transmission electron microscope. Desired martensitic lath with width of about 180- 250 nm was obtained. Nanostructured carbide precipitates with sizes of 20-50 nm,which contained Nb,Ti and Mo,were observed in the lath martensitic microstructure,and confirmed to be MC-type carbides with B1 structure by means of selected area electron *** compositional characteristics revealed by energy dispersive X-ray spectrometer mapping implied that the carbide forming elements Nb,Ti and Mo distributed in the precipitates evenly. Three-dimensional atom probe tomography reconstruction further indicated that Mo incorporated into the precipitates without enrichment in the carbide-matrix interface and probably substituted for Nb and Ti to form the（ Nb,Ti,Mo） C carbides.

关键词： ultrahigh strength steel precipitate (Nb Ti Mo) C compositional characteristic structural characteristic

Influence of Microstructural Evolution on the Hot Deformation Behavior of an Fe–Mn–Al Duplex Lightweight Steel

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Acta Metallurgica Sinica(English Letters) 2018年第4期31卷 389-400页

作者： Li-Xiong Xu hui-bin wu Xin-Tian Wang Collaborative Innovation Center of Steel Technology University of Science and Technology BeijingBeijing100083China National Engineering Research Center of Advanced Rolling University of Science and Technology Beijing Beijing100083China

The hot deformation behavior of Fe-26Mn-6.2A1-0.05C steel was studied by experimental hot compression tests in the temperature range of 800-1050℃ and strain rate range of 0.01-30 s-1 on a Gleeble-3500 thermal simulation *** microstructural evolution during the corresponding thermal process was observed in situ by confocal laser scanning *** backscattered diffraction and transmission electron microscopy analyses were carried out to observe the microstructural morphology before and after the hot ***,interrupted compression tests were conducted to correlate the microstructural characteristics and softening mechanisms at different deformation *** results showed that hot compression tests of this steel were all carried out on a duplex matrix composed of austenite and *** the deformation temperature increased from 800 to 1050℃,the volume fraction of austenite decreased from 70.9% to 44.0%,while that of 6-ferrite increased from 29.1% to 56.0%.Due to the different stress exponents（n）and apparent activation energies（Q）,the generated strain was mostly accommodated by δ-ferrite at the commencement of deformation,and then both dynamic recovery and dynamic recrystallization occurred earlier in δ-ferrite than in *** interaction of strain partitioning and unsynchronized softening behavior caused an abnormal hot deformation behavior profile in the Fe-Mn-A1 duplex steel,such as yield-like behavior,peculiar work-hardening behavior,and dynamic softening behavior,which are influenced by not only temperature and strain rate but also by microstructural evolution.

关键词： Microstructural evolution Dual-phase steel Lightweight component Hot deformation Dynamic recrystallization

Cold compression deformation method for reducing residual stress and uniformizing micro-property in ferrite steel

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Journal of Iron and Steel Research International 2022年第3期29卷 503-511页

作者： Bo Ning hui-bin wu Gang Niu Xin-pan Yu Collaborative Innovation Center of Steel Technology University of Science and Technology BeijingBeijing100083China Beijing Laboratory of Metallic Materials and Processing for Modern Transportation University of Science and Technology BeijingBeijing100083China

To reduce internal residual stress and homogenize micro-property of hot-rolled ferrite steel,the cold compression deformation method with small reduction rate has been performed in the hot-rolled samples,and X-ray diffraction and nanoindentation test have been used to detect the residual stress and *** samples with deformation rate of 0-5.59%or annealing at 550℃ are *** results show that,due to the coupling effect of thermal expansion and cold contraction and the volume expansion of microstructural transformation from austenite to ferrite,compressive residual stress was found inside the hot-rolled *** the increase in cold compression deformation,the dislocation density increased and the microhardness increased gradually,and there is no obvious rule for the change of mean nano-hardness in micro-zone for the center of ***,the uniformity of nano-hardness in the micro-zone increased first and then decreased,and the value of residual stress has obvious corresponding relationship with the uniformity of micro-zone *** cold compression deformation with appropriate reduction rate can reduce residual stress and improve nano-hardness uniformity of the hot-rolled samples,but more deformation(such as reduction rateε=5.59%)makes residual stress increase and makes uniformity of nano-hardness deteriorate.

关键词： Ferrite Cold compression deformation Residual stress Nano-hardness Uniformity Dislocation density