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Inductively Coupled Plasma(ICP) Mass Spectrometry(MS) Hyphenated with Atomic Emission Spectrometry(AES) for Simultaneous Determination of Major, Minor and Micro Amounts of Elements in Geochemical Samples

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Chemical Research in Chinese Universities 2005年第6期21卷 753-756页

作者： huang zhen-yu ZHANG Qin HU Ke WU Jian-ling YANG Peng-yuan Department of Chemistry Fudan University Shanghai 200433 P. R. China Academy of Chinese Geology Science Langfang 065000 P. R. China Lab Tech Beijing 101312 P. R. China Institute of Chemistry and Chemical Engineering Guangxi University Nanning 530004 P. R. China

Introduction Geological resource survey demands for determining various constituents including major, minor, micro, trace and ultra-trace levels of elements for preparing the map of resource distribution of our country. As a powerful and popularly used technique for multi-element analysis, inductively coupled plasma（ICP） atomic emission spectrometry （AES） has been applied to this field for a period of time. However, ICP spectrometric determination of those micro, trace and ultratrace elements needs enrichment procedures for improving the detection limit, which is unacceptable in case a great mass of samples should be analyzed as that in the task of geological resource survey. On the other hand, although ICP mass spectrometry （MS） is considered the most powerful method for trace elements determination, it is difficult for ICP-MS to be used to determine the trace and major analytes simultaneously in a spectrum.

关键词： ICP-MS ICP-AES Hyphenated method Geochemistry sample

High-precision,fast DEM reconstruction method for spaceborne InSAR

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Science China(Information Sciences) 2011年第11期54卷 2400-2410页

作者： WANG QingSong,huang HaiFeng,DONG zhen,yu AnXi & LIANG DianNong National University of Defense Technology,Changsha 410073,China National University of Defense Technology Changsha China

The primary objective of the spaceborne interferometric synthetic aperture radar (InSAR) system is to develop a consistent global digital elevation model (DEM).The improvement of the processing speed in global interferometry missions while maintaining the accuracy is becoming an important *** reconstruction is the most time-consuming step in the data processing required for spaceborne *** on a DEM reconstruction principle analysis,we exploited two basic characteristics of the mapping relation between the interferometric phase and 3-D position of target ***,the relation between the 3-D position of the target point and the interferometric phase can be approximated using ***,the corresponding polynomials change slowly in the local SAR ***,we verified the foundations of the two mentioned characteristics ***,we proposed a fast method of DEM reconstruction based on this *** descriptions of the step and key parameters of the fast algorithm are ***,the repeat-pass interferometric data obtained using TerraSAR-X was used to test the presented *** experimental results showed that a significant reduction in computation time is achieved with only a small loss in *** effectiveness and correctness of the proposed method were also validated.

关键词： interferometric synthetic aperture radar (InSAR) spaceborne SAR DEM reconstruction fast algorithm

Superconductivity of Nd_(1.85)Ce_(0.15)CuO_(4-y) by Electrochemical Oxidation

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Chinese Physics Letters 2000年第8期17卷 601-602页

作者： CHEN Ling CHE GUANG-CAN LI Hong DONG Cheng ZHOU Fang huang yu-zhen ZHAO Zhong-Xian National Laboratory for Superconductivity Institute of PhysicsChinese Academy of SciencesBeijing 100080 National Laboratory for Solid State Ionics Institute of PhysicsChinese Academy of SciencesBeijing 100080

Superconductivity of n-type superconductor Nd_(1.85)Ce_(0.15)CuO_(4-y)(NCCO)by electrochemical oxidation is re ported for the first time and the cyclic voltammogram curve for NCCO as working electrode is *** vestigations indicate that after oxidation,superconductivity of NCCO is improved:Tc is raised from 20 K up to 26 K,the superconducting volume fraction is increased *** valence electronic states of oxygen and copper in NCCO are studied by x-ray photoelectron *** is found that the Cu-2_(ps/2)peak shifts to the higher binding energy side about 0.4 e V,which indicates that the valence-state of copper ions is risen up after *** results imply that hole-carriers exist in n-type superconductor.

关键词： spectroscopy. copper Oxidation

Pharmacokinetics and tissue distribution of intraperitoneal 5-fluorouracil with a novel carrier solution in rats

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World Journal of Gastroenterology 2008年第14期14卷 2179-2186页

作者： Zhi-Gang Wei Guo-Xin Li Xiang-Cheng huang Li zhen Jiang yu Hai-Jun Deng Shan-Hua Qing Ce Zhang Department of General Surgery Nanfang Hospital Southern Medical University Guangzhou 510515 Guangdong Province China

AIM: To compare the pharmacokinetics and tissue distribution of 5-fluorouracil administered intraperitoneally with two isotonic carrier solutions: HAES-steri (neotype 6% hydroxyethyl starch), a novel carrier solution with middle molecular weight and physiologic saline (0.9% sodium chloride solution), a traditional carrier solution for intraperitoneal chemotherapy, in rats. METHODS: A total of 60 Sprague Dawley rats were randomized into groups according to the carrier solution administered. Each group was further randomized according to the intraperitoneal dwell period (1, 3, 6, 12, 18 and 24 h). At the end of the procedure the rats were killed, the peritoneal fluid was withdrawn completely and quantitated. Drug concentrations in peritoneal fluid, plasma, and tissues were determined by high- performance liquid chromatography. RESULTS: The mean volumes remaining in the peritoneal cavity were significantly higher with HAES- steri than those with physiologic saline at 1, 6, 12, 18, and 24 h (P = 0.047, 0.009, 0.005, 0.005 and 0.005 respectively, the percentages of remaining peritoneal fluid volume were 89.9 ± 5.6 vs 83.4 ± 4.9, 79.9 ± 2.8 vs 56.2 ± 15.7, 46.8 ± 5.5 vs 24.7 ± 9.7, 23.0 ± 2.8 vs 0.0 ± 0.0 and 4.2 ± 1.7 vs 0.0 ± 0.0 respectively). Mean concentrations in peritoneal fluid were significantly higher with HAES-steri than those with physiologic saline at 3, 12 and 18 h (P = 0.009, 0.009 and 0.005 respectively, the concentrations were 139.2768 ± 28.2317 mg/L vs mg/L, 11.5427 ± 3.0976 mg/L vs 0.0000 ± 0.0000 mg/L and 4.7724 ± 1.0936 mg/L vs 0.0000 ± 0.0000 mg/L respectively). Mean plasma 5-fluorouracil concentrations in portal vein were significantly higher with HAES-steri at 3, 12, 18 and 24 h (P = 0.009, 0.034, 0.005 and 0.019 respectively, the concentrations were 3.3572 ± 0.8128 mg/L vs 0.8794 ± 0.2394 mg/L, 0.6203 ± 0.9935 mg/L vs 0.0112 ± 0.0250 mg/L, 0.3725 ± 0.3871 mg/L vs 0.0000 ± 0.0000 mg/L, and 0.2469 ± 0.1457 mg/L vs 0.0000 ± 0.0000 mg/L respectively),

关键词： Carrier solutions Intraperitoneal chemo- therapy 5-fluorouracil Pharmacokinetics Tissue distribution

Integration of Electrical Properties and Polarization Loss Modulation on Atomic Fe–N‑RGO for Boosting Electromagnetic Wave Absorption

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Nano-Micro Letters 2025年第2期17卷 517-532页

作者： Kaili Zhang yuefeng Yan zhen Wang Guansheng Ma Dechang Jia Xiaoxiao huang yu Zhou State Key Laboratory of Precision Welding&Joining of Materials and Structures Harbin Institute of TechnologyHarbin 150001People’s Republic of China School of Materials Science and Engineering Harbin Institute of TechnologyHarbin 150001People’s Republic of China MIIT Key Laboratory of Advanced Structural‑Functional Integration Materials&Green Manufacturing Technology Harbin Institute of TechnologyHarbin 150001People’s Republic of China

Developing effective strategies to regulate graphene’s conduction loss and polarization has become a key to expanding its application in the electromagnetic wave absorption(EMWA)*** on the unique energy band structure of graphene,regulating its bandgap and electrical properties by introducing heteroatoms is considered a feasible ***,metal-nitrogen doping reduced graphene oxide(M–N-RGO)was prepared by embedding a series of single metal atoms M–N_(4) sites(M=Mn,Fe,Co,Ni,Cu,Zn,Nb,Cd,and Sn)in RGO using an N-coordination atom-assisted *** composites had adjustable conductivity and polarization to optimize dielectric loss and impedance matching for efficient EMWA *** results showed that the minimum reflection loss(RL_(min))of Fe–N-RGO reaches−74.05 dB(2.0 mm)and the maximum effective absorption bandwidth(EAB_(max))is 7.05 GHz(1.89 mm)even with a low filler loading of only 1 wt%.Combined with X-ray absorption spectra(XAFS),atomic force microscopy,and density functional theory calculation analysis,the Fe–N_(4) can be used as the polarization center to increase dipole polarization,interface polarization and defect-induced polarization due to d-p orbital hybridization and structural ***,electron migration within the Fe further leads to conduction loss,thereby synergistically promoting energy *** study demonstrates the effectiveness of metal-nitrogen doping in regulating the graphene′s dielectric properties,which provides an important basis for further investigation of the loss mechanism.

关键词： Electromagnetic wave absorption Fe-N-RGO Dipole polarization Conduction loss Impedance matching

The integrated monitoring system for running parameters of key mining equipment based on condition monitoring technology

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Journal of Coal Science & Engineering(China) 2010年第1期16卷 108-112页

作者： BIN Guang-fu LI Xue-jun BALBIR S Dhillon huang zhen-yu GUO Deng-ta Key Lab of Health Maintenance for Mechanical Equipment of Hunan Province Hunan University of Science and Technology Xiangtan 411201 China Department of Mechanical Eng. Univ/Ottawa Ottawa K1B 6N5 Canada Xiangtan Liangchuan Coal Mine Machine Co. Ltd. Xiangtan 411104 China Xiangtan Electric Manufacturing Corporation Ltd. Xiangtan 411101 China

An integrated monitoring system for running parameters of key mining equipmenton the basis of condition monitoring technology and modern communication networktechnology was *** system consists of a client computer with functions ofsignal acquisition and processing, and a host computer in the central control *** acquisition module of the client computer can collect the running parameters fromvarious monitoring terminals in *** DSP high-speed data processing system ofthe main control module can quickly achieve the numerical calculation for the *** signal modulation and signal demodulation are completed by the frequencyshift keying circuit and phase-locked loop frequency circuit, ***, the signalis sent to the host computer for logic estimation and diagnostic analysis using the networkcommunication technology, which is helpful for technicians and managers to control therunning state of equipment.

关键词： mining key equipment running parameters condition monitoring signal acquisition and processing integrated monitoring

Dynamic Regulation of Hydrogen Bonding Networks and Solvation Structures for Synergistic Solar‑Thermal Desalination of Seawater and Catalytic Degradation of Organic Pollutants

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Nano-Micro Letters 2025年第2期17卷 548-565页

作者： Ming‑yuan yu Jing Wu Guang Yin Fan‑zhen Jiao Zhong‑zhen yu Jin Qu Beijing Key Laboratory of Advanced Functional Polymer Composites Beijing University of Chemical TechnologyBeijing 100029People’s Republic of China State Key Laboratory of Organic‑Inorganic Composites College of Materials Science and EngineeringBeijing University of Chemical TechnologyBeijing 100029People’s Republic of China

Although solar steam generation strategy is efficient in desalinating seawater,it is still challenging to achieve continuous solar-thermal desalination of seawater and catalytic degradation of organic ***,dynamic regulations of hydrogen bonding networks and solvation structures are realized by designing an asymmetric bilayer membrane consisting of a bacterial cellulose/carbon nanotube/Co_(2)(OH)_(2)CO_(3)nanorod top layer and a bacterial cellulose/Co_(2)(OH)_(2)CO_(3)nanorod(BCH)bottom ***,the hydrogen bonding networks inside the membrane can be tuned by the rich surface–OH groups of the bacterial cellulose and Co_(2)(OH)_(2)CO_(3)as well as the ions and radicals in situ generated during the catalysis ***,both SO_(4)^(2−)and HSO_(5)−can regulate the solvation structure of Na^(+)and be adsorbed more preferentially on the evaporation surface than Cl^(−),thus hindering the de-solvation of the solvated Na^(+)and subsequent nucleation/growth of ***,the heat generated by the solar-thermal energy conversion can accelerate the reaction kinetics and enhance the catalytic degradation *** work provides a flow-bed water purification system with an asymmetric solar-thermal and catalytic membrane for synergistic solar thermal desalination of seawater/brine and catalytic degradation of organic pollutants.

关键词： Solar steam generation Seawater desalination Catalytic degradation Bacterial cellulose Cobalt hydroxycarbonate nanorods

连接界面不定性对于加筋板结构振动能量传递特性的影响分析

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振动与冲击 2015年第21期34卷 184-187,199页

作者：纪琳黄震宇山东大学机械工程学院济南250061 上海交通大学电子信息与电气工程学院上海200240

加筋板结构有着极为广泛的工程应用,准确预测振动能量(结构声)在加筋板中的传递特性是对于工程结构进行有效、合理声学设计的一个极为重要的环节。本文以板-筋-板组合系统为研究对象,将加强筋视为板件结构的中间连接件,通过仿真分析计算... 详细信息

加筋板结构有着极为广泛的工程应用,准确预测振动能量(结构声)在加筋板中的传递特性是对于工程结构进行有效、合理声学设计的一个极为重要的环节。本文以板-筋-板组合系统为研究对象,将加强筋视为板件结构的中间连接件,通过仿真分析计算,研究了加筋板的参数不确定性对筋板组合系统的功率流传递特性影响。考虑到加强筋与所连接板件通常具有较大的动态特性差异,仿真模拟以中频混合分析法(Hybrid FE-SEA method)为主。研究表明:在长短波并存的中频域,加筋板中的结构声传递特性受加强筋刚度和边界条件变化的影响较大,而受其材料属性和连接自由度数量变化的影响较小。

关键词：振动传递中频混合模型法统计能量法参数不确定性加筋板结构

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松突圆蚧化学防治技术研究

南京林业大学学报（自然科学版） 2006年第5期30卷 119-122页

作者：黄振裕福建省森林病虫害防治检疫总站福建福州350003

利用混合及单一杀虫剂,采用注干、涂干等方法对松突圆蚧进行林间药效试验,同时对几种方法处理后的松突圆蚧种群消长情况进行跟踪调查。结果表明:注干和涂干法处理时,混合药剂的最佳组合均为40%杀扑磷乳油(V(杀扑磷乳油)∶V(水)=1∶5)+40... 详细信息

利用混合及单一杀虫剂,采用注干、涂干等方法对松突圆蚧进行林间药效试验,同时对几种方法处理后的松突圆蚧种群消长情况进行跟踪调查。结果表明:注干和涂干法处理时,混合药剂的最佳组合均为40%杀扑磷乳油(V(杀扑磷乳油)∶V(水)=1∶5)+40%毒死蜱乳油(V(毒死蜱乳油)∶V(水)=1∶5)+40%氧乐果乳油(V(氧乐果乳油)∶V(水)=1∶2.5)混合,采用注干法和涂干法的防治效果分别达98%和81%,虫口减退较明显,而喷雾法处理的虫口波动较大。

关键词：松突圆蚧化学防治注干法涂干法喷雾法