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Late Early-Cretaceous Magma Mixing in the Langqi Island, Fujian Province, China: Evidences from Petrology, Geochemistry and Zircon Geochronology

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Journal of Earth Science 2020年第3期31卷 468-480页

作者： Liangliang Huang Liyuan wang hong-rui Fan Musen Lin Wenhui Zhang Key Laboratory of Mineral Resources Institute of Geology and GeophysicsChinese Academy of SciencesBeijing 100029China College of Zijin Mining Fuzhou UniversityFuzhou 350116China

The mafic enclaves from Mesozoic intermediate-acid magmatic rocks,widely developed along Fujian coast,are considered to be the results of large-scale crust-mantle interaction and magma *** this paper,petrography,mineralogy,and geochemistry of granites and mafic microgranular enclaves(MMEs)in Langqi Island are studied to provide new information for tracing crust-mantle *** zircon U-Pb dating results show that the Langqi rocks were formed at^101 Ma,which are metaluminous,enriched in silica and high-K calc-alkaline I-type *** enclaves have a typical magmatic structure,which is characterized by magma mixing between high-temperature basic magma and low-temperature acidic magma through *** enclaves and host granites show a tendency to mixed major and trace elements,displaying a clear-cut contact relationship,which is indicative of coeval *** genesis of Langqi rocks is related to the extensional setting caused by the subduction of Paleo-Pacific Plate,and they are the results of mixing of subduction-related metasomatized mantle-derived mafic and induced crustal-melted granitic magma originating from partial melting of the crustal material.

关键词： magma mixing granite mafic microgranular enclaves Langqi Fujian

Formation mechanism and preparation of YAl_(2) intermetallics by electro-deoxidation with different sintering conditions

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Rare Metals 2023年第3期42卷 1067-1074页

作者： Yue-Shan Wei Shi-hong Yan Lin Zhou De-hong Chen rui-Ying Miao Zhi-Qiang wang National Engineering Research Center for Rare Earth Materials General Research Institute for Nonferrous MetalsBeijing 100088China Grirem Advanced Materials Co. Beijing 100088China

A study was carried out on the preparation of YAl_(2) intermetallics from mixed oxide precursors using the method of electro-deoxidation.Y2O_(3) and Al_(2)O_(3) mixed in molar proportions of 1:2 were sintered at temperatures ranging from 800 to 12000C for different *** sintered pellet was then electrolyzed in a molten CaCl_(2) at850℃using a graphite anode at a potential of 3.1 *** this work,effects of sintering on the composition and the oxygen content in cathodic products were studied by X-ray diffraction(XRD)and oxygen-nitrogen *** mainly affects the porosity of the pellets,and it is found that porosity decreases gradually with the increase in sintering temperature and the extension of sintering *** sintered at 9000C for 4 h,the oxygen content in the cathodic product decreases to 1.85 wt%,and the efficiency of electro-deoxidation is 94.48%.At the same time,the mechanism of electrolysis was *** results suggest that the formation of YAl_(2) is a multi-step *** the reduction process from mixed oxides Y2O_(3)/Al_(2)O_(3) to YAl_(2) included many intermediate materials,such as YAlO_(3),Y3Al5O12 and YAl3,YAl_(2) intermediate alloy was prepared finally.

关键词： Yttrium aluminum oxide Molten salts YAl_(2)alloy Electro-deoxidation

Novel evaluation method for metal workability during cross wedge rolling process

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Advances in Manufacturing 2021年第3期9卷 473-481页

作者： Ming Cheng Ming-Jie Shi Petrenko Vladimir rui-Xue wang Shi-hong Zhang Institute of Metal Research(IMR) Chinese Academy of Sciences(CAS)Shenyang110016People’s Republic of China School of Materials Science and Engineering University of Science and Technology of ChinaHefei230026People’s Republic of China Physical-Technical Institute of the National Academy of Sciences of Belarus 220141MinskBelarus

This study presents a novel method using a disk-like sample to assess the workability of metal during the cross wedge rolling(CWR)*** this method,we can quantitatively evaluate the moment destruction which occurs at the center of the sample during *** this study,45 steel was selected to demonstrate the proposed ***,we designed a model for the tools and sample,conducted finite element simulations to analyze the distribution regulations of metal flow,stress,and strain,and evaluated the relationship between the damage and moving distance of the tool during the forming ***,we obtained the optimal deformation temperature range,rolling speed,and geometry parameters for the ***,experiments were conducted from 20℃ to 1200℃ to verify the accuracy of the developed *** was demonstrated that the model was significantly accurate in accessing the workability of 45 steel in the CWR *** proposed method could be generalized to investigate the CWR process for other materials,such as aluminum alloys,superalloys,titanium alloys,etc.

关键词： Cross wedge rolling(CWR) 45 steel Workability Damage Finite element simulation

Effect of Hydrostatic Pressure on LPSO Kinking and Microstructure Evolution of Mg–11Gd–4Y–2Zn–0.5Zr Alloy

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Acta Metallurgica Sinica(English Letters) 2021年第2期34卷 248-264页

作者： Ce Zheng Shuai-Feng Chen rui-Xue wang Shi-hong Zhang Ming Cheng Institute of Metal Research Chinese Academy of SciencesShenyang 110016China University of Chinese Academy of Sciences Beijing 100049China Department of Materials Science and Engineering and Research Institute of Advanced Materials(RIAM) Seoul National UniversitySeoul 08826Republic of Korea

Two different kinds of hot compressions,namely normal-compression and can-compression,were performed on the Mg–11 Gd–4 Y–2 Zn–0.5 Zr alloy,featured with long period stacking ordered(LPSO)*** kinking behavior of LPSO phase and microstructure evolution was investigated to clarify the effect of levels of imposed hydrostatic *** results suggest that the LPSO phases including both the intragranular 14 H-LPSO phase and intergranular 18 R-LPSO phase suffer severe kinking behavior under higher hydrostatic pressure induced by can-compression,which is firstly characterized with more kinking times and smaller relative kinking *** main reason for such enhanced LPSO kinking during cancompression may be mainly ascribed to the higher dislocation density under a higher level of hydrostatic ***,a competitive relationship between the kink behaviors of intergranular 18 R-LPSO phase and intragranular 14 H-LPSO phase was *** is,the intergranular 18 R-LPSO phase only kinks obviously on the condition that the surrounded intragranular 14 H-LPSO phase scarcely *** contrast to the distinctive kinking of LPSO phase,the dynamic recrystallization(DRX)mechanism shows less dependence on the hydrostatic ***,similar DRX fractions and crystallographic texture were attained for two compression processes owing to the similar operation of deformation mode.

关键词： Magnesium alloy Hydrostatic pressure Long period stacking ordered(LPSO)phase Kinking Dynamic recrystallization

Conducting polymer-functionalized mesoporous metal-organic frameworks for high-performance Li-S battery

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Nano Research 2023年第4期16卷 4867-4873页

作者： Xiao-Fei Liu Ya-rui wang hong Chen Bo Li Shuang-Quan Zang Henan Key Laboratory of Crystalline Molecular Functional Materials Henan International Joint Laboratory of Tumor Theranostical Cluster MaterialsGreen Catalysis Center and College of ChemistryZhengzhou UniversityZhengzhou 450001China Collaborative Innovation Center of Water Security for Water Source Region of Mid-line of South-to-North Diversion Project of Henan Province College of Chemistry and Pharmacy EngineeringNanyang Normal UniversityNanyang 473061China

It was known that mesoporous metal-organic frameworks(MOFs)with hierarchical pores and unsaturated metal sites can effectively inhibit the shuttle effect of lithium polysulfides in lithium-sulfur battery,however,the unsatisfactory structural stability and electrical conductivity limit the application of mesoporous MOFs(MMOFs)in Li-S *** at sensible solutions,the conductive polyaniline(PANI)was incorporated into the MMOF to enhance the discharge capacity and the cycling stability of proposed Li-S batteries,as the stability and the conductivity of the MMOF cathode was improved *** activated MMOF-PANI provides physical and chemical adsorption of polysulfides against their shuttle ***,the introduction of PANI into the channels of MMOF effectively improves the conductivity of MMOF,thus improving the electrochemical performance of the MMOF-PANI-based *** from these synergetic effects,the S@MMOF-PANI cathode delivers improved electrochemical performance including excellent rate performance and cycling *** battery shows an initial capacity of 777.7 mAh·g^(−1)at 2.0 C and a low decay rate of 0.06%per cycle in 1,000 cycles and approximately a repeatable rate performance.

关键词： metal-organic framework conductivity mesoporous shuttle effect Li-S battery

Vertically aligned W(Mo)S_(2)/N-W(Mo)C-based light-assisted electrocatalysis for hydrogen evolution in acidic solutions

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Rare Metals 2023年第5期42卷 1535-1544页

作者： Lan-Fang wang rui-Xia Yang Jin-Zhi Fu Yue-Yue Cao rui-Fang Ding Xiao-hong Xu Key Laboratory of Magnetic Molecules and Magnetic Information Materials of Ministry of Education&School of Chemistry and Materials Science of Shanxi Normal University Taiyuan030032China Kunshan Superior Silk Screen Printing Material Co. Ltd.Suzhou215300China

The development of non-noble-metal hydrogen evolution electrocatalysts holds great promises for a sustainable energy ***,a hybrid W(Mo)S_(2)/NW(Mo)C nanosheet with array structures was reported for an efficient light-as sis ted hydrogen evolution electrocatalysts in acidic *** resulting vertically aligned W(Mo)S_(2)/N-W(Mo)C was supported on a conductive carbon fiber paper,which can be produced through annealing W(Mo)S_(2)nanosheets by simultaneous carbonization and N-doping in Ar/H_(2)*** optimized WS_(2)/NWC and MoS_(2)/N-MoC electrode exhibits remarkable lightassisted electrocatalysis activity with overpotentials of0.120 and 0.122 V at 10 mA·cm^(-1)in acidic solutions,*** high hydrogen evolution activities should be attributed to the electrocatalytic synergistic effects of the abundant active sites existing in different phase boundaries and the absorption for ultraviolet-visible *** study shows that synthesis of low-cost and highly active W(Mo)S_(2)-based hydrogen evolution electrocatalyst opens up a route toward the development of scalable production of hydrogen fuels.

关键词： W(Mo)S_(2)/N-W(Mo)C heterostructures Vertically aligned nanosheets Hydrogen evolution Lightassisted electrocatalysis

Effect of boron addition on microstructure and mechanical properties of an additively manufactured superalloy

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Journal of Iron and Steel Research International 2023年第3期30卷 601-609页

作者： rui wang Dao-hong wang Peng Zhang Zhi-qing Yang Jing-jing Liang Jin-guo Li Shi-Changxu Innovation Center for Advanced Materials Institute of Metal ResearchChinese Academy of SciencesShenyang 110016LiaoningChina School of Materials Science and Engineering University of Science and Technology of ChinaHefei 230026AnhuiChina Jiang Su Feiyue Machine and Pump Group Co. Ltd.Jingjiang 225300JiangsuChina

The effect of boron addition(0.010,0.015,and 0.020 wt.%)on the microstructure and mechanical properties of an additively manufactured superalloy was *** as-built microstructure was investigated by scanning electron microscopy and transmission electron *** results demonstrate that boron precipitates as M_(3)B_(2)boride at the grain *** increase in boron content increases the amount ofγ/γ′eutectic and the size and fraction of M_(3)B_(2)*** creates nanoscale fine borides at grain boundaries,which significantly reinforces grain *** mechanical property analysis indicated that the addition of boron improved the tensile ductility at 760℃and stress rupture properties at 760℃/780 ***,with the excessive addition of boron,the mechanical property was reduced.

关键词： Additive manufacturing Superalloy Boron Grain boundary Stress rupture Tension

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自激式电感耦合等离子体光源设计及光谱分析

光谱学与光谱分析 2025年第1期45卷 66-71页

作者：卢思贤龙开红詹陈锐李明北方工业大学电气与控制工程学院北京100144 益阳职业技术学院电子与信息工程学院湖南益阳413055

电感耦合等离子体(ICP)光谱仪是一种应用范围很广的元素分析仪,主要用于元素定性与定量的分析。ICP光源是光谱仪的核心部件,它在光谱仪中扮演着至关重要的角色。目前主流的ICP光源有两种:自激式和他激式,各自具有优缺点。他激式光源电... 详细信息

电感耦合等离子体(ICP)光谱仪是一种应用范围很广的元素分析仪,主要用于元素定性与定量的分析。ICP光源是光谱仪的核心部件,它在光谱仪中扮演着至关重要的角色。目前主流的ICP光源有两种:自激式和他激式,各自具有优缺点。他激式光源电路复杂、体积庞大、阻抗匹配速度较慢、最大输出功率有限。设计了一种基于镀金工艺的高功率MOSFET和变频实现阻抗匹配的自激式ICP光源,该光源采用射频放大和阻抗匹配一体化的设计,把从负载线圈采样的频率信号f_(1)以及功率放大电路放大后的频率相位f_(0)进行相位比较,再根据两者相位差的变化,进而控制频率的变化,实现阻抗匹配;设计上采用了镀金工艺的金属化硅N通道型高功率的MOSFET实现功率放大,具有更大的功率密度、更小的体积,最大输出功率超过2400 W。对研制的ICP光源进行了电学静态测试,给出了鉴相器、压控振荡器以及功率的输出特性,验证了各电路在相应工作状态下的性能表现;同时结合光谱仪进行了包含Ba、Na和Li元素标准溶液的测试,获得了目标元素的光谱信号;另外,对获得的光谱信号进行了处理,使用了基于EEMD特征增强的方法对目标元素光谱信号进行有效增强,信号的线性决定系数(R^(2))从0.97降至0.99,相对标准偏差(RSD)从6.47%降至1.07%,增强了信号的准确性和可用性。本文所研制的自激式ICP光源,通过射频放大和阻抗匹配一体化设计缩小了体积,变频技术使阻抗匹配速度从毫秒级提升到纳秒级,镀金工艺的MOSFET技术使最大输出功率从原来的1800 W增加到2400 W,为ICP光源的进一步优化和应用奠定了基础,具有重要的科学研究和工程实践意义。

关键词：自激式ICP光源阻抗匹配光谱信号 EEMD算法

Effects of bortezomib in sensitizing human prostate ：ancer cell lines to NK-mediated cytotoxicity

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Asian Journal of Andrology 2012年第5期14卷 695-702页

作者： Wei Hu rui-rui Zheng Hui-Xia Cui Dan Yue Yong wang You-hong Jiang Cancer Research Institute First Affiliated HospitalChina Medical UniversityShenyang 110001China Department of Laboratory Medicine Tianjin Medical University Tianjin 300192China Tianjin Institute of Urology Tianjin Medical UniversityTianjin 300192China

The proteasome inhibitor, bortezomib, has been demonstrated to sensitize tumor cells to tumor necrosis factor-related apoptosis-inducing ligand （TRAIL）-mediated apoptosis. Natural killer （NK） cells represent potent antitumor effector cells. They also express TRAIL. Therefore, we investigated whether bortezomib could sensitize tumor cells to NK cell-mediated killing, and have the same effect in human prostate cancer cell lines （LNCaP and DU145）. We found that bortezomib strongly inhibits proliferation in both cell lines. Furthermore, compared with LNCaP cells, DU145 cells are more sensitive to bortezomib-induced apoptosis. However, bortezomib is unable to sensitize these two cell lines to NK cell-mediated killing in short-term assays. In long-term assays, we found that killing mediated by activated NK cells following bortezomib treatment leads to greater antitumor effects than either treatment alone. In addition, treatment with bortezomib causes these cells to upregulate apoptosis-related mRNA as well as death receptors and downregulate the major histocompatibility class （MHC）-I molecule on the cell surface of DU145 cells. In contrast, LNCaP cells are not sensitized by this treatment. Death receptors and the MHC-I molecule did not change in this cell line. These data suggest that bortezomib can be used to sensitize prostate cancer cells to NK cell-mediated killing and improve current cancer therapies. This theral）eutic stratelzv may be more effective in I）atients with androeen-insensitive orostate cancer.

关键词： bortezomib DU145 cells human prostate cancer LNCaP ceils NK cells